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Original Articles

The effect of chromatographic conditions on the separation of selected alkaloids on CN-silica layers

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References

  • Gupta, M. M.; Srivastava, A.; Tripathi, A. K.; Misra, H.; Verma, R. K. Use of HPTLC, HPLC, and Densitometry for Qualitative Separation of Indole Alkaloids from Rauvolfia serpentina Roots. J. Planar Chromatogr. 2006, 19, 282–287.
  • Wongpan, B.; Vallisuta, O.; Ruangwises, N.; Mitrevej, A. TLC–Densitometric Method for the Quantification of Crebanine in Stephania venosa (BI) Spreng. J. Planar Chromatogr. 2012, 25, 283–289.
  • Marutoiu, C.; Gogoasa, I.; Oprean, I.; Marutoiu, O.-F.; Moise, M.-I.; Tigae, C.; Rada, M. Separation and Identification of Piperine and Chavicine in Black Pepper by TLC and GC–MS. J. Planar Chromatogr. 2006, 19, 250–252.
  • De, S.; Nariya, P.; Jirankalgikar, N. A Rapid Validated High-performance Thin-layer Chromatographic–Densitometric Method for the Simultaneous Estimation of Different Chemical-Nature Compounds Piperine and Gallic Acid in Pharmaceutical Dosage Forms. J. Planar Chromatogr. 2013, 26, 325–330.
  • Rajopadhye, A. A.; Upadhye, A. S.; Mujumdar, A. M. HPTLC Method for Analysis of Piperine in Fruits of Piper Species. J. Planar Chromatogr. 2011, 24, 57–59.
  • Gopalakrishnana, R.; Shankar, B. Multiple Shoot Cultures of Ophiorrhiza rugosa var. decumbens Deb and Mondal – A Viable Renewable Source for the Continuous Production of Bioactive Camptotheca Alkaloids Apart from Stems of the Parent Plant of Nothapodytes foetida (Wight) Sleumer. Phytomedicine 2014, 21, 383–389.
  • Na, R.; Jiajia, L.; Dongliang, Y.; Yingzi, P.; Juan, H.; Xiong, L.; Nana, Z.; Jing, Z.; Yitian, L. Indentification of Vincamine Indole Alkaloids Producing Endophytic Fungi Isolated from Nerium indicum, Apocynaceae. Microbiol. Res. 2016, 192, 114–121.
  • do Prado Ribeiro, L.; Vendramim, J. D.; Bicalho, K. U.; dos Santos Andrade, M.; Fernandes, J. B.; de Andrade Moral, R.; Demétrio, C. G. B. Annona mucosa Jacq. (Annonaceae): A Promising Source of Bioactive Compounds Against Sitophilus zeamais Mots. (Coleoptera: Curculionidae). J. Stored Prod. Res. 2013, 55, 6e14.
  • Ghildiyal, S.; Gautam, M. K.; Joshi, V. K.; Goel, R. K. Pharmacognostical Study of Hedychium spicatum (Ham-Ex-Smith) Rhizome. Asian Pac. J. Trop. Dis. 2012, 2, S148–S153.
  • Shikanga, E. A.; Vermaak, I.; Viljoen, A. M. An HPTLC–Densitometry Method for the Quantification of Pharmacologically Active Alkaloids in Sceletium tortuosum Raw Material and Products. J. Planar Chromatogr. 2012, 25, 283–289.
  • Mallavadhani, U. V.; Sahu, G. HPTLC Method for Quantitative Evaluation of Preparations Containing Indian ‘Elixir’ Plant, Tinospora cordifolia, Using Jatrorrhizine as Marker. J. Planar Chromatogr. 2009, 22, 439–443.
  • Paillat, L.; Périchet, C.; Lavoine, S.; Meierhenrich, U.; Fernandez, X. Validated High-Performance Thin-layer Chromatography Method for the Determination of Nicotine in Tobacco (Nicotiana tabacum L.) Extracts. J. Planar Chromatogr. 2012, 25, 23–29.
