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Short Communication

Microwave-assisted synthesis of α-aminophosphonates and related derivatives by the Kabachnik-Fields reaction

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Pages 379-381 | Received 31 Oct 2018, Accepted 04 Nov 2018, Published online: 04 Mar 2019

References

  • Keglevich, G.; Bálint, E. The Kabachnik–Fields Reaction: Mechanism and Synthetic Use. Molecules 2012, 17, 12821–12835. DOI:10.3390/molecules171112821.
  • Kabachnik, M. I.; Medved, T. Y. New Synthesis of Aminophosphonic Acids. Dokl. Akad. Nauk SSSR 1952, 83, 689–692.
  • Fields, E. K. The Synthesis of Esters of Substituted Amino Phosphonic Acids. J. Am. Chem. Soc. 1952, 74, 1528–1531. DOI:10.1021/ja01126a054.
  • Bálint, E.; Tripolszky, A.; Tajti, Á. Synthesis of α-Aminophosphonates by the Kabachnik–Fields Reaction and by the Pudovik Reaction, In: Organophosphorus Chemistry, Keglevich, G. ed., Walter de Gruyter GmbH: Berlin, 2018; pp 108–147.
  • Keglevich, G.; Szekrényi, A. Eco-Friendly Accomplishment of the Extended Kabachnik–Fields Reaction; a Solvent- and Catalyst-Free Microwave-Assisted Synthesis of α-Aminophosphonates and α-Aminophosphine Oxides. Lett. Org. Chem. 2008, 5, 616–622. DOI:10.2174/157017808786857598.
  • Tajti, Á.; Bálint, E.; Keglevich, G. Synthesis of Ethyl Octyl α-Aminophosphonate Derivatives. Curr. Org. Synth. 2016, 13, 638–675. DOI:10.2174/1570179413666151218202757.
  • Bálint, E.; Tajti, Á.; Drahos, L.; Ilia, G.; Keglevich, G. Alcoholysis of Dialkyl Phosphites under Microwave Conditions. Curr. Org. Chem. 2013, 17, 555–562. DOI:10.2174/1385272811317050010.
  • Bálint, E.; Tajti, Á.; Tóth, N.; Keglevich, G. Continuous Flow Alcoholysis of Dialkyl H-Phosphonates with Aliphatic Alcohols. Molecules 2018, 23, 1618. DOI:10.3390/molecules23071618.
  • Bálint, E.; Tóth, R. E.; Keglevich, G. Synthesis of Alkyl α‐Aminomethyl‐Phenylphosphinates and N,N‐Bis(alkoxyphenylphosphinylmethyl)Amines by the Microwave‐Assisted Kabachnik–Fields Reaction. Heteroatom Chem. 2016, 27, 323–335. DOI:10.1002/hc.21343.
  • Bálint, E.; Tajti, Á.; Kalocsai, D.; Mátravölgyi, B.; Konstantin, K.; Czugler, M.; Keglevich, G. Synthesis and Utilization of Optically Active α-Aminophosphonate Derivatives by Kabachnik-Fields Reaction. Tetrahedron 2017, 73, 5659–5667.

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