References
- Europe Commission. Commission Regulation (EC) No 293/2013 of 20th March 2013 amending Annex II and III to Regulation (EC) No 396/2005 of the European parliament and of the Council as regards maximum residue levels for emamectin, benzoate, etofenprox, etoxazole, flutriafol, glyphosate, phosmet, pyraclostrobin, spinosad and spirotetramat in or on certain products. Off. J. Eur. Union I.96 of 5.4.2013. https://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2013:096:0001:0030:en:PDF.
- Granby, K.; Johannesen, S.; Vahl, M. Analysis of glyphosate residues in cereals using liquid chromatography-mass spectrometry (LC-MS/MS). Food Addit. Contam. 2003, 20, 692–698. DOI:https://doi.org/10.1080/0265203031000109477.
- Chiarello, M.; Jiménez-Medina, M. L.; Marín Saéz, J.; Moura, S.; Garrido Frenich, A.; Romero-González, R. Fast analysis of glufosinate, glyphosate and its main metabolite, aminomethylphosphonic acid, in edible oils, by liquid chromatographycoupled with electrospray tandem mass spectrometry. Food Addit. Contam. Part A Chem. Anal. Control Expo Risk Assess 2019, 36, 1376–1384. DOI:https://doi.org/10.1080/19440049.2019.1631493.
- Kruve, A.; Auling, R.; Herodes, K.; Leito, I. Study of liquid chromatography/electrospray ionization mass spectrometry matrix effect on the example of gluphosate analysis from cereals. Rapid Commun. Mass Spectrom. 2011, 25, 3252–3258. DOI:https://doi.org/10.1002/rcm.5222.
- Adams, S.; Guest, J.; Dickinson, M.; Fussell, R. J.; Beck, J.; Schoutsen, F. Development and validation of ion chromatography-tandem mass spectrometry-based method for the multiresidue determination of polar ionic pesticides in food. J Agric Food Chem 2017, 65, 7294–7304. DOI:https://doi.org/10.1021/acs.jafc.7b00476.
- Gasparini, M.; Angeloni, B.; Ferretti, E. Glyphosate and highly polar pesticides in fruit, vegetables and honey using ion chromatography coupled with high resolution mass spectrometry. Method validation and its applicability in an official laboratory. J. Mass Spectrum 2020, 4624–4637. DOI:https://doi.org/10.1002/jms.4624.
- Granby, K.; Vahl, M. Investigation of the herbicide glyphosate and the plant growth regulators chlormequat and mepiquat in cereals produced in denmark. Food Addit. Contam. 2001, 18, 898–905. DOI:https://doi.org/10.1080/02652030119594.
- Yang, J.; Zhaoyun, C.; Ruilin, J.; Hui, Q.; Mingxue, C. Determination of glyphosate and aminomethylphophonic acid in rice using hydrophilic interaction chromatography-tandem mass spectrometry. Se Pu 2012, 30, 39–44. : DOI:https://doi.org/10.3724/sp.j.1123.2011.08040.
- Botero-Coy, A. M.; Ibáñez, M.; Sancho, J. V.; Hernández, F. Direct liquid chromatography-tandem mass spectrometry determination of underivatized glyphosate in rice, maize and soybean. J. Chromatogr. A. 2013, 1313, 157–165. DOI:https://doi.org/10.1016/j.chroma.2013.07.037.
- Santilio, A.; Pompili, C.; Giambenedetti, A. Determination of glyphosate residue in maize and rice using a fast and easy method involving liquid chromatography-mass spectrometry LC/MS/MS. J. Environ. Sci. Health Part B 2019, 54, 205–210. DOI:https://doi.org/10.1080/03601234.2018.1550306.
- Cutillas, V.; Fernandez-Alba, A. R. Analysis by LC-MS/MS of polar pesticides in fruits and vegetables using new hybrid stationary phase . MethodsX 2021, 8, 101306. DOI:https://doi.org/10.1016/j.mex.2021.101306.
- European Commission. SANTE/12682/2019. Guidance document on analytical quality control and method validation procedures for pesticides residues analysis in food and feed. Available at https://www.eurl-pesticides.eu/userfiles/file/EurlALL/AqcGuidance_SANTE_2019_12682.pdf.
- Magnusson, B.; Örnemark, U. The Fitness for Purpose of Analytical Methods – a Laboratory Guide to Method Validation and Related Topics. 2nd ed. Eurachem Guide, 2014. Available at https://www.eurachem.org/index.php/publications/guides/mv