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Original Articles

Development of Techniques of Generation of Gaseous Standard Mixtures

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Pages 31-55 | Received 04 Jan 2005, Accepted 25 Feb 2005, Published online: 12 Jan 2007

REFERENCES

  • Hedrich , M. and Heine , H. J. 1999 . Gaseous reference materials—A chalenge in preparation and stability . Spec. Publ.—R. Soc. Chem. , 238 : 115 – 126 .
  • Namieśnik , J. and Zygmunt , B. 1999 . Role of reference materials in analysis of environmental pollutants . Sci. Total. Environ. , 228 : 243 – 257 . [CROSSREF] [CSA]
  • Namieśnik , J. and Zygmunt , B. 2000 . Reference materials in environmental trace organic analysis . Accred. Qual. Assur. , 5 : 191 – 197 . [CROSSREF]
  • Jerzak , B. 2003 . Racjonalne stosowanie materiałów odniesienia . Analityka , 4 : 40 – 42 .
  • Namieśnik , J. and Górecki , T. 2001 . Quality of analytical results . Rev. Roum. Chim. , 46 : 953 – 962 .
  • Cuadros-Rodriguez , L. , Gámiz-Gracia , L. , Almansa-López , E. and Laso-Sánchez , J. 2001 . Calibration in chemical measurement processes. II. A methodological approach . Trends Anal. Chem. , 20 : 620 – 636 . [CROSSREF]
  • Quevauviller , Ph. and Donard , O. F. X. 2001 . Stated references for ensuring traceability of chemical measurements for long-term environmental monitoring . Trends Anal. Chem. , 20 : 600 – 613 . [CROSSREF]
  • 1992 . Trends and definitions used in connections with reference materials , Geneva : ISO . ISO guide 30
  • Konieczka , P. , Namieśnik , J. , Zygmunt , B. , Bulska , E. , Świtaj-Zawadka , A. , Naganowska , A. , Kremer , E. and Rompa , M. 2004 . Ocena i kontrola jakości wyników analitycznych (in Polish) , Gdańsk : CEEAM .
  • Brown , R. H. , Curtis , M. , Saunders , K. J. and Vandendriessche , S. 1992 . Clean Air at Work New Trends in Assessment and Measurement for the 1990s , Cambridge, , UK : Royal Society of Chemistry . (red.)
  • Namieśnik , J. , Górecki , T. , Kozdroń , B. and Torres , L. 1989 . Determination of Selekted Organicpollutants in Indoor Air Using Permeation Passive Samplers . Intern. J. Environ. Anal. Chem. , 37 : 139 – 147 .
  • Namieśnik , J. 1985 . Zagszczanie lotnych organicznych zanieczyszczeńatmosfery , Gdańsk : Zeszyty Naukowe Politechniki Gdańskiej . Chemia 28
  • Namieśnik , J. 1984 . Generation of standard gaseous mixtures . J. Chromatogr. , 300 : 79 – 108 . [CROSSREF]
  • 1994 . Kontrola chemiczna zanieczyszczeń środowiska (in Polish) , Gdańsk : skrypt Politechniki Gdańskiej . Namieśnik J. (red.)
  • King , B. 2003 . The selection and use of reference materials—a basic guide for laboratories and accreditation bodies . Accred. Qual. Assur. , 8 : 429 – 433 . [CROSSREF]
  • Morris , C. , Berkley , R. and Bumgarner , J. 1983 . Preparation of multicomponent volatile organic standards using static dilution bottles . Anal. Letters , 16 : 1585 – 1593 .
  • Rhoderick , G. C. and Zieliński , W. L. jr. 1988 . Preparation of accurate multicomponent gas standards of volatile toxic organic compounds in the low-parts-per-billion range . Anal. Chem. , 60b : 2454 – 2460 . [CROSSREF]
  • 1992 . Metody instrumentalne w kontroli chemicznych zanieczyszczeń środowiska (in Polish) , Gdańsk : skrypt Politechniki Gdańskiej . Namieśnik J. (red.)
