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Original Articles

HEXAALKOXY AND HEXAARYLOXY 1,3,2λ5,4λ5-DIAZADIPHOSPHETIDINES

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Pages 163-172 | Received 15 Aug 1990, Accepted 18 Sep 1990, Published online: 28 Aug 2008

References

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  • R [dbnd] Σ|Fo| - |Fo||/Σ/|Fo| and Rw = {Σw(|Fo| - |Fc|)2/Σw|Fo|2}1/2
  • The 31P chemical shifts for (MeNPCl3)2, (MeNPF3)2, and (PhNPCl3)2 are -76.0, -70.3, and -77.0 δ in CHCI3
  • A value of 1307 cm−1 is reported for v(P[dbnd]N) in MeN[dbnd]P(OMe)2 3
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  • The 1H chemical shift for the N-methyl protons of the monophosphazene MeN[dbnd]P(OMe)3 is 2.78 δ with a J PH of 24 Hz2
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