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Nucleosides and Nucleotides Volume 17, 1998 - Issue 1-3
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Original Articles

New Approach to the Synthesis of 2′,3′-dideoxyadenosine and 2′,3′-Dideoxyinosine

K. V. Antonov Shemyakin—Ovchinnikov Institute of Bioorganic Chemistry, Russian Academy of Sciences, ul. Mikhlukho-Maklaya 16/10, Moscow, V-437, GSP-7, 117871, Russia
,
I. D. Konstantinova Shemyakin—Ovchinnikov Institute of Bioorganic Chemistry, Russian Academy of Sciences, ul. Mikhlukho-Maklaya 16/10, Moscow, V-437, GSP-7, 117871, Russia
&
A. I. Miroshnikov Shemyakin—Ovchinnikov Institute of Bioorganic Chemistry, Russian Academy of Sciences, ul. Mikhlukho-Maklaya 16/10, Moscow, V-437, GSP-7, 117871, Russia
Pages 153-159 | Published online: 22 Aug 2006

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  • The mixture also contains starting inosine and a quantity of di-O-formil derivatives
  • It has been observed, that an increased pressure doesn't influence the yield of ddN and in the case of the large scale preparation the high pressure is due to the technical reason
  • The discrepancy in the melting points may be due to the different solvents used for the crystallization

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