Simple UHPLC-DAD Method for the Direct Determination of Donepezil in Cerebrospinal Fluid

References

• Kafkala, S.; Matthaiou, S.; Alexaki, P.; Abatzis, M.; Bartzeliotis, A.; Katsiabani, M. New Gradient High-performance Liquid Chromatography Method for Determination of Donepezil Hydrochloride Assay and Impurities Content in Oral Pharmaceutical Formulation. J. Chromatogr. A 2008, 1189, 392–397.
   PubMed Web of Science ®Google Scholar
• Parnetti, L.; Amici, S.; Lanari, A.; Romani, C.; Antognelli, C.; Andreasen, N.; Minthon, L.; Davidsson, P.; Pottel, H.; Blennow, K.; Gallai, V. Cerebrospinal Fluid Levels of Biomarkers and Activity of Acetylcholinesterase (AChE) and Butyrylcholinesterase in AD Patients Before and After Treatment with Different AChE Inhibitors. Neurol. Sci. 2002, 23, 895–896.
   Web of Science ®Google Scholar
• Parnetti, L.; Chiasserini, D.; Andreasson, U.; Ohlson, M.; Hüls, C.; Zetterberg, H.; Minthon, L.; Wallin, A. K.; Andreasen, N.; Talesa, V. N.; Blennow, K. Changes in CSF Acetyl- and Butyrylcholinesterase Activity After Long-term Treatment with AChE Inhibitors in Alzheimer’s Disease. Acta Neurol. Scandinavica 2011, 124, 122–129.
   PubMed Web of Science ®Google Scholar
• Darreh-Shori, T.; Meurling, L.; Pettersson, T.; Hugosson, K.; Hellström-Lindahl, E.; Andreasen, N.; Minthon, L.; Nordberg, A. Changes in the Activity and Protein Levels of CSF Acetylcholinesterases in Relation to Cognitive Function of Patients with Mild Alzheimer’s Disease Following Chronic Donepezil Treatment. J. Neural Transmission 2006, 113, 1791–1801.
   PubMed Web of Science ®Google Scholar
• Lu, Y. H.; Wen, H. M.; Li, W.; Chi, Y. M.; Zhang, Z. X. Determination of Donepezil in human Plasma by HPLC-MS. Yao Xue Xue Bao 2003, 38, 203–206.
   PubMedGoogle Scholar
• Lu, Y.; Wen, H.; Li, W.; Chi, Y.; Zhang, Z. Determination of donepezil hydrochloride (E2020) in Plasma by Liquid Chromatography-mass Spectrometry and Its Application to Pharmacokinetic Studies in Healthy, Young, Chinese Subjects. J. Chromatogr. Sci. 2004, 42, 234–237.
   PubMed Web of Science ®Google Scholar
• Yu, Q.; Xiang, J.; Shi, L. Z.; Liang, M. Z.; Qin, Y. P.; Nan, F. Determination of Donepezil Enantiomer in Human Plasma by Normal-HPLC-MS/MS. Sichuan Da Xue Xue Bao Yi Xue Ban 2012, 43, 779–781.
   PubMedGoogle Scholar
• Apostolou, C.; Dotsikas, Y.; Kousolos, C.; Loukas, Y. L. Quantitative Determination of Donepezil in Human Plasma by Liquid Chromatography/Tandem Mass Spectrometry Employing an Automated Liquid-liquid Extraction Based on 96-well Format Plates: Application to a Bioequivalence Study. J. Chromatogr. B 2007, 848, 239–244.
   PubMed Web of Science ®Google Scholar
• Xie, Z.; Liao, Q.; Xu, X.; Yao, M.; Wan, J.; Liu, D. Rapid and Sensitive Determination of Donepezil in Human Plasma by Liquid Chromatography/Tandem Mass Spectrometry: Application to a Pharmacokinetic Study. Rapid Commun. Mass Spectrom. 2006, 20, 3193–3198.
