References
- (a) Bálint, E.; Tajti, A.; Tripolszky, A. Keglevich, G. Dalton Trans. 2018, 47, 4755–4778. (b) Cao, B.; Elsegood, M. R. J.; Lastra-Calvo, N.; Smith, M. B. J. Organomet. Chem. 2017, 853, 159–167.
- Holm, S. C.; Rominger, F.; Straub, B. F. J. Organomet. Chem. 2012, 719, 54–63.
- Crystal data for 1·CHCl3: C48H55Cl7NOPRu2S, M = 1175.25; triclinic, P1¯, a = 10.4855(7), b = 13.762(1), c = 19.2009(14) Å, α = 105.267(3), β = 99.201(2), γ = 107.657(3)°, V = 2458.8(3) Å3; Z = 2, ρcal 1.587 g cm−3; µ(Mo-Kα) = 1.11 mm−1; λ = 0.71073 Å, T = 100(2) K; 33338 reflections were collected on a Rigaku Saturn724+ diffractometer using narrow ω-scans, 11217 of which were independent (Rint = 0.053). The structure was solved by direct methods and refined on F2 values to give a final R1 = 0.040 for 9586 data with F2>2σ (F2); wR2 = 0.103 for all data. A complete set of X-ray crystallographic structural data for compound 1·CHCl3 (CCDC 1860382) are available at the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, UK (fax: +44 1223 336 033; e-mail: [email protected]) on request, quoting the deposition number.
- Rigaku CrystalClear-SM Expert 3.1 b27, Rigaku Corp., 2012.
- Sheldrick, G. M. Acta Crystallogr. C Struct. Chem. 2015, 71, 3–8.
- Sheldrick, G. M. SHELXTL User Manual, Version 6.12. Bruker AXS Inc.: Madison, WI, USA, 2001.