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Original Articles

Extraction of Caprolactam with Toluene in a Pulsed Disc and Doughnut Column—Part I: Recommendation of a Model for Hydraulic Characteristics

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Pages 499-517 | Received 26 Aug 2005, Accepted 03 Mar 2006, Published online: 15 Feb 2007

References

  • Simons , A. J.F. and Haasen , N. F. 1983 . “ Extraction of Caprolactam ” . In Handbook of Solvent Extraction Edited by: Lo , T. C. , Baird , M. H.I. and Hanson , C. 557 – 566 . New York : Wiley .
  • Movsowitz , R. L. , Kleinberger , R. , Buchalter , E. M. and Grinbaum , B. . Comparison of the Performance of Full Scale Pulsed Columns vs. Mixer‐Settlers for Uranium Solvent Extraction . Proceedings of the 30th Annual Hydrometallurgical Conference, 2000 . pp. 181 – 191 . Saskatoon, Saskatchewan
  • Kleinberger , R. . Zinc Sulfate Extraction by Bateman Pulsed Column Technology . Proceedings of the Copper, Cobalt, Nickel and Zinc Recovery conference . 2001 . pp. K1 – K13 . Johannesburg : South African Institute of Mining and Metallurgy .
  • Buchalter , E. M. , Kleinberger , R. and Grinbaum , B. . Copper Solvent Extraction Using a Bateman Pulsed Column . Proceedings of the Extraction Metallurgy Africa conference . 1998 . pp. 185 – 199 . Johannesburg : South African Institute of Mining and Metallurgy .
  • Jahya , A. B. , Stevens , G. W. and Pratt , H. R.C. . Mass Transfer Studies for a Pulsed Disc and Doughnut Extraction Column . Proceedings of the International Congress on Mineral Processing and Extractive Metallurgy . 2000 . pp. 281 – 284 . Melbourne : Australasian Institute of Mining and Metallurgy .
  • Angelov , G. , Gourdon , C. and Liné , A. 1998 . Simulation of Flow Hydrodynamics in a Pulsed Solvent Extraction Column under Turbulent Regimes . Chem. Eng. J. , 71 : 1 – 9 .
  • Mate , A. , Masbernat , O. and Gourdon , C. 2000 . Detachment of a Drop from an Internal Wall in a Pulsed Liquid‐Liquid Column . Chem. Eng. Sci. , 55 : 2073 – 2088 .
  • Mate , A. , Morchain , J. , Masbernat , O. and Gourdon , C. 1996 . A Transient Method for the Study of Wetting in a Liquid‐Liquid Contactor . Chem. Eng. Sci. , 51 : 5313 – 5323 .
  • Aoun Nabli , M. S. , Guiraud , P. and Gourdon , C. 1998 . CFD Contribution to a Design Procedure for Discs and Doughnuts Extraction Columns . Trans. IChemE. , 76 : 951 – 960 .
  • Milot , J. F. , Duhamet , J. , Gourdon , C. and Casamatta , G. 1990 . Simulation of a Pneumatically Pulsed Liquid‐Liquid Extraction Column . Chem. Eng. J. , 45 : 111 – 122 .
  • Angelov , G. and Gourdon , C. 2002 . Turbulent Viscosity in Pulsed Stagewise Extraction Columns . Bulgarian Chem. Comm. , 34 : 124 – 134 .
  • Angelov , G. and Gourdon , C. 2002 . Study on the Turbulence in Pulsed Stagewise Extraction Columns: Turbulence Macroscale . Hungarian J. Ind. Chem. , 30 : 137 – 142 .
  • Bardin‐Monnier , N. , Guiraud , P. and Gourdon , C. 2003 . Langrangian Simulations Contribution to the Knowledge of Discs and Doughnuts Pulsed Solvent Extraction Columns Hydrodynamics . Chem. Eng. Proc. , 42 : 503 – 516 .
  • Bardin‐Monnier , N. , Guiraud , P. and Gourdon , C. 2003 . Residence Time Distribution of Droplets within Discs and Doughnuts Pulsed Extraction Columns via Langrangian Experiments and Simulations . Chem. Eng. J. , 94 : 241 – 254 .
  • Aoun Nabli , M. S. , Guiraud , P. and Gourdon , C. 1997 . Numerical Experimentation: a Tool to Calculate the Axial Dispersion Coefficient in Discs and Doughnuts Pulsed Extraction Columns . Chem. Eng. Sci. , 52 : 2353 – 2368 .
  • Angelov , G. and Gourdon , C. 1999 . Influence of Stage Configuration on Flow Parameters in a Stagewise Extraction Column . Hungarian J. Ind. Chem. , 27 : 281 – 286 .
  • Jahya , A. B. , Stevens , G. W. and Pratt , H. R.C. . Flood Point and Dispersed Phase Hold‐up in a Pulsed Disc and Doughnut Liquid‐Liquid Extraction Column, In . Proceedings of the Chemeca'99 Conference ,
  • Al Khani , S. D. , Gourdon , C. and Gasamatta , G. 1988 . Simulation of Hydrodynamics and Mass Transfer of a Disks and Rings Pulsed Column . Ind. Eng. Chem. Res. , 27 : 329 – 333 .
  • Godfrey , J. C. and Slater , M. J. 1994 . Liquid‐Liquid Extraction Equipment New York : John Wiley & Sons, Inc. .
  • Pratt , H. R.C. and Stevens , G. W. 1992 . “ Selection, Design and Pilot Testing of Equipment ” . In Science and Practice of Liquid‐Liquid Extraction Edited by: Thornton , J. D. Oxford : Clarendon Press .