  • Namieśnik , J. , Jamrógiewicz , Z. , Pilarczyk , M. and Torres , L. 1997 . Przygotowanie próbek urodowiskowych do analizy (in Polish) . Chem. Inż. Ekol. , 3
  • Gorlo , D. 1998 . Nowe zastosowania analityczne techniki mikroekstrakcji do fazy stacjonarnej (in Polish) Ph.D. dissertation, Wydział Chemiczny, Politechnika Gdańska
  • Bonate , P. L. 1992 . Concepts in Calibration Theory, Part III: Weighted Least-Squares Regression . 10 : 310 LC-GC
  • Kalivas , J. H. and Suter , J. M. 1991 . Generalized Simulated Annealing for Calibration Sample Selection From an Existing Set and Orthogonalization of Undesigned Experiments . J. Chemom. , 5 : 37 – 48 .
  • Cowper , C. J. and DcRose , A. J. 1988 . Chromatograficzna analiza Gazów , WNT .
  • Konieczka , P. 1997 . Kalibracja jako etap procedury analitycznej . Chem. Inż. Ekol. , 4 : 37 – 47 .
  • Danzer , K. , Matthias , O. and Currie , L. A. 2004 . Guidelines for calibration in analytical chemistry. Part 2: Multicomponent calibration (IUPAC Technical Report) . Pure Appl. Chem. , 76 : 1215 – 1225 .
  • Caroli , S. , Forte , G. and Iamiceli , A. L. 1999 . ICP-AES and ICP-MS quantification of trace elements in the marine macroalga fucus sample, a new candidate certified reference material . Microchem. J. , 62 ( 2 ) : 244 – 250 . [CROSSREF]
  • Ross , A. , Sutherland and Filip , M. G. 2002 . Tack, Determination of Al, Cu, Fe, Mn, Pb and Zn in certified reference materials using the optimized BCR sequential extraction procedure . Anal. Chim. Acta , 454 ( 2 ) : 249 – 257 . [CROSSREF] [CSA]
  • Caroli , S. , Senofonte , O. , Caimi , S. , Robouch , P. , Pauwels , J. and Kramer , G. N. 1988 . Certified reference materials for research in antarctica: The case of marine sediment . Microchem. J. , 59 ( 1 ) : 136 – 143 . [CROSSREF]
  • Dybczyński , R. , Danko , B. and Polkowska-Motrenko , H. 2001 . Some difficult problems still existing in the preparation and certification of CRMs . Fresenius J. Anal. Chem. , 370 : 126 – 130 . [CROSSREF]
  • Dybczyński , R. , Danko , B. and Polkowska-Motrenko , H. 2000 . NAA study on homogeneity of reference materials and their suitability for microanalytical techniques . J. Radioanal. Nucl. Chem. , 245 : 97 – 104 . [CROSSREF]
  • Dybczyński , R. , Polkowska-Motrenko , H. , Samczyński , Z. and Szopa , Z. 1998 . Virginia tobacco leaves (CTA-VTL-2)—New Polish CRM for inorganic trace analysis including microanalysis . Fresenius J. Anal. Chem. , 360 : 384 – 387 . [CROSSREF]
  • http://www.nist.gov/
  • Barratt , R. S. 1981 . The preparation of standard gas mixtures. A review . Analyst , 106 : 817 – 849 . [CROSSREF] [CSA]
  • Namieśnik , J. and Przyk , E. 1999 . Kierunki rozwojowe w zakresie sporz dzania gazowych mieszanin wzorcowych . Chem Inż. Ekol. , 6 : 289 – 300 . [CSA]
  • Szulc , J. and Witkiewicz , Z. 1981 . Wytwarzanie niskich st żeń par w gazach do wzorcowania detektorów . Chem. Anal. , 26 : 375 – 387 .
