Solid State Bimolecular Photoreaction in a Simple Polycrystalline Mixture of Acridine and Carbazole

References

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• Selected data for 3: mp 257–259 °C (MeCN); IR (KBr) no NH band; 1H NMR (THF-d8) δ 8.17–8.42 (m, 4H), 7.62–7.90 (m, 2H), 7.06–7.40 (m, 8H), 6.70–6.83 (m, 2H); UV λmax (5% THF in MeCN) 361 (log ϵ 4.04), 289 (4.18), 249 nm (5.07). Anal. calcd for C25H16N2: C, 87.18; H, 4.68; N, 8.13. Found: C, 87.58; H, 4.81; N, 8.17.
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• Crystal data of 3: yellow prism crystal (MeCN); M = 344.42; 0.10 × 0.10 × 0.30 mm; monoclinic; space group P21; a = 11.366(1), b = 11.8813(9), c = 12.7956(8) Å, β = 93.172(6)°; V = 93.172(6) Å3; Z = 4; Dc = 1.326 g cm 3; GOF 2.47. The structure was solved by direct method (SHELX86) and refined by the full-matrix least-squares procedure to R = 0.050 and Rw = 0.090 for 2392 independent observed reflectons [F0 > 3[sgrave](F0)] of total 2877 reflections with 2θ < 120.1° using Cu Kα radiation.
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