References
- Jia, W.; Chen, X.; Guo, R.; Sui-Seng, C.; Amoroso, D.; Lough, A. J.; Abdur-Rashid, K. Aminophosphine Ligands R2P(CH2)nNH2 and Ruthenium Hydrogenation Catalysts RuCl2(R2P(CH2)nNH2)2. Dalton Trans. 2009, 8301–8307.
- Crystal data for 2: C23H28N2PPd+.Cl–, M = 505.29; monoclinic, P21/c, a = 11.31313(19), b = 24.1283(3), c = 8.62924(16) Å, β = 108.4639(19)°, V = 2234.24(7) Å3; Z = 4, ρcal 1.502 g cm−3; µ(Mo-Kα) = 1.03 mm−1; λ = 0.71075 Å, T = 100(2) K; 48149 reflections were collected on a Rigaku AFC12 FRE+/HyPix 6000 diffractometer3 using narrow ω-scans, 5128 of which were independent (Rint = 0.034). The structure was solved by a charge flipping method and refined on F2 values to give a final R1 = 0.021 for 4663 data with F2>2σ (F2); wR2 = 0.052 for all data.4,5 A complete set of X-ray crystallographic structural data for compound 2 (CCDC 1860468) are available at the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, UK (fax: +44 1223 336 033; e-mail: [email protected]) on request, quoting the deposition number.
- CrysAlis PRO 1.171.39.34b, Rigaku Corp., 2017.
- Sheldrick, G. M. Crystal Structure Refinement with SHELXL. Acta Crystallogr. C Struct. Chem. 2015, 71, 3–8.