Chemometric Approach for RP-HPLC Determination of Azithromycin, Secnidazole, and Fluconazole Using Response Surface Methodology

References

• Malhotra, M.; Sharma, J. B.; Batra, S.; Arora, R.; Sharma, S. Ciprofloxacin-Tinidazole Combination, Fluconazole- Azithromicin-Secnidazole-Kit and Doxycycline- Metronidazole Combination Therapy in Syndromic Management of Pelvic Inflammatory Disease: A Prospective Randomized Controlled Trial. Indian J. Med. Sci. 2003, 57, 549–555.
   PubMedGoogle Scholar
• Sharma, J. B.; Mittal, S.; Raina, U.; Chanana, C. Comparative Efficacy of Two Regimens in Syndromic Management of Lower Genital Infections. Arch. Gynecol. Obstet. 2006, 273 (4), 232–235.
   PubMedGoogle Scholar
• Vander Heyden, Y.; Nijhuis, A.; Smeyers-Verbeke, J.; Vandeginste, B. G. M.; Massart, D. L. Guidance for Robustness: Ruggedness Tests in Method Validation. J. Pharm. Biomed. Anal. 2001, 24 (5), 723–753.
   PubMed Web of Science ®Google Scholar
• Sahu, P. K.; Patro, C. S. Application of Chemometric Response Surface Methodology in Development and Optimization of a RP-HPLC Method for the Separation of Metaxalone and Its Base Hydrolytic Impurities. J. Liq. Chromatogr. Related Technol. 2013, 37 (17), 2444–2464.
   Web of Science ®Google Scholar
• Al-Rimawi, F.; Kharoaf, M. Analysis of Azithromycin and Its Related Compounds by RP-HPLC with UV Detection. J. Chromatogr. Sci. 2010, 48, 86–90.
   PubMed Web of Science ®Google Scholar
• Zubata, P.; Ceresole, R.; Rosasco, M. A.; Pizzorno, M. T. A New HPLC Method for Azithromycin Quantitation. J. Pharm. Biomed. Anal. 2002, 27 (5), 833–836.
   PubMed Web of Science ®Google Scholar
• Yang, Z. Y.; Wang, L.; Tang, X. Determination of Azithromycin by Ion-Pair HPLC with UV Detection. J. Pharm. Biomed. Anal. 2009, 49 (3), 811–815.
   PubMed Web of Science ®Google Scholar
• Miguel, L.; Barbas, C. LC Determination of Impurities in Azithromycin Tablets. J. Pharm. Biomed. Anal. 2003, 33 (2), 211–217.
   PubMed Web of Science ®Google Scholar
• Wigman, L. S.; Darrington, R. T.; Young, J. W. An Accurate Procedure for the Analysis of Azithromycin in Ferret Feces Using Solid Phase Extraction and HPLC. J. Liq. Chromatogr. Related Technol. 1998, 21 (6), 819–828.
   Web of Science ®Google Scholar
• El-Gindy, A.; Attia Khalid, A.; Wafaa, N. M.; Al Abasawi Nasr, M.; Al-Shabrawi, M. Optimization and Validation of a Stability-Indicating RP-HPLC Method for Determination of Azithromycin and Its Related Compounds. J. AOAC Int. 2011, 94 (2), 513–522.
   PubMed Web of Science ®Google Scholar
• Li, X.; Sun, J.; Wang, G.; Zheng, Y.; Yan, B.; Xie, H.; Gu, Y.; Ren, H. Determination of Secnidazole in Human Plasma by High-Performance Liquid Chromatography with UV Detection and its Application to the Bioequivalence Studies. Biomed. Chromatogr. 2007, 21 (3), 304–309.
   PubMed Web of Science ®Google Scholar
• El Wallily, A. F.; Abdine, H. H.; Razak, O. A.; Zamel, S. Spectrophotometric and HPLC Determination of Secnidazole in Pharmaceutical Tablets. J. Pharm. Biomed. Anal. 2000, 22 (6), 887–897.
