REFERENCES
- Freedman , D. A. , Keresztes , I. and Asbury , A. L. 2002 . J. Organomet. Chem. , 642 : 97
- Meacham , A. P. , Druce , K. L. , Bell , Z. R. , Ward , M. D. , Keister , J. B. and Lever , A. B. P. 2003 . Inorg. Chem. , 42 : 7887
- Schultze , X. , Serin , J. , Adronov , A. and Fréchet , J. M. J. 2001 . Chem. Commun. , : 1160
- Koefod , R. S. and Mann , K. R. 1991 . Inorg. Chem. , 30 : 2221
- Lin , Q. and Leong , W. K. 2003 . Organometallics , 22 : 3639
- DeRosa , M. C. , Hodgson , D. J. , Enright , G. D. , Dawson , B. , Evans , C. E. B. and Crutchley , R. J. 2004 . J. Am. Chem. Soc. , 126 : 7619
- Budzisz , E. , Keppler , B. K. , Giester , G. , Wozniczka , M. , Kufelnicki , A. and Nawrot , B. 2004 . Eur. J. Inorg. Chem. , : 4412
- Anderson , C. , Freedman , D. A. , Jennings , M. and Gray , B. 2005 . J. Organomet. Chem. , 690 : 168
- Lee , S. H. , Kim , H. J. , Lee , Y. O. , Vicens , J. and Kim , J. S. 2006 . Tetrahedron Lett. , 47 : 4373
- Alonso , M. T. , Brunet , E. , Hernandez , C. and Rodríguez-Ubis , J. C. 1993 . Tetrahedron Lett. , 34 : 7465
- Zhang , H. and Rudkevich , D. M. 2007 . Chem. Commun. , : 1238
- Smith , M. B. , Dale , S. H. , Coles , S. J. , Gelbrich , T. , Hursthouse , M. B. , Light , M. E. and Horton , P. N. 2007 . Cryst. Eng. Comm. , 9 : 165
- Elsegood , M. R. J. , Smith , M. B. and Staniland , P. M. 2006 . Inorg. Chem. , 45 : 6761
- Downing , J. H. and Smith , M. B. 2004 . Comprehensive Coordination Chemistry II , Vol. 1 , 253 Oxford : Elsevier .
- Hoyos , O. L. , Bermejo , M. R. , Fondo , M. , García-Deibe , A. , González , A. M. , Maneiro , M. and Pedrido , R. 2000 . J. Chem. Soc. Dalton Trans. , : 3122
- Crystal data for 4: C40H36Cl3N2O3P2Pd, M = 867.40; orthorhombic, Pnma a = 28.571(3), b = 17.5634(18), c = 8.2536(8) Å, V = 4141.6(7) Å3; Z = 4, ρ cal 1.391 g cm–3; μ(Mo-Kα) = 0.757 mm−1; λ = 0.71073 Å, T = 150(2) K; 32496 reflections were collected on a Bruker SMART 1000 CCD diffractometer13 using narrow ω -scans, 4871 of which were independent (R int = 0.0611). The structure was solved by Patterson synthesis and refined on F 2 values to give a final R = 0.0628 for 4871 data with F 2 > 2σ (F 2); wR 2 = 0.1612 for all data.14 The chloride/methyl ligands exhibit 50:50 positional disorder across the crystallographic mirror plane. 4 was found to contain disordered molecules of CH2Cl2; these were modelled by the Platon Squeeze procedure.15 A complete set of X-ray crystallographic structural data for compound 4 (CCDC no. 642380) is available at the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, UK (fax: +44 1223 336 033; [email protected]) on request, quoting the deposition number
- 2001 . SMART and SAINT Software for CCD diffractometers , Madison, WI : Bruker AXS Inc. .
- Sheldrick , G. M. 2000 . SHELXTL User Manual , Madison, WI : Bruker ACS Inc. . Version 6.10
- Spek , A. L. 1990 . Acta Crystallogr., Sect. A , 46 : C34