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Original Articles

Comparison of the limits of detection and quantification of estradiol hemihydrate determined by thin-layer chromatography using different chromatographic conditions

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References

  • Yilmaz, B.; Kadioglu, Y. Quantitation of 17 β-estradiol in Rabbit Plasma by High-performance Liquid Chromatography with Fluorescence Detection. J. Liq. Chromatogr. & Rel. Technol. 2013, 36, 1126–1137.
  • Havlíková, L.; Nováková, L.; Matysová, L.; Sícha, J.; Solich, P. Determination of Estradiol and its Degradation Products by Liquid Chromatography. J. Chromatogr. A. 2006, 1119, 216–223.
  • Nováková, L.; Solich, P.; Matysová, L.; Sícha, J. HPLC Determination of Estradiol, its Degradation Product, and Preservatives in New Topical Formulation Estrogel HBF. Anal. Bioanal. Chem. 2004, 379, 781–787.
  • Szarka, S.; Nguyen, V.; Prokai, L.; Prokai-Tatrai, K. Separation of Dansylated 17β-Estradiol, 17α-estradiol, and Estrone on a Single HPLC Column for Simultaneous Quantitation by LC-MS/MS. Anal. Bioanal. Chem. 2013, 405, 3399–3406.
  • Li, H.; Jiang, Y.; Liu, Y. Enrichment and Determination of Trace Estradiol in Environmental Water Samples by Hollow-Fiber Liquid-Phase Microextraction Prior to HPLC. J. Chromatogr. Sci. 2011, 49, 676–682.
  • Bhawani, S. A.; Sulalman, O.; Hashim, R.; Mohamad, M. N. Thin-layer Chromatographic Analysis of Steroids: A Review. Trop. J. Pharm. Res. 2010, 9, 301–313.
  • ICH. ICH Harmonized Tripartite Guideline: Validation of Analytical Procedures: Text and Methodology Q2(R1); ICH: Geneva, Switzerland, 2005; http://www.ich.org/fileadmin/Public_Web_Site/ICH_Products/Guidelines/Quality/Q2_R1/Step4/Q2_R1__Guideline.pdf
  • Brynn Hibbert, D. Method Validation of Modern Analytical Techniques In Validation in Chemical Measurement; Bievre, P., Gűnzler, H., Eds.; Springer-Verlag, Heidelberg, Berlin, 2005, pp. 134–138.
  • Ferenczi-Fodor, K.; Renger, B.; Végh, Z. The Frustrated Reviewer – Recurrent Failures in Manuscripts Describing Validation of Quantitative TLC/HPTLC Procedures for Analysis of Pharmaceuticals. J. Planar Chromatogr. – Mod. TLC. 2010, 23, 173–179.
  • Nagy-Turák, A.; Végh, Z.; Ferenczi-Fodor, K. Validation of the Quantitative Planar Chromatographic Analysis of Drug Substances. III. Robustness Testing in OPLC. J. Planar Chromatogr. – Mod. TLC. 1995, 8, 188–193.
  • Ferenczi-Fodor, K.; Nagy-Turák, A.; Végh, Z. Validation and Monitoring of Quantitative Thin Layer Chromatographic Purity Tests for Bulk Drug Substances. J. Planar Chromatogr. – Mod. TLC. 1995, 8, 349–356.
  • Konieczka, P.; Namieśnik, J. Eds. Validation of Analytical Procedures (in Polish). In The Estimation and Quality Control of Analytical Measurements; WNT: Warsaw, 2007; 225–227 pp., 269–289 pp.
  • Dołowy, M.; Maryszczak, J.; Pyka A. Comparison of the Detection and Quantitative Limits of Hydrocortisone Acetate in Different Chromatographic Conditions in TLC. J. Liq. Chromatogr. & Rel. Technol. 2014, 37, 2929–2941.
  • Pyka, A.; Klimczok, W.; Gurak, D. Evaluation of Visualizing Reagents for Estradiol on Thin Layer by Densitometric Method. J. Liq. Chromatogr. & Rel. Technol. 2002, 25, 1483–1495.
  • Dołowy, M.; Kurowska, A.; Pyka, A. Development and Validation of a TLC-densitometry Method for Assay of Estradiol Hemihydrate in Tablets. Curr. Pharm. Anal. 2014, 10, 112–121.

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