A NOVEL HPLC METHOD FOR THE DETERMINATION OF ALPHA-KETO ACIDS IN HUMAN SERUM USING MESO STILLBENEDIAMINE AS DERIVATIZATION REAGENT

REFERENCES

• Funai , T. ; Ichiyana , A. High-Performance Liquid Chromatographic Determination of Glyoxylate in Rat Liver . J. Biochem. 1986 , 99 , 323 – 327 .
   Google Scholar
• Wang , Z. J. ; Zaitsu , K. ; Ohkura , Y. High-Performance Liquid Chromatographic Determination of α-keto Acids in Human Serum and Urine Using 1, 2-diamino-4, 5-Methylenedioxybenzene as a Precolumn Fluorescence Derivatization Reagent . J. Chromatogr. 1988 , 430 , 223 – 231 .
   PubMed Web of Science ®Google Scholar
• Livesey , G. ; Lund , P. Binding of Branched-Chain 2-oxo Acids to Bovine Serum Albumin . J. Biochem. 1982 , 204 , 265 – 72 .
   Google Scholar
• Hutson , S. M. ; Harper , A. E. Blood and Tissue Branched-Chain Amino and Alpha-Keto Acid Concentrations: Effect of Diet, Starvation, and Disease . Am. J. Clin. Nutr. 1981 , 34 , 173 – 183 .
   PubMed Web of Science ®Google Scholar
• Schauder , P. ; Herbertz , L. ; Langenbeck , U. Serum Branched Chain Amino and Keto Acid Response to Fasting in Humans . Metabolism. Jan. 1985 , 34 , 58 – 61 .
   PubMed Web of Science ®Google Scholar
• Schauder , P. ; Schröder , K. ; Matthaei , D. ; Henning , H. V. ; Langenbeck , U. Influence of Insulin on Blood Levels of Branched Chain Keto and Amino Acids in Man . Metabolism. Apr. 1983 , 32 , 323 – 327 .
   PubMed Web of Science ®Google Scholar
• Nakahara , T. ; Ishida , J. ; Yamaguchi , M. ; Nakamura , M. Determination of α-keto Acids Including Phenylpyruvic Acid in Human Plasma by High-Performance Liquid Chromatography with Chemiluminescence Detection. Anal. Biochem. 1990, 190, 309–313.
   PubMed Web of Science ®Google Scholar
• Lange , M. ; Malyusz , M. Fast Method for the Simultaneous Determination of 2- oxo Acids in Biological Fluids by High Performance Liquid Chromatography . J. Chromatogr. B. 1994 , 662 , 97 – 102 .
   PubMedGoogle Scholar
• Fu , X. ; Kimura , M. ; lga , M. ; Yamaguchi , S. GAS CHROMATOGRAPHIC–MASS Spectrometric Screening for Organic Acidemias Using Dried Urine Filter Paper: Determination of α-ketoacids . J. Chromatogr. B. 2001 , 758 , 87 – 94 .
   PubMedGoogle Scholar
• Pailla , K. ; Blonde-Cynober , F. ; Aussel , C. ; De Bandt , J. P. ; Cynober , L. Branched Chain α-keto acids and Pyruvate in Blood Measurement by HPLC with Fluorimetric Detection and Changes in Order Subjects . Clin. Chem. 2000 , 46 , 848 – 853 .
   PubMed Web of Science ®Google Scholar
• Muhling , J. ; Fuchs , M. ; Campos , M. E. ; Gonter , J. ; Engel , J. M. ; Sablotzki , A. ; Menges , T. ; Weiss , S. ; Dehne , M. G. ; Krull , M. ; Hempelmann , G. Quantitative Determination of Free Intracellular Alpha-keto Acids in Neutrophils . J. Chromatogr. B 2003 , 789 , 383 – 392 .
   PubMed Web of Science ®Google Scholar
• Mitsui , A. ; Nohta , H. ; Ohkur , Y. High-Performance Liquid Chromatography of Plasma Catechol Amines Using 1, 2-diphenylethylenediamines as a Precolumn Fluorescence Derivatization Reagent . J. Chromatogr. 1985 , 344 , 61 – 70 .
   PubMed Web of Science ®Google Scholar
• Schwartz , H. P. ; Karl , l. E. ; Bler , D. M. The α - keto acids of Branched Chain Amino Acids: Simplified Derivatization for Physiological Samples and Complete Separation as Quinoxalinols by Packed Column Gas Chromatography . Anal. Biochem. 1980 , 108 , 360 – 366 .
   PubMed Web of Science ®Google Scholar
• Urbansky , E. T. Isotopic Determination of Organic Keto Acid Pentafluorobenzyl Esters in Biological Fluids by Negative Chemical Ionization in Gas Chromatography /Massspectrometry . J. Environ. Moit. 2000 , 2 , 334 – 338 .
   PubMedGoogle Scholar
• Hara , S. ; Takemori , Y. ; Yamaguchi , M. ; Nakamura , M. ; Ohkura , Y. Determination of Alpha-Keto Acids in Serum and Urine by High-Performance Liquid Chromatography with Fluorescence Detection . J. Chromatogr. 1985 , 344 , 33 – 39 .
   PubMed Web of Science ®Google Scholar
• Garibotto , G. ; Ancarani , P. ; Russo , R. ; Sala , M. R. ; Fiorini , F. ; Paoletti , E. Reversed-Phase High-Performance Liquid Chromatographic Analysis of Branched-Chain Keto Acid Hydrazone Derivatives: Optimization of Techniques and Application to Branched-Chain Keto Acid Balance Studies Across the Forearm . J. Chromatogr. 1991 , 572 , 11 – 23 .
   PubMed Web of Science ®Google Scholar
• Hirata , T. ; Kai , M. ; Kohashi , K. ; Ohkura , Y. Determination of Phenylpyruvic Acid in Urine and Serum by High-Performance Liquid Chromatography with Fluorescence Detection . J. Chromatogr. 1981 , 226 , 25 .
   PubMed Web of Science ®Google Scholar
• Fuchs , M. ; Engel , J. ; Compos , M. ; Matejec , R. ; Henrich , M. ; Harbach , H. ; Wolff , M. ; Weismuller , K. ; Menges , T. , Heidt , M. C. ; Welters , I. D. ; Krull , M. ; Hempelmann , G. ; Muhling , J. Intracellular Alpha-Keto Acid Quantification by Fluorescence-HPLC . Amino Acid. 2009 , 36 , 1 – 11 .
   PubMed Web of Science ®Google Scholar
• Vander Hoorn , F. A. J. ; Boomsma , F. ; Man In't Veld , A. J. ; Schalekamp , M. A. Determination of Catecholamines in Human Plasma by High-Performance Liquid Chromatography: Comparison Between a New Method with Fluorescence Detection and an Established Method with Electrochemical Detection . J. Chromatogr. B. 1989 , 487 , 17 – 28 .
   Google Scholar
• Khuhawar , M. Y. ; Kandro , A. J. ; khand , F. D. Liquid Chromatographic Determination of Glyoxal and Methylglyoxal from serum of Diabetic Patients using Meso Stilbenediamine as Derivatizing Reagent . Anal. Lett. 2006 , 39 , 2205 – 2215 .
   Web of Science ®Google Scholar
• Shabir , G. A. ; Lough , W. J. ; Shafique , A. A. ; Bradshaw , T. K. Evaluation and Application of Best Practice in Analytical Method Validation . J. Liq. Chromatogr. R. T. 2007 , 30 , 311 – 333 .
   Web of Science ®Google Scholar