   PubMed Web of Science ®Google Scholar
• Zhang, J. L.; Yuan, Y. Z.; Qian, W.; Zhang, M. Determination of Secnidazole and Its Related Substances by HPLC. J. China Pharm. Univ. 2009, 40 (6), 527–530.
   Google Scholar
• Montovani, P. A. B.; Pinto, A. M. P.; Santos, B. D. M.; Vieira, D. L.; Prado, W. D. A.; Manfio, J. L. Bioavailability of Two Oral Formulas of Secnidazole in Healthy Volunteers. Braz. J. Pharm. Sci. 2009, 45 (4), 687–692.
   Web of Science ®Google Scholar
• Moustafa, A. A.; Bibawy, L. I. Stability-Indicating Assay of Secnidazole in the Presence of Its Degradation Products. Spectrosc. Lett. Int. J. Rapid Commun. 1999, 32 (6), 1073–1098.
   Web of Science ®Google Scholar
• Majcherczyk, P. A.; Moreillon, P.; Decosterd, L. A.; Sanglard, D.; Bille, J.; Glauser, M. P.; Marchetti, O. Single-Step Extraction of Fluconazole from Plasma by Ultra-Filtration for the Measurement of Its Free Concentration by High Performance Liquid Chromatography. J. Pharm. Biomed. Anal. 2002, 28 (3), 645–651.
   PubMed Web of Science ®Google Scholar
• Wattananat, T.; Akarawut, W. Validated HPLC Method for the Determination of Fluconazole in Human Plasma. Biomed. Chromatogr. 2006, 20 (1), 1–3.
   PubMed Web of Science ®Google Scholar
• Al-Rimawi, F. Development and Validation of Analytical Method for Fluconazole and Fluconazole Related Compounds (A, B, and C) in Capsule Formulations by HPLC with UV Detection. Jordan J. Chem. 2009, 4 (4), 357–365.
   Google Scholar
• Aloudah, N. M.; Radwan, M. A.; Al Omar, N. F.; Jacobs, S. HPLC Assay of Fluconazole and Its Application to Patients with Early Septic Shock. J. Liq. Chromatogr. Related Technol. 2005, 28, 591–600.
   Web of Science ®Google Scholar
• Singh, A.; Sharma, P. K.; Majumdar, D. K. Development and Validation of New HPLC-Methods for Estimation of Fluconazole in Different Simulated Biological Fluids: A Comparative Study. J. Liq. Chromatogr. Related Technol. 2014, 37 (4), 594–607.
   Web of Science ®Google Scholar
• Yanamandra, R.; Chaudhary, A.; Rao, B. S.; Patro, B.; Murthy, Y. L. N.; Ramaiah, P. A.; Sastry, C. S. P. UPLC Method for Simultaneous Separation and Estimation of Secnidazole, Fluconazole and Azithromycin in Pharmaceutical Dosage Forms. E-J. Chem. 2010, 7 (S1), S363–S371.
   Google Scholar
• Schmidt, A. H.; Molnár, I. Using an Innovative Quality-by-Design Approach for Development of a Stability Indicating UHPLC Method for Ebastine in the API and Pharmaceutical Formulations. J. Pharm. Biomed. Anal. 2013, 78–79, 65–74.
   PubMed Web of Science ®Google Scholar
• Snyder, L. R.; Kirkland, J. J.; Glajch, J. L. Practical HPLC Method Development, 2nd ed.; Wiley-Interscience: New York, 1997.
   Google Scholar
• Barmpalexis, P.; Kanaze, F. I.; Georgarakis, E. Developing and Optimizing a Validated Isocratic Reversed-Phase High-Performance Liquid Chromatography Separation of Nimodipine and Impurities in Tablets Using Experimental Design Methodology. J. Pharm. Biomed. Anal. 2009, 49, 1192–1202.
   PubMed Web of Science ®Google Scholar