  • Logsdail , D. H. and Slater , M. J. 1983 . “ Pulsed Perforated‐Plate Columns ” . In Handbook of Solvent Extraction Edited by: Lo , T. C. , Baird , M. H.I. and Hanson , C. 355 – 372 . New York : Wiley .
  • Klicka , V. and Cermak , J. 1971 . Zweiphasenströmung in der Pulsier‐Extraktionskolonne . Verfahrenstechnik , 5 : 320 – 327 .
  • Berger , R. and Walter , K. 1985 . Flooding in Pulsed Sieve Plate Extractors . Chem. Eng. Sci. , 40 : 2175 – 2184 .
  • van Delden , M. L. , Kuipers , N. J.M. and de Haan , A. B. 2004 . Liquid‐liquid Equilibria and Physical Properties of the Quaternary System Water+Caprolactam+Ammonium Sulfate+Benzene and Toluene . J. Chem. Eng. Data , 49 : 1760 – 1770 .
  • Boyadzhiev , L. and Spassov , M. 1982 . On the Size of Drops in Pulsed and Vibrating Plate Extraction Columns . Chem. Eng. Sci. , 37 : 337 – 340 .
  • Baird , M. H.I. and Lane , S. J. 1973 . Drop Size and Hold‐up in a Reciprocating Plate Extraction Column . Chem. Eng. Sci. , 28 : 947 – 957 .
  • Baird , M. H.I. and Shen , Z. J. 1984 . Holdup and Flooding in Reciprocating Plate Extraction Columns . Can. J. Chem. Eng. , 62 : 218 – 227 .
  • Kumar , A. and Hartland , S. 1996 . Unified Correlations for the Prediction of Drop Size in Liquid‐Liquid Extraction Columns . Ind. Eng. Chem. Res. , 35 : 2682 – 2695 .
  • Kumar , A. and Hartland , S. 1986 . Prediction of Drop Size in Pulsed Perforated‐Plate Extraction Columns . Chem. Eng. Comm. , 44 : 163 – 182 .
  • Kumar , A. and Hartland , S. 1988 . Prediction of Dispersed Phase Hold‐up in Pulsed Perforated‐Plate Extraction Columns . Chem. Eng. Process. , 23 : 41 – 59 .
  • Kumar , A. and Hartland , S. 1988 . Prediction of Dispersed Phase Hold‐up and Flooding Velocities in Karr Reciprocating‐Plate Extraction Columns . Ind. Eng. Chem. Res. , 27 : 131 – 138 .
  • Kumar , A. and Hartland , S. 1995 . A Unified Correlation for the Prediction of Dispersed‐Phase Hold‐up in Liquid‐Liquid Extraction Equipment . Ind. Eng. Chem. Res. , 34 : 3925 – 3940 .
  • Hinze , J. O. 1955 . Fundamentals of the Hydrodynamic Mechanism of Splitting in Dispersion Processes . AIChE J. , 1 : 289 – 295 .
  • Arai , K. , Konno , M. , Matunaga , Y. and Saito , S. 1977 . Effect of Dispersed‐Phase Viscosity on the maximum Stable Drop Size for Breakup in Turbulent Flow . J. Chem. Eng. Japan , 10 : 325 – 330 .
  • Godfrey , J. C. and Slater , M. J. 1991 . Slip Velocity Relationships for Liquid‐Liquid Extraction Columns . Trans. IChemE. , 69 : 130 – 141 .
  • Kumar , A. and Hartland , S. 1989 . Independent Prediction of Slip Velocity and Hold‐up in Liquid‐Liquid Extraction Columns . Can. J. Chem. Eng. , 67 : 17 – 25 .
  • Gayler , R. and Pratt , H. R.C. 1951 . Hold‐up and Pressure Drop in Packed Columns . Trans. IChemE. , 29 : 110 – 125 .
  • Gayler , R. , Roberts , N. W. and Pratt , H. R.C. 1953 . Liquid‐Liquid Extraction Studies: Part IV . A Further Study of Hold‐up in Packed Columns. Trans. IChemE. , 31 : 57 – 68 .
  • Thornton , J. D. 1956 . Spray Liquid Extraction Columns: Prediction of Limiting Hold‐up and Flooding Rates . Chem. Eng. Sci. , 5 : 201 – 208 .
  • Sakiadis , B. C. 1984 . “ Fluid and Particle Mechanics ” . In Perry's Chemical Engineer's Handbook Edited by: Perry , R. H. and Green , D. Singapore : McGraw‐Hill Book Co. .
  • Edwards , R. B. and Beyer , G. H. 1956 . Flooding Characteristics of a Pulse Extraction Column . AIChE J. , 2 : 148 – 152 .
  • Selker , A. H. and Sleicher , C. A. 1965 . Factors Affecting which Phase will Disperse when Immiscible Liquids are Stirred Together . Can. J. Chem. Eng. , 43 : 298 – 301 .
  • Quinn , J. A. and Sigloh , D. B. 1963 . Phase Inversion in the Mixing of Immiscible Liquids . Can. J. Chem. Eng. , 41 : 15 – 18 .
  • Deshpande , K. B. and Kumar , S. 2003 . A New Characteristic of Liquid‐Liquid Systems– Inversion Holdup of Intensely Agitated Dispersions . Chem. Eng. Sci. , 58 : 3829 – 3835 .
  • Yeo , L. Y. , Matar , O. K. , Perez de Ortiz , E. S. and Hewitt , G. F. 2002 . A Simple Predictive Tool for Modelling Phase Inversion in Liquid‐Liquid Dispersions . Chem. Eng. Sci. , 57 : 1069 – 1072 .
  • Kumar , S. 1996 . On Phase Inversion Characteristics of Stirred Dispersions . Chem. Eng. Sci. , 51 : 831 – 834 .

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