  • Muniak , W. , Witkiewicz , Z. , Woryna , E. , Kusińska , E. , Twardowski , A. and Goca , B. 1988 . Preparation of standard gaseous mixtures by a manometric method using the Benedict—Webb—Rubin equation . J. Chromatogr. , 436 : 323 – 327 . [CROSSREF]
  • Pracazbiorowa pod redakcja Namieśnika , J. and i Jamrógiewicza , Z. 1998 . Fizykochemiczne metody kontroli zanieczyszczeń środowiska (in Polish) , Warszawa : WNT .
  • Denyszyn , R. B. and Sassaman , T. 1987 . Parts-Per-Billion gaseous mixtures: A new challenge . ASTM, STP , 957 : 101 – 109 .
  • Miller , J. A. , Grubaugh , K. W. and Jordon , L. M. 1980 . Analysis of stack gases using a portable gas chromatographic sampling and analyzing system . Environ. Sci. Technol. , 14 ( 1 ) : 97 – 100 . [CROSSREF]
  • Rhoderick , G. C. 1995 . Development of gas standards from solid 1,4-dichlorobenzene . J. Chromatogr. A , 710 ( 1 ) : 229 – 235 . [CROSSREF]
  • Rhoderick , G. C. and Fresenius , J. 1997 . Development of a fifteen component hydrocarbon gas standard reference material at 5 nmol/mol in nitrogen . Anal. Chem. , 359 : 477 – 483 .
  • Gerboles , M. , Diaz , E. and Noriega-Guerra , A. 1998 . Uncertainty calculation and implementation of the static volumetric method for the preparation of NO and SO2 standard gas mixtures . Accred. Qual. Assur. , 2 : 69 – 78 . [CROSSREF]
  • Lucero , D. P. 1976 . Ultra low-level calibration gas generation by multistage dilution techniques . Calibration in Air Monitoring, ASTM Spec. Tech. Publ. , 598 : 301 – 319 .
  • Guenier , J. P. and Muller , J. 1981 . Sampling of gaseous pollutants. Badges: Use and comparison with activated charcoal tubes . Cah. Notes Doc. , 105 : 493 – 507 .
  • Morris , C. , Berkley , R. and Bumgarner , J. 1983 . Preparation of multicomponent volatile organic standards using static dilution bottles . Anal. Letters , 16 : 1585 – 1593 . to samo co 16
  • Wright , R. S. and Murdoch , R. W. 1994 . Laboratory evaluation of gas dilution systems for analyzer calibration and calibration gas analysis . Air & Waste , 44 : 428 – 430 .
  • Namieśnik , J. and Konieczka , P. 1991 . Sporzadzanie gazowych mieszanin wzorcowych technika autorozcienczania . Chem. Anal. , 36 : 356 – 361 .
  • Namieśnik , J. and Konieczka , P. 1989 . Sporz dzanie gazowych mieszanin wzorcowych technik autorozcieńczania (in Polish) . materiały IV Ogólnopolskiej Konferencji chromatograficznej . 09 04–08 1989 , Lublin. str. P-44.
  • Konieczka , P. 1989 . Sporzdzanie gazowych mieszanin wzorcowych technik autorozcieńczania (in Polish) , Gdańsk : Praca dyplomowa .
  • Frary , B. D. 1998 . Multipoint calibration from one standard solution and automatic dilution of overrange samples for flame atomic absorption spectrometry . Analyst , 123 ( 2 ) : 233 – 237 . [CROSSREF]
  • Braun , W. , Peterson , N. C. , Bass , A. M. and Kurylo , M. 1971 . A vacuum ultraviolet atomic emission detector: Quantitative and qualitative chromatographic analysis of typical C, N, and S containing compounds . J. Chromatogr. , 55 ( 2 ) : 237 – 248 . [CROSSREF]
  • Ichinose , M. , Yasuoka , T. , Takano , J. , Mitsuzawa , S. and Zimmerman , P. R. 1985 . reprinted from the Proceedings of the Faculty Science . 1985 . pp. XX Tokai University .
