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Original Articles

Molecular Inclusion Crystals of Novel Heterocyclic Host Compounds

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Pages 173-184 | Published online: 04 Oct 2006

References

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  • Crystal data of 8 (R1=C1, R2=R3=R4=H) C31H34N8Cl6, M=731.38, triclinic, space group P1 (#2), a=10.42(1), b=14.557(8). c=12.13(1)Å, α=90.00(6)° β=105.78(8)°, γ= 90.03 (8)°.V=1772(3)Å3, Z=2, Dc=1.371 gcm−3 μ=5.20 cm−1. The structure solution (direct methods) and refinement (full-matrix least-squares) was performed using the TEXSAN software and basedon 2677 observed intensities [F>3.0σ(F)] from 8570 measured data (2θ55.1°). Final R and RW values were 0.117 and 0.131
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  • Matsumoto , K. , Okamoto , T. , Sera , A. , Itoh , K. and Hamada , K. 1987 . Chem. Lett. , : 805
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  • Crystal data of 11: C32H26N6O4, M=558.60, monoclinic, space group Cc (#9), a=8.548(4), b=24.467(4), c=14.966 (2)Å, β=100.59 (2)°, V=3077(1)Å3, Z=4, Dc=1.206 gcm−3, μ=0.77 cm−1. The structure solution (direct methods) and refinement (full-matrix least-squares) was performed using the TEXSAN software and based on 183 observed intensities [F>3.0σ(F)] from 818 measured data (2θ<55.1°). Final R and Rw values were 0.068 and 0.066
  • Acheson , R. M. 1965 . Adv. Heterocycl. Chem. , 1 : 125
  • Acheson , R. M. and Elmore , N. F. 1978 . Adv, Heterocycl. Chem. , 23 : 263
  • Matsumoto , K. , Uchida , T. , Aoyama , K. , Nishikawa , M. , Kuroda , T. and Okamoto , T. 1988 . J. Heterocycl. Chem. , 25 : 1793
  • Matsumoto , K. , Ikemi , Y. , Toda , M. , Uchida , T. and Kakehi , A. 1992 . Heterocycles , 34 : 2239
  • Crystal data of 13: C42H32N4O8Cl2, M=791.64, monoclinic, space group P21/c (#14), a=15.005(2), b=8.9852(9), c=29.129(4)Å, β=100.92(1)°, V=3856.2(9)Å3, Z=4, Dc=1.363 gcm−3, μ=20.14 cm−1. The structure solution (direct methods) and refinement (full-matrix least-squares) was performed using the TEXSAN software and based on 3001 observed intensities [F>3.0σ(F)]from 5481 measured data (2θ<120°). Final R and Rw values were 0.053 and 0.071

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