References
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- TLC was carried out on glass plates coated with silica gel G (E. Merck) using solvent system A (ethyl acetate/acetic acid/methanol/water, 60/15/15/10, v/v) or B (hexane/ethyl acetate, 20/1, v/v). Compounds were visualized by treatment with concentrated sulfuric acid/methanol, 10/90, v/v, and heating for a few minutes.
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- 1H NMR spectra were recorded on a Tesla BS 487 C spectrometer at 80 MHz. 13C NMR spectra were obtained on a Varian CFT 20 spectrometer at 20 MHz.
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- The exact structure of this product is still uncertain. It failed to undergo typical aldehyde reactions. The fragmentation pattern in the mass spectrum and the presence of a single spot on TLC raised the question as to whether a pyranose had been formed by migration of a trimethylsilyl group. Results concerning this problem will be published later.