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Original Articles

The First Perselenoborate with a Novel Three-Dimensional Anion Network

Pages 169-172 | Received 24 Aug 2000, Published online: 30 Apr 2008

References

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  • a) Hammerschmidt A. Küper J. Stork L. Krebs B. , Z. Anorg. Allg. Chem. 620 1898 ( 1994 ); b) A. Lindemann, J. Kuchinke, C. Köster, B. Krebs, Z. Anorg. Allg. Chem. (in preparation) .
  • Lindemann A. Kuchinke J. Köster C. Krebs B. , Z. Anorg. Allg. Chem. (in preparation).
  • a) Küper J. Conrad O. Krebs B. , Angew. Chem. 109 1995 ( 1997 ); Angew. Chem. Int. Ed. Engl. 36 1903 (1997); b) A. Lindemann J. Kuchinke, B. Krebs, Z. Anorg. Allg. Chem. 625 1165 (1999) .
  • Li2B2Se5: monoclinic; space group: C2/c; a = 10.616(2) Å, b = 5.318(1) Å, c = 12.382 Å, β = 109.97(3)°; V = 657.0(2) Å3; μ = 27.4 mm−1; Z = 4; R1 = 0.0207 for 710 reflections with I ≥ 2σ(I); wR2 = 0.0572 for all 775 unique reflections; MoKα-radiation; graphite monochromator; structure solution with SHELXS-97; refinement with SHELXL-97 (G. M. Sheldrick, University of Göttingen). Further details of the crystal structure investigations may be obtained from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen, Germany, (Fax: (+49)7247–808–666, e-mail: [email protected]) on quoting the depository number CSD-411410.

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