REFERENCES
- Katti , K. V. , Raghuraman , K. , Pillarsetty , N. , Volkert , W. A. , Jurisson , S. S. and Hoffman , T. J. 2002 . Technetium, Rhenium and Other Metals in Chemistry and Nuclear Medicine 6 , Edited by: Nicolini , M. , Bandoli , G. and Mazzi , U. 69 – 72 . Padova, Italy : SGE Editorali .
- Katti , K. V. , Gali , H. , Smith , C. J. and Berning , D. E. 1999 . Acc. Chem. Res. , 32 : 9
- 31P NMR chemical shifts are quoted relative to an 85% solution of phosphoric acid in D2O, as an external reference. The % yields are 31P NMR integration %
- Vullo , W. J. 1968 . J. Org. Chem. , 33 : 3665
- Petrov , K. A. , Parshina , V. A. and Luzanova , M. B. 1962 . J. Gen. Chem. USSR , 32 : 542
- X-ray crystallography data was collected at 120 K using a Nonius Kappa CCD area detector diffractometer mounted at the window of a molybdenum rotating anode (50 KV, 90 mA, λ = 0.71069 Å). The crystal-to-detector distance was 30 mm and φ and Ω scans (1.0° increments, 20 s exposure time) were carried out to fill the Ewald sphere. Data collection and processing were carried out using COLLECT, DENZO and maXus and empirical absorption correction was applied using SORTAV. The structure was solved by the heavy-atom method using DIRDIF-99 and refined anisotropically (non-hydrogen atoms) by full-matrix least-squares on F 2 using the SHELXL-97 program. The H atoms were calculated geometrically and refined with the riding model. The programs ORTEP-3 and PLATON were used for drawing the molecule. WINGX was used to prepare material for publication
- 31P NMR spectra were recorded on a JEOL EX 270 with the sample in an evacuated WILMAD® NMR tube with a J. Young valve
- The data have been deposited with the Cambridge Crystallographic Data Center as CCDC 676677; available online at http://www.ccdc.cam.ac.uk/data_request/cif