  • Skarkova, J.; Ostry, V.; Ruprich, J. Instrumental HPTLC Determination of α-Solanine and α-Chaconine in Peeled Potato Tubers. J. Planar Chromatogr. 2008, 21, 113–117.
  • Pozzi, F.; Shibayama, N.; Leonaa, M.; Lombardi, J. R. TLC-SERS Study of Syrian Rue (Peganum harmala) and Its Main Alkaloid Constituents. J. Raman Spectrosc. 2013, 44, 102–107.
  • Berkov, S.; Bastida, J.; Nikolova, M.; Viladomat, F.; Codina, C. Rapid TLC/GC–MS Identification of Acetylcholinesterase Inhibitors in Alkaloid Extracts. Phytochem. Anal. 2008, 19, 411–419.
  • Jaremicz, Z.; Luczkiewicz, M.; Kisiel, M.; Zárate, R.; El Jaber-Vazdekis, N.; Migas, P. Multi-development–HPTLC Method for Quantitation of Hyoscyamine, Scopolamine and their Biosynthetic Precursors in Selected Solanaceae Plants Grown in Natural Conditions and as In Vitro Culture. Phytochem. Anal. 2014, 25, 29–35.
  • El-Hawary, S. S.; Mohammed, R.; AbouZid, S. F.; Bakeer, W.; Ebel, R.; Sayed, A. M.; Rateb, M. E. Solamargine Production by a Fungal Endophyte of Solanum nigrum. J. Appl. Microbiol. 2016, 120, 900–911.
  • Pallant, C. A.; Cromarty, A. D.; Steenkamp, V. Effect of an Alkaloidal Fraction of Tabernaemontana elegans (Stapf.) on Selected Micro-organisms. J. Ethnopharmacol. 2012, 140, 398–404.
  • Shawky, E. Multivariate Analyses of NP-TLC Chromatographic Retention Data for Grouping of Structurally-related Plant Secondary Metabolites. J. Chromatogr. B 2016, 1029, 10–15.
  • Liu, W.; Wang, Y.; He, D.-d.; Li, S.-p.; Zhu Y.-d.; Jiang, B.; Cheng, X.-m.; Wang, Z.-t.; Wang, C.-h. Antitussive, Expectorant, and Bronchodilating Effects of Quinazoline Alkaloids (±)-Vasicine, Deoxyvasicine, and (±)-Vasicinone from Aerial Parts of Peganum harmala L. Phytomedicine 2015, 22, 1088–1095.
  • Musharraf, S. G.; Shoaib, M.; Najam-ul-Haq. TLC–Densitometric Method Development and Validation for the Quantification of Nicotine in Tobacco Smoked, Sniffing, Dipping, and Chewing Products. J. Planar Chromatogr. 2011, 24, 381–387.
  • Singh, A.; Alvi, N. I. High-performance Thin-layer Chromatographic Quantification of Yohimbine in the Stem Bark of Pausinystalia yohimbe. J. Planar Chromatogr. 2011, 24, 253–256.
  • Kumbhalkar, B. B.; Rajopadhye, A. A.; Upadhye, A. S. Development and Validation of HPTLC–Densitometric Method for Estimation of Trigonelline in Leaves of Abrus precatorius L. and Its Formulation. Acta Chromatogr. 2012, 24, 511–518.
  • Pandey, D. K.; Radha; Dey, A. A Validated and Densitometric HPTLC Method for the Simultaneous Quantification of Reserpine and Ajmalicine in Rauvolfia serpentina and Rauvolfia tetraphylla. Rev. Bras. Farmacogn. 2016, 26, 553–557. doi:10.1016/j.bjp.2016.04.002
  • Mehta, F. A.; Patel, B. G.; Pandya, S. S.; Ahir, K. B. High-performance Thin-layer Chromatographic Analysis of Betaine in Alcohol Extracts of Achyranthes aspera L. J. Planar Chromatogr. 2011, 24, 136–139.
