Production and Fractionation of Xylose Oligomers from Switchgrass Hemicelluloses Using Centrifugal Partition Chromatography

References

• Somerville, C.; Bauer, S.; Brininstool, G.; Facette, M.; Hamann, T.; Milne, J.; Osborne, E.; Paredez, A.; Persson, S.; Raab, T.; Vorwerk, S.; Youngs, H. Toward a Systems Approach to Understanding Plant Cell Walls. Science 2004, 306, 2206–2210.
   PubMed Web of Science ®Google Scholar
• Saha, B. Hemicellulose Bioconversion. J. Ind. Microbiol. Biotechnol. 2003, 30, 279–291.
   PubMed Web of Science ®Google Scholar
• Moure, A.; Gullon, P.; Dominguez, H.; Parajo, J. Advances in the Manufacture, Purification and Applications of Xylo-Oligosaccharides as Food Additives and Nutraceuticals. Proc. Biochem. 2006, 41, 1913–1923.
   Web of Science ®Google Scholar
• Li, X.; Converse, A.; Wyman, C. Characterization of Molecular Weight Distribution of Oligomers from Autocatalyzed Batch Hydrolysis of Xylan. J. Ind. Microbiol. Biotechnol. 2003, 105–108, 515–520.
   Google Scholar
• Nabarlatz, D.; Farriol, X.; Montane, D. Kinetic Modeling of the Autohydrolysis of Lignocellulosic Biomass for the Production of Hemicellulose-Derived Oligosaccharides. Ind. Eng. Chem. Res. 2004, 43, 4124–4131.
   Web of Science ®Google Scholar
• Vazquez, M.; Alonso, J.; Dominguez, H.; Parajo, J. Xylooligosaccharides: Manufacture and Applications. Trend. Food Sci. Technol. 2000, 11, 387–393.
   Web of Science ®Google Scholar
• Kamiyama, Y.; Sakai, Y. Rate of Hydrolysis of Xylo-oligosaccharides in Dilute Sulfuric Acid. Carbohydr. Res. 1979, 73, 151–158.
   Web of Science ®Google Scholar
• Lloyd, T.; Wyman, C. Application of a Depolymerization Model for Predicting Thermochemical Hydrolysis of Hemicellulose. Appl. Biochem. Biotechnol. 2003, 105–108, 53–67.
   PubMed Web of Science ®Google Scholar
• Kumar, G.; Pushpa, A.; Prabha, H. A Review on Xylooligosaccharides. Int. Res. J. Pharm. 2012, 3, 71–74.
   Google Scholar
• Sims, R.; Mabee, W.; Saddler, J.; Taylor, M. An Overview of Second-Generation Biofuel Technologies. Bioresour. Technol. 2010, 101, 1570–1580.
   PubMed Web of Science ®Google Scholar
• Kumar, R.; Wyman, C. The Impact of Dilute Sulfuric Acid on the Selectivity of Xylooligomer Depolymerization to Monomers. Carbohydr. Res. 2008, 343, 290–300.
   PubMed Web of Science ®Google Scholar
• Kim, Y.; Kreke, T.; Ladisch, M. Reaction Mechanisms and Kinetics of Xylooligosaccharides Hydrolysis by Dicarboxylic Acids. AIChE J. 2013, 59, 188–199.
   Web of Science ®Google Scholar
• Qing, Q.; Yang, B.; Wyman, C. Xylooligomers are Strong Inhibitors of Cellulose Hydrolysis by Enzymes. Bioresour. Technol. 2010, 101, 9624–9630.
   PubMed Web of Science ®Google Scholar
• Swennen, K.; Courtin, C.; Bruggen, B.; Vandecasteele, C.; Delcour, J. Ultrafiltration and Ethanol Precipitation for Isolation of Arabinoxylooligosaccharides with Different Structures. Carbohydr. Polym. 2005, 62, 283–292.
   Web of Science ®Google Scholar
• Yuan, Q.; Zhang, H.; Qian, Z.; Yang, J. Pilot-Plant Production of Xylo-Oligosaccharides from Corncob by Steaming, Enzymatic Hydrolysis and Nanofiltration. J. Chem. Technol. Biotechnol. 2004, 79, 1073–1079.
