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- Kim , J.U. , Cha , S.H. , Shin , K. , Jho , J.Y. and Lee , J.C. 2005 . J. Am. Chem. Soc. , 127 : 9962 – 9963 . The specimens for TEM analysis were not stained. The larger (20–30 nm) and very dark spots present on the fibres correspond to elemental Ag nanoparticles (as confirmed by EDS), coming from the reduction of part of the Ag+ during the formation of 4, where the thiol acts as the reducing agent. These nanoparticles are also formed during the TEM analysis, by reduction with the electron beam. See for example:
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