  • Gupta , J. P. and Swarup , G. 1991 . A laboratory method for preparation of low concentration gas mixtures . Indian J. Technol. , 29 : 214 – 216 .
  • Debbrecht , F. J. , Daugherty , D. T. and Neel , T. M. 1979 . Diffusion tubes as a primary standard for OSHA-type calibration . Nat. Bur. Stand., (U.S.) Spec. Publ. , 519 : 761 – 769 .
  • Namieśnik , J. , Torres , L. , Kozłowski , E. and Mathieu , J. 1981 . Evaluation of the suitability of selected porous polymers for preconcentrations of volatile organic compounds . J. Chromatogr. , 208 ( 2 ) : 239 – 252 . [CROSSREF]
  • Namieśnik , J. , Bownik , M. and Kozłowski , E. 1982 . Urzadzenia z przegrodami polprzepuszczalnymi do sporzadzania gazowych mie-szanin wzorcowych . Pomiary Autom. Kontrola , 28 : 67 – 69 .
  • Maria , P.-Ch. , Gal , J.-F. , Balza , M. , Peré-Trepat , E. and Tumbiolo , S. 2002 . Using thermogravimetry for weight loss monitoring of permeation tubes used for generation of trace concentration gas standards . Anal. Chem. , 74 : 305 – 307 . [PUBMED] [INFOTRIEVE] [CROSSREF]
  • Wedel , A. , Müller , K. P. , Ratte , M. and Rudolph , J. 1998 . Measurements of Volatile Organic Compounds (VOC) during POPCPRN 1994: Applying a new on-line GC-MS-technique . J. Atmos. Chem. , 31 : 73 – 103 . [CROSSREF] [CSA]
  • Pérez Ballesta , P. , Baldan , A. and Cancelinha , J. 1999 . Atmosphere generation system for the preparation of ambient air volatile organic compound standard mixtures . Anal. Chem. , 71 : 2241 – 2245 . [CROSSREF]
  • Barkó , G. and Hlavay , J. 1998 . Development of a calibration instrument for the dynamic generation of organic vapors . Fresenius J. Anal. Chem. , 360 : 119 – 121 . [CROSSREF]
  • Janicki , W. , Wolska , L. , Górecki , T. and Namieśnik , J. 1993 . Apparatus for calibration of gas chromatographic systems for thermal desrption . Chem. Anal. , 38 : 423 – 428 .
  • Spicer , C. V. , Kenny , D. W. , Slivon , L. E. and Ward , G. F. 1988 . Development and evaluation of a rapid multicomponent calibration procedure for air toxic analysis using the trace atmospheric gas analyzer (TAGA) . Proc. APCA Annu. Meet. February 24–26 1988 , San Francisco. paper 88-150.7.
  • Spinhirne , J. P. and Koziel , J. A. 2003 . Generation and calibration of standard gas mixtures for volatile fatty acids using permeation tubes and solid-phase microextraction . Transactions of ASAE , 46 : 1639 – 1646 .
  • Kozdroń-Zabiegała , B. , Namieśnik , J. and Przyjazny , A. 1995 . Use of passive dosimeters for evaluation of the quality of indoor and out-door air . Indoor Built. Environ. , 4 : 189 – 203 .
  • Knopf , D. 2001 . Continuous dynamic-gravimetric preparation of calibration gas mixtures for air pollution measurements . Accred. Qual. Assur. , 6 : 113 – 119 . [CROSSREF]
  • Van Merbel , N. C. , Hagemon , J. J. and Th , K. A. 1993 . Brinkman, Membrane-based sample preparation for chromatography . J. Chromatogr. , 634 ( 1 ) : 1 – 29 .