   Web of Science ®Google Scholar
• Kabel, M., Schols, H., Voragen, A. Complex Xylo-Oligosaccharides Identified from Hydrothermally Treated Eucalyptus Wood and Brewery’s Spent Grain. Carbohydr. Polym. 2002, 50, 191–200.
   Web of Science ®Google Scholar
• Katapodis, P.;Vardakou, M.; Kalogeris, E.; Kekos, D.; Macris, B.; Christakopoulos, P. Enzymic Production of a Feruloylated Oligosaccharide with Antioxidant Activity from Wheat Flour Arabinoxylan. Eur. J. Nutr. 2003, 42, 55–60.
   PubMed Web of Science ®Google Scholar
• Ohsaki, S.; Tamura, M.; Yamaura, T. Method for Purification of Saccharide. U.S. Patent 6,548,662, April 15, 2003.
   Google Scholar
• Lau, C.; Bunnell, K.; Clausen, E.; Thoma, G.; Lay, J. O.; Gidden, J.; Carrier, D. J. Separation and Purification of Xylose Oligomers Using Centrifugal Partition Chromatography. J. Ind. Microbiol. Biotechnol. 2011, 38, 363–370.
   PubMed Web of Science ®Google Scholar
• Lau, C.; Clausen, E.; Lay, J. O.; Gidden, J.; Carrier, D. J. Separation of Xylose Oligomers Using Centrifugal Partition Chromatography with a Butanol-Methanol-Water System. J. Ind. Microbiol. Biotechnol. 2013, 40, 51–62.
   PubMed Web of Science ®Google Scholar
• Ito, Y. Golden Rules and Pitfalls in Selecting Optimum Conditions for High-Speed Counter-Current Chromatography. J. Chromatogr, A 2005, 1065, 145–168.
   PubMed Web of Science ®Google Scholar
• Cazes, J.; Nonogaki, K. Centrifugal Partition Chromatography. Am. Lab. (Southport, CT) 1987, 19, 126–132.
   Web of Science ®Google Scholar
• Chevolot, L.; Jouault, S.; Foucault, A.; Ratiskol, J.; Sinquin, C. Preliminary Report on Fractionation of Fucans by Ion-Exchange Displacement Centrifugal Partition Chromatography. J. Chromatogr. B 1998, 706, 43–54.
   PubMed Web of Science ®Google Scholar
• Schmer, M.; Vogel, K.; Mitchell, R.; Perrin, R. Net Energy of Cellulosic Ethanol from Switchgrass. Proc. Natl. Acad. Sci. 2008, 105, 464–469.
   PubMed Web of Science ®Google Scholar
• Bunnell, K.; Rich, A.; Luckett, C.; Wang, Y.; Martin, E.; Carrier, D. J. Plant Maturity Effects on the Physicochemical Properties and Dilute Acid Hydrolysis of Switchgrass (Panicum virgatum, L.) Hemicelluloses. Sustainable Chem. Eng. 2013, 1, 649–654.
   Google Scholar
• Engelberth, A.; Clausen, E.; Carrier, D. J. Comparison of Pressurized Hot Water and Ultrasonic Extraction Methods for Recovery of Ginseng Saponins from American Ginseng (Panax) Followed by Purification Using FCPC with HPLC Verification. Sep. Purif. Technol. 2010, 72, 1–6.
   Web of Science ®Google Scholar
• Sluiter, A.; Hames, B.; Ruiz, R.; Scarlata, C.; Sluiter, J.; Templeton, D.; Crocker, D. D. Determination of structrual carbohydrates and lignin in biomass. Technical Report NREL/TP- 510–42618. National Renewable Energy Laboratory: Golden, CO, 2008; http://www.nrel.gov/biomass/pdfs/42618.pdf.
   Google Scholar
• Bartley, L.; Peck, M.; Kim, S.; Ebert, B.; Manisseri, C.; Chiniquy, D.; Sykes, R.; Gao, L.; Rautengarten, C.; Vega-Sánchez, M.; Benke, P.; Canlas, P.; Cao, P.; Brewer, S.; Lin, F.; Smith, W.; Zhang, X.; Keasling, J.; Jentoff, R.; Foster, S.; Zhou, J.; Ziebell, A.; An, G.; Scheller, H.; Ronald, P. Overexpression of a BAHD Acyltransferase, OsAt10, Alters Rice Cell Wall Hydroxycinnamic Acid Content and Saccharification. Plant Physiol. 2013, 161, 1615–1633.
   Google Scholar