Publication Cover
Journal of Environmental Science and Health, Part B
Pesticides, Food Contaminants, and Agricultural Wastes
Volume 44, 2009 - Issue 3
217
Views
14
CrossRef citations to date
0
Altmetric
ARTICLES

Evaluation of a multiresidue method for pesticides in cereals using supercritical fluid extraction and gas chromatographic detection

, , &
Pages 204-213 | Received 02 Sep 2008, Published online: 11 Mar 2009

References

  • Luke , M. A. , Froberg , J. E. and Masumoto , H. T. 1975 . Extraction and cleanup of organochlorine, organophosphate, organonitrogen, and hydrocarbon pesticides in produce for determination by gas-liquid chromatography . J. Assoc. Off. Anal. Chem. , 58 : 1020 – 1026 .
  • Stan , H. J. 2000 . Pesticide residue analysis in foodstuffs applying capillary gas chromatography with mass spectrometric detection . J. Chromatogr. A , 892 : 347 – 377 .
  • Štajnbaher , D. and Zupančič-Kralj , L. 2003 . Multiresidue method for determination of 90 pesticides in fresh fruits and vegetables using solid-phase extraction and gas chromatography-mass spectrometry . J. Chromatogr. A , 1015 : 185 – 198 .
  • Hernando , M. D. , Agüera , A. , Fernández-Alba , A. R. , Piedra , L. and Contreras , M. 2001 . Gas chromatographic determination of pesticides in vegetable simples by sequential positive and negative chemical ionization and tandem mass spectrometric fragmentation using an ion trap analyzer . Analyst , 126 : 46 – 51 .
  • Andersson , A. and Pålsheden , H. 1991 . Comparison of the efficiency of different GLC multiresidue methods on crops containing pesticide residues . Fr. J. Anal. Chem. , 339 : 365 – 367 .
  • Lee , M. S. , Papathakis , M. L. , Feng , H. M.C. , Hunter , G. F. and Carr , J. E. 1991 . Multipesticide residue method for fruits and vegetables: California Department of Food and Agriculture . Fr. J. Anal. Chem. , 339 : 376 – 383 .
  • Anastassiades , M. , Lehotay , S. J. , Štajnbaher , D. and Schenck , F. J. 2003 . Fast and easy multiresidue method employing acetonitrile extraction/partitioning and dispersive solid-phase extraction for the determination of pesticide residues in produce . J. AOAC Int. , 86 : 412 – 431 .
  • Fillion , J. , Sauvé , F. and Selwyn , J. 2000 . Multiresidue methods for the determination of residues of 251 pesticides in fruits and vegetables by gas chromatography/mass spectrometry and liquid chromatography with fluorescence detection . J. AOAC Int. , 83 : 698 – 713 .
  • Andersson , A. and Palsheden , H. 1998 . Multiresidue methods for analysis of pesticide residues in fruits and vegetables using ethyl acetate extraction, GPC clean up and GC determination . Livsmedels-verket Rapport , 17 : 9 – 41 .
  • Schenck , F. J. and Howard-King , V. 1999 . Rapid solid phase extraction clean up for pesticide residues in fresh fruits and vegetables . Bull. Environ. Contam. Toxicol. , 63 : 277 – 281 .
  • Liu , P. , Liu , Q. , Ma , Y. , Liu , J. and Jia , X. 2006 . Analysis of pesticide multiresidues in rice by gas chromatography-mass spectrometry . Chinese Journal of Chromatography , 24 : 228 – 234 .
  • Lehotay , S. J. 1997 . Supercritical fluid extraction of pesticides in food . J. Chromatogr. A , 785 : 289 – 312 .
  • Mc Hugh , M. A. and Krukonis , V. J. 1986 . Supercritical Fluid Extraction. Principles and Practice , Boston : Butterworths .
  • Hawthorne , S. B. 1990 . Analytical-scale supercritical fluid extraction . Anal. Chem. , 62 : 633A – 642A .
  • Valverde , A. , Fernández-Alba , A. R. , Agüera , A. and Contreras , M. 1995 . Extraction of methamidophos residues from vegetables with supercritical fluid carbon dioxide . J. AOAC Int. , 78 : 867 – 876 .
  • Lehotay , S. J. and Eller , K. I. 1992 . Development of a method of analysis for 46 pesticides in fruits and vegetables by supercritical fluid extraction and gas chromatography/ion trap mass spectrometry . J. AOAC Int. , 78 : 821 – 830 .
