REFERENCES AND NOTES
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- 1H and 13C NMR spectra were recorded at 400 and 100.62 MHz, respectively, on a Bruker Avance-DRX 400 instrument. Unless otherwise specified, CDCl3 was used as the solvent and TMS as internal standard. GC-MS analyses were carried out with an HP-6890 gas chromatograph (dimethyl silicone column, 12.5 m) equipped with an HP-5973 mass-selective detector. IR spectra were recorded on a JASCO FT/IR-410 spectrophotometer using a multiple reflection horizontal ATR (HATR) accessory. Optical rotations were measured with a JASCO DIP-1000 digital polarimeter
- Jonsson , S. , Adolfsson , H. and Backvall , J.-E. 2001 . Org. Lett. , 3 : 3463