   PubMed Web of Science ®Google Scholar
• Pilli, N. R.; Inamadugu, J. K.; Kondreddy, N.; Karra, V. K.; Damaramadugu, R.; Rao, J. V. A Rapid and Sensitive LC-MS/MS Method for Quantification of Donepezil and Its Active Metabolite, 6-o-Desmethyldonepezil in Human Plasma and Its Pharmacokinetic Application. Biomed. Chromatogr. 2011, 25, 943–951.
   PubMed Web of Science ®Google Scholar
• Park, E. J.; Lee, H. W.; Ji, H. Y.; Kim, H. Y.; Lee, M. H.; Park, E. S.; Lee, K. C.; Lee, H. S. Hydrophilic Interaction Chromatography-tandem Mass Spectrometry of Donepezil in Human Plasma: Application to a Pharmacokinetic Study of Donepezil in Volunteers. Arch. Pharm. Res. 2008, 31, 1205–1211.
   PubMed Web of Science ®Google Scholar
• Koeber, R.; Kluenemann, H. H.; Waimer, R.; Koestlbacher, A.; Wittmann, M.; Brandl, R.; Doerfelt, A.; Jahner, T.; Melchner, D.; Haen, E. Implementation of a Cost-effective HPLC/UV-Approach for Medical Routine Quantification of Donepezil in Human Serum. J. Chromatogr. B 2012, 881–882, 1–11.
   PubMed Web of Science ®Google Scholar
• Yasui-Furukori, N.; Furuya, R.; Takahata, T.; Tateishi, T. Determination of Donepezil, an Acetylcholinesterase Inhibitor, in Human Plasma by High-performance Liquid Chromatography with Ultraviolet Absorbance Detection. J. Chromatogr. B 2002, 768, 261–265.
   PubMed Web of Science ®Google Scholar
• Abonassif, M. A.; Hefnawy, M. M.; Kassem, M. G.; Mostafa, G. A. Determination of Donepezil Hydrochloride in Human Plasma and Pharmaceutical Formulations by HPLC with Fluorescence Detection. Acta. Pharm. 2011, 61, 403–413.
   PubMed Web of Science ®Google Scholar
• Nakashima, K.; Itoh, K.; Kono, M.; Nakashima, M. N.; Wada, M. Determination of Donepezil Hydrochloride in Human and Rat Plasma, Blood and Brain Microdialysates by HPLC with a Short C30 Column. J. Pharm. Biomed. Anal. 2006, 41, 201–206.
   PubMed Web of Science ®Google Scholar
• Radwan, M. A.; Abdine, H. H.; Al-Quadeb, B. T.; Aboul-Enein, H. Y.; Nakashima, K. Stereoselective HPLC Assay of Donepezil Enantiomers with UV Detection and Its Application to Pharmacokinetics in Rats. J. Chromatogr. B 2006, 830, 114–119.
   PubMed Web of Science ®Google Scholar
• Noetzli, M.; Ansermot, N.; Dobrinas, M.; Eap, C. B. Simultaneous Determination of Antidementia Drugs in Human Plasma: Procedure Transfer from HPLC-MS to UPLC-MS/MS. J. Pharm. Biomed. Anal. 2012, 64–65, 16–25.
   PubMed Web of Science ®Google Scholar
• García-Ayllón, M. S.; Silveyra, M. X.; Andreasen, N.; Brimijoin, S.; Blennow, K.; Sáez-Valero, J. Cerebrospinal Fluid Acetylcholinesterase Changes After Treatment with Donepezil in Patients with Alzheimer’s Disease. J. Neurochem. 2007, 01, 1701–1711.
   Web of Science ®Google Scholar
• Nordberg, A.; Darreh-Shori, T.; Peskind, E.; Soininen, H.; Mousavi, M.; Eagle, G.; Lane, R. Different Cholinesterase Inhibitor Effects on CSF Cholinesterases in Alzheimer Patients. Curr. Alzheimer Res. 2009, 6, 4–14.
   PubMed Web of Science ®Google Scholar
• Guidance for Industry. Bioanalytical Method Validation. FDA, September 2013. www.fda.gov/downloads/Drugs/Guidances/ucm070107.pdf (accessed Mar, 2014)
   Google Scholar