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Original Articles

A Combination of Isocratic and Gradient Elution Modes in HPLC with the Aid of Time-Overlapping Process for Rapid Determination of Methyldopa in Human Urine

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References

  • Benowitz , N. L. Basic and Clinical Pharmacology, , 9th ed. ; Katzung , B. G. , Ed.; The McGraw-Hill Companies : New York , 2004 , p 166 .
  • The United States Pharmacopoeia, , 24th ed. ; The United States Pharmacopoeial Convention : Rockville , MD , 2000 .
  • Salem , F. B. Spectrophotometric and Fluorimetric Determination of Catecholamines . Anal. Lett. 1993 , 26 ( 2 ), 281 – 294 .
  • Ribeiro , P. R. S. ; Pezza , L. ; Pezza , H. R. Spectrophotometric Determination of Methyldopa in Pharmaceutical Formulation . Eclética Quími. 2005 , 30 ( 3 ), 23 – 28 .
  • Alexey , E. P. ; Anastasia , V. D. ; Svetlana , V. M. ; Tatiana , N. S. A Peroxidase-Based Method for the Determination of Dopamine, Adrenaline, and α-Methyldopa in the Presence of Thyroid Hormones in Pharmaceutical Forms . Talanta 2011 , 84 ( 3 ), 710 – 716 .
  • Athanasiou-Malaki , E. M. ; Koupparis , M. A. Indirect Potentiometric Determination of α-Amino acids with a Copper-Selective Electrode and Determination of Dopa and Methyldopa in Pharmaceutical Preparations . Anal. Chim. Acta 1984 , 161 , 349 – 353 .
  • Martens , J. ; Guenther , K. ; Schickedanz , M. Resolution of Optical Isomers by Thin-Layer Chromatography: Enantiomeric Purity of Methyldopa . Archiv. Pharm. 1986 , 319 ( 6 ), 572 – 574 .
  • Watson , J. R. ; Lawrence , R. C. Specific Quantitative Gas-Liquid Chromatographic Analysis of Methyldopa and Some Foreign Related Amino Acids in Raw Material and Commercial Tablets . J. Chromatogr. A 1975 , 103 ( 1 ), 63 – 70 .
  • Rosa , M. V. C. ; Jose , M. S. M. ; Jose , R. T. L. ; Guillermo , R. R. Analysis of Pharmaceutical Preparations Containing Catecholamines by Micellar Liquid Chromatography with Spectrophotometric Detection . Analyst 1995 , 120 ( 6 ), 1767 – 1772 .
  • Róna , K. ; Ary , K. ; Gachályi , B. ; Klebovich , I. Determination of α-Methyldopa in Human Plasma by Validated High-Performance Liquid Chromatography with Fluorescence Detection. J. Chromatogr. A 1996, 730 (1–2), 125–131.
  • Li , S. F. ; Wu , H. L. ; Yu , Y. J. ; Li , Y. N. ; Nie , J. F. ; Fu , H. Y. ; Yu , R. Q. Quantitative Analysis of Levodopa, Carbidopa and Methyldopa in Human Plasma Samples Using HPLC-DAD Combined with Second-Order Calibration Based on Alternating Trilinear Decomposition Algorithm . Talanta 2010 , 81 ( 3 ), 805 – 812 .
  • Bahrami , G. ; Kiani , A. ; Mirzaeei , S. A Rapid High Performance Liquid Chromatographic Determination of Methyldopa in Human Serum with Fluorescence Detection and Alumina Extraction: Application to a Bioequivalence Study . J. Chromatogr. B 2006 , 832 ( 2 ), 197 – 201 .
  • Zečević , M. ; Živanović , L. J. ; Agatonovic-Kustrin , S. ; Minic , D. The Use of a Response Surface Methodology on HPLC Analysis of Methyldopa, Amiloride and Hydrochlorothiazide in Tablets . J. Pharm. Biomed. Anal. 2001 , 24 ( 5–6 ), 1019 – 1025 .
  • Muzzi , C. ; Bertocci , E. ; Terzuoli , L. ; Porcelli , B. ; Ciari , I. ; Pagani , R. ; Guerranti , R. Simultaneous Determination of Serum Concentrations of Levodopa, Dopamine, 3-O-Methyldopa and α-Methyldopa by HPLC . Biomed. Pharmacother. 2008 , 62 ( 4 ), 253 – 258 .
  • Lucarelli , C. ; Betto , P. ; Ricciarello , G. ; Grossi , G. High-Performance Liquid Chromatographic Determination of L-3- (3,4-Dihydroxyphenyl)-2-Methylalanine (α-Methyldopa) in Human Urine and Plasma . J. Chromatogr. A 1991 , 541 ( 1–2 ), 285 – 296 .
  • Kochak , G. M. ; Mason , W. D. Determination of Free Methyldopa in Plasma by High-Pressure Liquid Chromatography and Electrochemical Detection . J. Pharm. Sci. 1980 , 69 ( 8 ), 897 – 900 .
  • Mell , L. D. ; Gustafson , A. B. Urinary Free Methyldopa Determined by Reversed-Phase High-Performance Liquid Chromatography . Clin. Chem. 1978 , 24 ( 1 ), 23 – 26 .
  • Metwally , M. el-S. Stability-Indicating High-Performance Liquid Chromatographic Assay for α-Methyldopa in Sustained-Release Capsules . J. Chromatogr. A 1991 , 549 ( 1–2 ), 221 – 228 .