  • Lehotay , S. J. and Valverde , A. 1997 . Evaluation of different solid-phase traps for automated collection and clean-up in the analysis of multiple pesticides in fruits and vegetables after supercritical fluid extraction . J. Chromatogr. A , 765 : 69 – 84 .
  • Valverde , A. , Fernandez-Alba , A. R. , Contreras , M. and Agüera , A. 1996 . Supercritical fluid extraction of pesticides from vegetables using anhydrous magnesium sulfate for sample preparation . J. Agric. Food Chem. , 44 : 1780 – 1784 .
  • Boulaid , M. , Aguilera , A. , Busonera , V. , Camacho , F. , Monterreal , A. V. and Valverde , A. 2007 . Assessing supercritical fluid extraction for the analysis of friponil, kresoxim-methyl, acrinathrin, and pyridaben residues in melon . J. Environ. Sci. Health, Part B , 42 : 809 – 815 .
  • Fiddler , W. , Pensabene , J. W. , Gates , R. A. and Donoghue , D. J. 1999 . Supercritical fluid extraction of organochlorine pesticides in eggs . J. Agric. Food Chem. , 47 : 206 – 211 .
  • Juhler , R. K. 1998 . Supercritical fluid extraction of pesticides from meat: a systematic approach for optimisation . The Analyst , 123 : 1551 – 1556 .
  • Rissato , S. R. , Galhiane , M. S. , Knoll , F. R.N. and Apon , B. M. 2004 . Supercritical fluid extraction for pesticide multiresidue analysis in honey: determination by gas chromatography with electron-capture and mass spectrometry detection . J. Chromatogr. A , 1048 : 153 – 159 .
  • Kim , D. H. , Heo , G. S. and Lee , D. W. 1998 . Determination of organophoshorus pesticides in wheat flour by supercritical fluid extraction and gas chromatography with nitrogen-phosphorus detection . J. Chromatogr. A , 824 : 63 – 70 .
  • Izquierdo , A. , Tena , M. T. , Luque de Castro , M. D. and Valcarcel , M. 1996 . Supercritical fluid extraction of carbamate pesticides from soils and cereals . Chromatographia , 42 : 206 – 212 .
  • Eller , K. I. and Lehotay , S. J. 1997 . Evaluation of hydromatrix and magnesium sulphate drying agents for supercritical fluid extraction of multiple pesticides in produce . The Analyst , 122 : 429 – 435 .
  • Aguilera , A. , Brotons , M. , Rodriguez , M. and Valverde , A. 2003 . Supercritical fluid extraction of pesticides from a table-ready food composite of plant origin (gazpacho) . J. Agric. Food Chem. , 51 : 5616 – 5621 .
  • Ohlin , B. 1998 . Pesticide analytical methods in Sweden . Part 1: A capillary gas chromatographic multi-residue method for the determination of pesticides in cereals and cereals products. Livsmedelsverket Rapport , 17 : 75 – 86 .
  • Aguilera , A. , Rodriguez , M. , Brotons , M. , Boulaid , M. and Valverde , A. 2005 . Evaluation of Supercritical Fluid Extraction/Aminopropyl Solid-Phase “in-line” Cleanup for Analysis of Pesticide Residues in Rice . J. Agric. Food Chem. , 53 : 9374 – 9382 .
  • McNally , M. E.P. 1995 . Advances in environmental SFE . Anal. Chem. , 67 : 308 – 315 .
  • Hopper , M. L. 1999 . Automated one-step supercritical fluid extraction and clean up system for the analysis of pesticide residues in fatty matrices . J. Chromatogr. A , 840 : 93 – 105 .
  • Poustka , J. , Holadová , K. and Hajšlová , J. 1995 . Application of supercritical fluid extraction for analysis of organophosphates in cereals . Int. J. Environ. Anal. Chem. , 60 : 139 – 144 .
  • European Commision, Directorate General Health and Consumer Protection (DG-SANCO) . Method Validation and Quality Control Procedures for Pesticide Residues Analysis in Food and Feed Document SANCO/2007/3131, October 31, 2007. EC, Brussels
  • Ambrus , A. , Solymosné , M. E. and Korsós , I. 1996 . Estimation of uncertainty of sample preparation for the analysis of pesticide residues . J. Environ. Sci. Health, Part B , 31 : 443 – 450 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.