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Original Articles

Polymerization of Diphenylcarbodiimide Catalysed by Fullerene-60

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Pages 399-406 | Received 16 Oct 1995, Published online: 19 Aug 2006

References

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  • Representative data for 4: 13C NMR (JEOL GSX 400 MHz, DMSO-d6 + CDC13) δ 152.766, 149.153, 139.955, 134.991, 129.147, 129.071, 128.965, 128.495, 121.952 and 118.340 ppm.; 1H NMR (JEOL GSX 400 MHz DMSO-d6+CDCl3) δ 7.437 (q).; FT-IR (KBr) cm−1 : 3327.5(m), 3061.7(w), 2924(w), 2853.4(w), 2138.9(w), 1711(vs), 1650.2(s), 1593.8(s), 1554.7(s), 1494.9(s), 1415.5(s), 1314.1(m), 1209.9(s), 1072.9(w), 1027(w), 895.8(w), 827.4(w), 755(s), 694(s), 690(m), 529.2(w) and 510.4(w).; UV-Vis λ max (CH2C12) 284.5 nm.; Anal. (C13N2H10)6 C, H, N: Calcd, 80.39.; found, 73.58: calcd, 5.19.; found, 5.30.; Calcd, 14.42.; found, 11.85.

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