  • Ehrenström , F. ; Johansson , P. A Method for Very Rapid Determinations of Catechols Using Ion-Pairing Reverse Phase HPLC with Electrochemical Detection: Effects of L-Dopa Treatment on the Catechol Content in Various Rat Brain Structures . Life Sci. 1985 , 36 ( 9 ), 867 – 879 .
  • Causon , R. C. ; Carruthers , M. E. Measurement of Catecholamines in Biological Fluids by High-Performance Liquid Chromatography: A Comparison of Fluorimetric with Electrochemical Detection . J. Chromatogr. B 1982 , 229 ( 2 ), 301 – 309 .
  • Cooper , M. J. ; O'Dea , R. F. ; Mirkin , B. L. Determination of Methyldopa and Metabolites in Human Serum by High-Performance Liquid Chromatography with Electrochemical Detection . J. Chromatogr. B 1979 , 162 ( 4 ), 601 – 604 .
  • Munion , G. L. ; Seaton , J. F. ; Harrison , T. S. HPLC for Urinary Catecholamines and Metanephrines with Alpha-Methyldopa . J. Surg. Res. 1983 , 35 ( 6 ), 507 – 514 .
  • Kochak , G. M. ; Mason , W. D. A Simplified Method of Determining Free Methyldopa in Urine . Anal. Lett. 1981 , 14 ( 6 ), 439 – 449 .
  • Ribeiro , P. R. ; Neto , J. A. ; Pezza , L. ; Pezza , H. R. Flow-Injection Spectrophotometric Determination of Methyldopa in Pharmaceutical Formulations . Talanta 2005 , 67 ( 1 ), 240 – 244 .
  • Ali , S. A. ; Sami , M. A. Cyclic Voltametric Study of Alpha-Methyldopa at Carbon Paste Electrode . Pak. J. Pharm. Sci. 2005 , 18 ( 1 ), 6 – 17 .
  • Talebpour , Z. ; Haghgoo , S. ; Shamsipur , M. 1H Nuclear Magnetic Resonance Spectroscopy Analysis for Simultaneous Determination of Levodopa, Carbidopa and Methyldopa in Human Serum and Pharmaceutical Formulations . Anal. Chim. Acta 2004 , 506 ( 1 ), 97 – 104 .
  • Matthieu , T. ; Debora , C. D. V. B. ; Jose , A. R. R. Kinetic Method for the Determination of α‐Methyldopa in Pharmaceutical Preparations: Analytical Procedure and Reaction Mechanism Considerations . Anal. Lett. 2006 , 39 ( 2 ), 327 – 339 .
  • Stewart , J. T. ; Lo , H. C. ; Mason , W. D.. Determination of Methyldopa in Pharmaceutical Dosage Forms and Biological Fluids Based on Oxidation at the Tubular Carbon Electrode . J. Pharm. Sci. 1974 , 63 ( 6 ), 954 – 955 .
  • Ballantine , J. ; Woolfson , A. D.. Determination of Catecholamines in Pharmaceutical Preparations by Differential Pulse Polarography at the Glassy Carbon Electrode . Int. J. Pharm. 1979 , 3 ( 4–5 ), 239 – 246 .
  • Salmanipour , A. ; Taher , M. A. ; Beitollahi , H. Voltammetric Behavior of a Multi-Walled Carbon Nanotube Modified Electrode-Ferrocene Electrocatalyst System as a Sensor for Determination of Methyldopa in the Presence of Folic Acid . Anal. Methods 2012 , 4 ( 9 ), 2982 – 2988 .
  • Shahrokhian , S. ; Rastgar , S. Electrodeposition of Pt–Ru Nanoparticles on Multi-Walled Carbon Nanotubes: Application in Sensitive Voltammetric Determination of Methyldopa . Electrochim. Acta 2011 , 58 , 125 – 133 .
  • Gholivand , M. B. ; Amiri , M. Preparation of Polypyrrole/Nuclear Fast Red Films on Gold Electrode and Its Application on the Electrocatalytic Determination of Methyl-Dopa and Ascorbic Acid . Electroanalysis 2009 , 21 ( 22 ), 2461 – 2467 .
  • Gholivand , M. B. ; Amiri , M. Highly Sensitive and Selective Determination Methyldopa in the Presence of Ascorbic Acid Using OPPy/TY/Au Modified Electrode . J. Electroanal. Chem. 2013 , 694 , 56 – 60 .
  • Rezaei , B. ; Askarpour , N. ; Ensafi , A. A. Adsorptive Stripping Voltammetry Determination of Methyldopa on the Surface of a Carboxylated Multiwall Carbon Nanotubes Modified Glassy Carbon Electrode in Biological and Pharmaceutical Samples . Colloids Surf., B 2013 , 109 , 253 – 258 .
  • Oliveira , C. H. ; Barrientos-Astigarraga , R. E. ; Sucupira , M. ; Graudenz , G. S. ; Muscará , M. N. ; De , N. G. Quantification of Methyldopa in Human Plasma by High-Performance Liquid Chromatography–Electrospray Tandem Mass Spectrometry Application to a Bioequivalence Study . J. Chromatogr. B 2002 , 768 ( 2 ), 341 – 348 .
  • Guideline ICH: Q2 (R1): Validation of Analytical Procedures: Text and Methodology. The International Conference on Harmonization: London, 2005 .

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