  • Goelen , E. , Lambrechts , M. , Geyskens , F. and Rymen , T. 1992 . Development and performance characteristics of a capillary dosage unit with in situ weight sensor for the preparation of known amounts of gaseous VOC's in air . Intern. J. Environ. Anal. Chem. , 47 : 217 – 225 . [CSA]
  • McKinlej , J. J. and Merriman , D. C. 1996 . Permeation tube sources for internal standards in process samples . Proc. Control Qual. , 8 ( 2–3 ) : 69 – 74 .
  • Quaβ , U. and Schilling , M. 1994 . A new test gas generator for atmospheric trace compounds . Fresenius J. Anal. Chem. , 350 : 461 – 466 . [CROSSREF]
  • Balasubramanian , N. and Krishnameorthy , S. 1995 . Development of simple permeation device for the generation of hydrogen sulfide . Analyst , 120 : 2287 – 2289 . [CROSSREF]
  • Altshuller , A. P. and Cohen , J. R. 1960 . Application of diffusion cells to production of known concentration of gaseous hydrocarbons . Anal. Chem. , 32 : 802 – 810 . [CROSSREF]
  • Gautrois , M. and Koppmann , R. 1999 . Diffusion technique for the production of gas standards for atmospheric measurements . J. Chromatogr. A , 848 : 239 – 249 . [CROSSREF]
  • Pitombo , L. R. M. and Cardoso , A. A. 1990 . Standard gas mixture production based on the diffusion method . Intern. J. Environ. Anal. Chem. , 39 : 349 – 360 .
  • Gautrois , M. and Koppmann , R. 1999 . Diffusion technique for the production of gas standards for atmospheric measurements . J. Chromatogr. A , 848 : 239 – 249 . [CROSSREF]
  • Eiceman , G. A. , Preston , D. , Tiano , G. , Rodriguez , J. and Parmeter , J. E. 1997 . Quantitative calibration of vapor levels of TNT, RDX, and PETN using a diffusion generator with gravimetry and ion mobility spectrometry . Talanta , 45 : 57 – 74 . [CROSSREF]
  • Tanaka , H. 1997 . On-line Generation methods of highly reactive reagents and their application to flow analyses . J. Flow. Injection Anal. , 14 ( 1 ) : 1 – 14 .
  • Ishikawa , K. , Hobo , T. , Suzuki , S. and Watabe , K. 1984 . Generation of trace amounts of alkanethiol standard gases using reaction gas chromatography . J. Chromatogr. , 295 : 445 – 452 . [CROSSREF]
  • Oms-Molla , M. T. and Klockow , D. 1996 . Generation of test atmospheres of 2,4-dinitrophenol and evaluation of sampling methods for its determination in air . Intern. J. Environ. Anal. Chem. , 62 : 281 – 288 . [CSA]
  • Tocksteinova , Z. and Opekar , F. 1986 . The electrochemical generation of small amounts of hydrogen cyanide . Talanta , 33 ( 8 ) : 688 – 690 . [CROSSREF]
  • Ishikawa , K. , Watabe , K. , Hobo , T. and Suzuki , S. 1983 . Generation of trace amonut of acrolein standard gas using reaction gas chromatography . Bunseki Kagaku , 32 : 321 – 325 .
