Advanced search
Publication Cover
Integrated Ferroelectrics
An International Journal
Volume 213, 2021 - Issue 1
Submit an article Journal homepage
169
Views
0
CrossRef citations to date
0
Altmetric
Research Article

Preparation of Silicalite-1 Nanosheets and its Application in Vapor-Phase Beckmann Rearrangement of Cyclohexanone Oxime

Chao Gea College of Textile Engineering, Taiyuan University of Technology, Taiyuan, ChinaView further author information
,
Xiaofeng Lib College of Chemistry and Chemical Engineering, Taiyuan University of Technology, Taiyuan, ChinaView further author information
,
Zhou Zhaoa College of Textile Engineering, Taiyuan University of Technology, Taiyuan, ChinaView further author information
,
Zhifeng Yana College of Textile Engineering, Taiyuan University of Technology, Taiyuan, ChinaView further author information
,
Dandan Liana College of Textile Engineering, Taiyuan University of Technology, Taiyuan, ChinaView further author information
&
Jianjun Lua College of Textile Engineering, Taiyuan University of Technology, Taiyuan, ChinaCorrespondence[email protected]
View further author information
Pages 12-20 | Received 30 May 2019, Accepted 06 Aug 2019, Published online: 28 Feb 2021

References

  • H. J. Kiely-Collins et al., Mild, calcium catalysed Beckmann rearrangements, Chem. Commun. (Camb.) 54 (6), 654 (2018). DOI: 10.1039/c7cc09491d.
  • Z. Wang et al., Acidity enhanced [Al]MCM-41 via ultrasonic irradiation for the Beckmann rearrangement of cyclohexanone oxime to ɛ -caprolactam, J. Catal. 358, 71 (2018). DOI: 10.1016/j.jcat.2017.11.013.
  • L. Forni et al., Vapor phase Beckmann rearrangement using high silica zeolite catalyst, Phys. Chem. Chem. Phys. 6 (8), 1842 (2004). DOI: 10.1039/B316810G.
  • R. Kumar, and B. Chowdhury, Comprehensive study for vapor phase Beckmann rearrangement reaction over zeolite systems, Ind. Eng. Chem. Res. 53 (43), 16587 (2014). DOI: 10.1021/ie503170n.
  • S. A. Khayyat, R. Selvin, and A. Umar, Beckmann rearrangement of cyclohexanone oxime using nanocrystalline titanium silicalite-1 (TS-1), J. Nanosci. Nanotechnol. 17 (3), 2170 (2017). DOI: 10.1166/jnn.2017.12724.
  • C. C. Tsai et al., Vapor phase Beckmann rearrangement of cyclohexanone oxime over MCM-22, Appl. Catal. A: Gen. 267 (1–2), 87 (2004). DOI: 10.1016/j.apcata.2004.02.026.
  • G. P. Heitmann, G. Dahlhoff, and W. Hölderich, Catalytically active sites for the Beckmann rearrangement of cyclohexanone oxime to ε-caprolactam, J. Catal. 186 (1), 12 (1999). DOI: 10.1006/jcat.1999.2552.
  • C. Ge et al., Kinetic study of vapor-phase Beckmann rearrangement of cyclohexanone oxime over silicalite-1, Chem. Eng. Sci. 153, 246 (2016). DOI: 10.1016/j.ces.2016.07.029.
  • I. Yoshitaka et al., Development and industrialization of the vapor-phase Beckmann rearrangement process, Bull. Chem. Soc. Jpn. 80, 1280 (2007).
  • R. Kumar et al., Highly stable In-SBA-15 catalyst for vapor phase Beckmann rearrangement reaction, Micropor. Mesopor. Mat. 234, 293 (2016). DOI: 10.1016/j.micromeso.2016.07.024.
  • Z. Wang et al., Idenification of vicinal silanols and promotion of their formation on MCM-41 via ultrasonic assisted one-step room-temperature synthesis for Beckmann rearrangement, Ind. Eng. Chem. Res. 57 (16), 5550 (2018). DOI: 10.1021/acs.iecr.8b00274.
  • Y. Q. Deng, S. F. Yin, and C. T. Au, Preparation of nanosized silicalite-1 and its application in vapor-phase Beckmann rearrangement of cyclohexanone oxime, Ind. Eng. Chem. Res. 51 (28), 9492 (2012). DOI: 10.1021/ie3001277.
  • J. Kim, W. Park, and R. Ryoo, Surfactant-directed zeolite nanosheets: A high-performance catalyst for gas-phase Beckmann rearrangement, ACS Catal. 1 (4), 337 (2011). DOI: 10.1021/cs100160g.
  • M. Choi et al., Stable single-unit-cell nanosheets of zeolite MFI as active and long-lived catalysts, Nature 461 (7261), 246 (2009). DOI: 10.1038/nature08288.
  • H. Mochizuki et al., Facile control of crystallite size of ZSM-5 catalyst for cracking of hexane, Micropor. Mesopor. Mat. 145 (1–3), 165 (2011). DOI: 10.1016/j.micromeso.2011.05.011.
  • A. G. Machoke et al., Synthesis of multilamellar MFI-type zeolites under static conditions: The role of gel composition on their properties, Micropor. Mesopor. Mat. 190, 324 (2014). DOI: 10.1016/j.micromeso.2014.02.026.
  • G. P. Heitmann et al., Active sites of a [B]-ZSM-5 zeolite catalyst for the Beckmann rearrangement of cyclohexanone oxime to caprolactam, J. Catal. 194 (1), 122 (2000). DOI: 10.1006/jcat.2000.2928.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Order Reprints Request Corporate Permissions

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

Request Academic Permissions

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.

Related research

People also read lists articles that other readers of this article have read.

Recommended articles lists articles that we recommend and is powered by our AI driven recommendation engine.

Cited by lists all citing articles based on Crossref citations.
Articles with the Crossref icon will open in a new tab.