  • Shakeel, S.; Gul, S.; Zahoor, A.; Khan, S. S.; Sheikh, Z. A.; Naveed, S.; Usmanghani, K. Standardization of Biomarkers Gallic Acid and Berberine in Polyherbal Formulation Entoban Capsules by High-performance Thin-layer Chromatography–Densitometry. J. Planar Chromatogr. 2015, 28, 386–390.
  • Satija, S.; Malik, S.; Garg, M. Development of a New, Rapid, and Sensitive Validated High-performance Thin-layer Chromatographic Method for the Estimation of Berberine in Tinospora cordifolia. J. Planar Chromatogr. 2016, 29, 209–215.
  • Mirakor, V.; Vaidya, V.; Menon, S.; Champanerker, P.; Laud, A. HPTLC Method for Determination of Colchicine in a Pharmaceutical Formulation. J. Planar Chromatogr. 2008, 21, 187–189.
  • Shariatgorji, M.; Spacil, Z.; Maddalo, G.; Cardenas, L. B.; Ilag, L. L. Matrix-free Thin-layer Chromatography/Laser Desorption Ionization Mass Spectrometry for Facile Separation and Identification of Medicinal Alkaloids. Rapid Commun. Mass Spectrom. 2009, 23, 3655–3660.
  • Pan, F.; Hou, K.; Gao, F.; Hu, B.; Chen, Q.; Wu, W. Peimisine and Peiminine Production by Endophytic Fungus Fusarium sp. Isolated from Fritillaria unibracteata Var. wabensis. Phytomedicine 2014, 21, 1104–1109.
  • McGaw, L. J.; Steenkamp, V.; Eloff, J. N. Evaluation of Athrixia Bush Tea for Cytotoxicity, Antioxidant Activity, Caffeine Content and Presence of Pyrrolizidine Alkaloids. J. Ethnopharmacol. 2007, 110, 16–22.
  • SatheeshKumar, N.; Mukherjee, P. K.; Bhadra, S.; Saha, B. P. Acetylcholinesterase Enzyme Inhibitory Potential of Standardized Extract of Trigonella foenum graecum L and Its Constituents. Phytomedicine 2010, 17, 292–295.
  • Jin, W.; Zhang, Y.; Mei, S.; Xiong, Y.; Yang, Q.; Yu, L. Identification of Lepidium meyenii (Walp.) Based on Spectra and Chromatographic Characteristics of Its Principal Functional Ingredients. J. Sci. Food Agric. 2007, 87, 2251–2258.
  • Oellig, C.; Melde, T. Screening for Total Ergot Alkaloids in Rye Flour by Planar Solid Phase Extraction–Fluorescence Detection and Mass Spectrometry. J. Chromatogr. A 2016, 1441, 126–133.
  • Raj, D.; Kokotkiewicz, A.; Łuczkiewicz, M.; Densitometric HPTLC Analysis of Indolizidine Alkaloids in the Herb and In-vitro Cultures of Securinega suffruticosa. J. Planar Chromatogr. 2009, 22, 371–376.
  • Glensk, M.; Żbikowska, B.; Cisowski, W. TLC Separation of Uncaria tomentosa Alkaloids on Chemically Modified Stationary Phases. J. Planar Chromatogr. 2004, 17, 14–17.
  • Łuczkiewicz, M.; Migas, P.; Kokotkiewicz, A.; Walijewska, M.; Cisowski, W. Two-Dimensional TLC with Adsorbent Gradient for Separation of Quinolizidine Alkaloids in the Herb and In-Vitro Cultures of Several Genista Species. J. Planar Chromatogr. 2004, 17, 89–94.
  • Migas, P.; Heyka, M.; Pobłocka-Olech, L.; Krauze-Baranowska, M.; BMD-TLC – The Useful Technique for Quantitative Analysis of Chelidonine, Chelerithrine and Berberine in Herbal Drugs. J. Planar Chromatogr. 2012, 25, 439–444.
  • Petruczynik, A.; Karczmarz, A.; Waksmundzka-Hajnos, M. Effect of Multiple Development Techniques on the Chromatographic Parameters and Separation Selectivity of Some Alkaloids on C18 and CN-Silica Layers. J. Planar Chromatogr. 2014, 27, 333–339.

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