  • Przyjazny , A. 1984 . Stable standard solutions for gas chromatographic determination of volatile thiols . J. Chromatogr. , 292 ( 1 ) : 189 – 196 . [CROSSREF]
  • Grosjean , O. , Fung , K. , Collins , J. , Harrison , J. and Breitung , E. 1984 . Portable generator for on-site calibration of peroxyacetyl nitrate analyzers . Anal. Chem. , 56 : 569 – 573 . [CROSSREF]
  • Nunnermacker , L. J. , Dickerson , R. R. , Fried , A. and Sams , R. 1989 . A new gas-phase nitric acid calibration system . Environ. Sci. Technol. , 23 ( 1 ) : 106 – 110 . [CROSSREF] [CSA]
  • Hashimoto , Y. and Tanaka , S. 1980 . A new method of generation of gases at parts per million levels for preparation of standard gases . Environ. Sci. Technol. , 14 ( 4 ) : 413 – 416 . [CROSSREF]
  • Vejrosta , J. and Novak , J. 1979 . Method for the preparation of continuous streams of gaseous calibration mixtures with defined contents of standard substances . J. Chromatogr. , 175 : 261 – 267 . [CROSSREF]
  • Meddle , D. W. and Smith , A. F. 1981 . Field method for the determination of aromatic primary amines in air. Part I. Generation of standard atmospheres of amines . Analyst , 106 ( 1267 ) : 1082 – 1087 . [CROSSREF] [CSA]
  • Greenhouse , S. and Andrawes , F. 1990 . Generation of gaseous standard using exponential dilution flasks in series . Anal. Chim. Acta , 236 : 221 – 226 . [CROSSREF]
  • De Souza , T. L. C. and Laweless , S. P. 1976 . Development of calibration systems for measuring total reduced sulfur and sulfur dioxide in ambient concentrations in the parts per billion range . Anal. Chem. , 48 : 2234 – 2239 . [PUBMED] [INFOTRIEVE] [CROSSREF]
  • Bruner , F. , Canulli , C. and Possanzini , M. 1973 . Coupling of permeation and exponential dilution methods for use gas chromatographic trace analysis . Anal. Chem. , 45 : 1970 – 1971 .
  • Fowlis , I. A. and Scott , R. P. W. 1963 . A vapor dilution system for detector calibration . J. Chromatogr. , 11 : 1 – 10 . [PUBMED] [INFOTRIEVE] [CROSSREF]
  • Wang , J.-L. , Lin , W.-Ch. and Chen , T.-Y. 2000 . Using atmospheric CCl4 as an internal reference in gas standard preparation . Atmos. Environ. , 34 : 4393 – 4398 . [CROSSREF]
  • Wolska , L. 1996 . Zastosowanie połczenia termiczna desorpcja—chromatografia gazowa w analityce próbek środowiskowych (in Polish) PhD dissertation, Wydział Chemiczny, Politechnika Gdańska
  • Prokopowicz , M. 1999 . Gazowe mieszaniny wzorcowe sporzdzane w oparciu o termiczny rozkład zwizków powierzchniowych (in Polish) PhD dissertation, Wydział Chemiczny, Politechnika Gdańska
  • Raymond Scott , P. W. 1993 . Silica gel and bonded phases, their production, properties and use in LC , Chichester, New York, Brisbane, Toronto, , Singapore : John Wiley & Sons .
  • Unger , K. K. 1979 . “ Porous silica—its properties and use as support in column liquid chromatography ” . In J. Chromatogr. , Amsterdam : Elsevier Scientific Publishing Como. . Library, 16, chapter 2
  • Ligor , M. , Ścibiorek , M. and Buszewski , B. 1997 . New coating surfaces of fibres for solid phase microextraction (SPME) . J. Microcol. Sep. , 11 ( 5 ) : 377 – 383 . [CROSSREF]
  • Out , E. O. and Pawliszyn , J. 1993 . Solid phase micro-extraction of metal ions . Mikrochim. Acta , 112 : 41 – 46 . [CROSSREF]
  • Ligor , M. and Buszewski , B. 1999 . Determination of menthol and menthone in food and pharmaceutical products by solid-phase microextraction–gas chromatography . J. Chromatogr. A , 847 : 161 – 169 . [CROSSREF]
  • Zeng , Z. , Qiu , W. and Huang , Z. 2001 . Solid-phase microextraction using fused-silica fibers coated with sol-gel-derived hydroxy-crown ether . Anal. Chem. , 73 : 2429 – 2436 . [PUBMED] [INFOTRIEVE] [CROSSREF]
  • Gbatu , T. P. , Sutton , K. L. and Caruso , J. A. 1999 . Development of new SPME fibers by sol–gel technology for SPME-HPLC determination of organometals . Anal. Chim. Acta , 402 : 67 – 79 . [CROSSREF]
  • Zygmunt , B. , Jastrzebska , A. and Namieśnik , J. 2001 . Solid phase microextraction—a convenient tool for the determination of organic pollutants in environmental matrices . Crit. Rev. Anal. Chem. , 31 : 1 – 18 . [CSA]
  • Namieśnik , J. , Zygmunt , B. and Jastrzebska , A. 2001 . Application of solid-phase microextraction for determination of organic vapours in gaseous matrices . J. Chromatogr. A , 885 : 405 – 418 .
