References
- Veith M. Mathur C. Huch V. , Organometallics , 15 , 2528 ( 1996 ).
- Veith M. Mathur C. Mathur S. Huch V. , Organometallics , 16 , 1292 ( 1997 ).
- Crystal data for 1 C22H32GeMoO8Sn, M = 710.69, orthorhombic, space group Pnma, a = 12.552(14) Å, b = 14.044(14) Å, c = 16.06(2) Å, V = 2831(5) Å3, Z = 2, Dcal = 1.668, F(000) = 1404, λ(MoKα) = 0.71073 Å, T = 293(2) K, μ = 2.405 mm−1 R1 = 0.0258, wR2 = 0.0612. The structure solution (direct methods) and refinement (by full-matrix least squares on F2) were carried out using SHELXS program package.
- Veith M. , Coord. Chem. Rev. , 137 , 297 ( 1994 ).
- Spectral data of 1 : 1H NMR (C6D6, 20 °C) δ 1.40 (s, 27H, OC(CH3)3), 6.33 (s, 5H, C5H5). 13C NMR (C6D6, 20 °C) δ 32.43 (OC(CH3)3), 77.12 (OC(CH3)3), 111.11( C5H5), 207.32 (CO). 119Sn NMR (C6D6, 20 °C) δ - 184.6.