  • Lord , H. and Pawliszyn , J. 2000 . Evolution of solid-phase microextraction technology . J. Chromatogr. A , 885 : 153 – 193 . [PUBMED] [INFOTRIEVE] [CROSSREF]
  • Eisert , R. and Pawliszyn , J. 1998 . Automated in-tube solid phase microextraction coupled to high-performance liquid chromatography . Anal. Chem. , 69 : 3140 – 3147 . [CROSSREF]
  • Eiser , R. and Levsen , K. 1996 . Development of a prototype system for quasi-continuous analysis of organic contaminants in surface or sewage water based on in-line coupling of solid-phase microextraction to gas chromatography . J. Chromatogr. , 737 : 59 – 65 . [CROSSREF]
  • Motlagh , S. and Pawliszyn , J. 1993 . On-line of flowing samples using solid phase microextraction-gas chromatography . Anal. Chim. Acta , 284 : 265 – 273 . [CROSSREF]
  • Świtaj-Zawadka , A. 2004 . Badania możliwości wytwarzania bezmatrycowych materiałów odniesienia lotnych analitów (in Polish) PhD dissertation, Wydział Chemiczny, Politechnika Gdańska
  • Przyk , E. , Konieczka , P. , Szczygielska-Tao , J. , Teschner , R. , Biernat , J. F. and Namiesnik , J. 2001 . Use of porous glass and silica gel as support media of a surface compound for generation of analytes in gaseous standard mixtures. New method for the determination of the amount of analyte generated . J. Chromatogr. A , 928 : 99 – 108 . [PUBMED] [INFOTRIEVE] [CROSSREF]
  • Konieczka , P. 2000 . Influence of process parameters on the composition of gaseous standard mixtures of n-propanethiol obtained by thermal decomposition of surface compounds . Fresenius J. Anal. Chem. , 367 : 132 – 140 . [PUBMED] [INFOTRIEVE] [CROSSREF]
  • Konieczka , P. 1994 . Nowa metoda sporzdzania gazowych mieszanin wzorcowych (in Polish) PhD dissertation, Wydział Chemiczny, Politechnika Gdańska
  • Świtaj , A. , Przyk , E. , Szczygelska-Tao , J. , Wójcik , J. , Biernat , J. F. and Namieśnik , J. 2003 . Applicability of glass fiber as a support material for generation of gaseous standard mixtures using thermal decomposition of the surface compound. Calibration of analytical equipment . J. Sep. Sci. , 26 : 1057 – 1062 . [CROSSREF]
  • Przyk , E. , Świtaj-Zawadka , A. , Konieczka , P. , Szczygelska-Tao , J. , Biernat , J. F. and Namieśnik , J. 2003 . Thermal decomposition of surface compounds for the generation of small quantities of acetaldehyde. Calibration of a thermal desorption gas chromatography-flame ionization detection . Anal. Chim. Acta , 488 : 89 – 96 . [CROSSREF]
  • Świtaj-Zawadka , A. , Konieczka , P. , Szczygelska-Tao , J. , Biernat , J. F. and Namieśnik , J. 2004 . New procedure of silica gel surface modification. Preparation of gaseous standard mixtures for calibration purposes . J. Chromatogr. A , 1033 : 145 – 151 . [CROSSREF]
  • Konieczka , P. , Makarewicz , J. , Luboch , E. , Namieśnik , J. and Biernat , J. F. 1994 . Preparation of standard gaseous mixtures of carbon dioxide in nitrogen by thermal decomposition of surface compounds. Determination of the influence of some parameters of thermal decomposition process on the composition of the generated mixtures . Chem. Anal. , 39 : 179 – 188 .
  • Konieczka , P. , Namieśnik , J. , Przyjazny , A. , Luboch , E. and Biernat , J. F. 1995 . Utilization of thermal decomposition immobilized compounds for the generation of gaseous standard mixtures used in the calibration of gas analyses . Analyst , 120 : 2041 – 2046 . [CROSSREF]
  • Prokopowicz , M. , Luboch , E. , Namieśnik , J. , Biernat , J. F. and Przyjazny , A. 1997 . Utilization of standards generated in the process of thermal decomposition chemically modified silica gel for a single point calibration of a GC/FID system . Talanta , 44 : 1551 – 1561 . [CROSSREF]
  • Prokopowicz , M. , Luboch , E. , Przyjazny , A. , Biernat , J. F. and Namieśnik , J. 1998 . Quartz rod coated with modified silica gel as a source of CO and CO2 for standard gaseous mixtures . JHRC , 21 : 303 – 308 .
  • Prokopowicz , M. , Lewandowska , K. , Skwierawska , A. , Przyjazny , A. , Biernat , J. F. and Namieśnik , J. 1997 . Synthesis and characterization of modified silica gel as an intermediate ingeneration of gaseous standard mixtures . Chromatographia , 44 : 483 – 490 .
  • Konieczka , P. , Prokopowicz , M. , Skwierawska , A. , Przyjazny , A. , Biernat , J. F. and Namieśnik , J. 1997 . Thermal decomposition of immobilized compounds for the generation of gaseous standard mixtures containing ammonia and amines . Mikrochim. Acta , 127 : 211 – 217 . [CROSSREF]
  • Konieczka , P. , Luboch , E. , Namieśnik , J. and Biernat , J. F. 1992 . Study of a method for the preparation of standard gas mixtures based on thermal decomposition of surface compounds. Application to isothiocynates . Anal. Chim. Acta , 265 : 127 – 132 . [CROSSREF]
  • Konieczka , P. , Namieśnik , J. and Biernat , J. F. 1991 . Generation of standard gaseous mixtures by thermal decomposition of surface compounds. Standard mixtures of thiols . J. Chromatogr. , 540 : 449 – 455 . [CROSSREF]
  • Konieczka , P. , Wolska , L. , Luboch , E. , Namieśnik , J. , Przyjazny , A. and Biernat , J. F. 1996 . Calibration of the thermal desorption-gas chromatography-mass spectrometry system using standards generated in the process of thermal decomposition of chemically modified silica gel . J. Chromatogr. , 742 : 175 – 179 . [CROSSREF]
  • Konieczka , P. , Świtaj-Zawadka , A. and Namieśnik , J. 2004 . Gaseous standard mixtures—the challenge of obtaining small amounts of measurand . Trends Anal. Chem. , 23 : 450 – 458 .
  • Prokopowicz , M. , Przyjazny , A. , Biernat , J. F. and Namieśnik , J. 1998 . Characterization of modified silica gel as a source of ethene for standard gaseous mixtures . Microchem J. , 59 : 437 – 447 .
  • Konieczka , P. , Prokopowicz , M. , Zygmunt , B. , Biernat , J. F. and Namieśnik , J. 2000 . Thermal decomposition of silica based surface compounds as a source of volatile standards. A new approach to the generation of gaseous calibration mixtures . Chromatographia Supl. , 51 : 249 – 260 .
  • Namieśnik , J. , Konieczka , P. , Chrzanowski , W. and Biernat , J. F. 1994 . Trends in development of techniques of preparation of gaseous standard mixtures . Chem. Anal. , 39 : 245 – 262 .

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