173
Views
4
CrossRef citations to date
0
Altmetric
Original Articles

Comparison of photodiode array, evaporative light scattering, and single-quadrupole mass spectrometric detection methods for the UPLC analysis of pyrolysis liquids

, &

References

  • Saidur, R.; Abdelaziz, E. A.; Demirbas, A.; Hossain, M. S.; Mekhilef, S. A Review on Biomass as a Fuel for Boilers. Renewable Sustainable Energy Rev. 2011, 15(5), 2262–2289.
  • Bai, X.; Brown, R. C. Modeling the Physiochemistry of Levoglucosan during Cellulose Pyrolysis. J. Anal. Appl. Pyrolysis 2014, 105, 363–368.
  • Lian, J.; Garcia-Perez, M.; Chen, S. Fermentation of Levoglucosan with Oleaginous Yeasts for Lipid Production. Bioresour. Technol. 2013, 133, 183–189.
  • Linger, J. G.; Hobdey, S. E.; Franden, M. A.; Fulk, E. M.; Beckham, G. T. Conversion of Levoglucosan and Cellobiosan by Pseudomonas putida KT2440. Metab. Eng. Commun. 2016, 3, 24–29.
  • Černý, M.; Staněk Jr, J. 1,6-Anhydro Derivatives of Aldohexoses. In Advances in Carbohydrate Chemistry and Biochemistry; Tipson, R. S., Derek, H., Eds.; Academic Press: USA, 1977; Vol. 34, 23–177 pp.
  • Sviridov, A. F.; Borodkin, V. S.; Ermolenko, M. S.; Yashunsky, D. V.; Kochetkov, N. K. Stereocontrolled Synthesis of Erythronolides A and B in a (C5–C9) + (C3–C4) + (C1–C2) + (C11–C13) sequence from 1,6-anhydro-β-D-glycopyranose (levoglucosan). Part 1. Synthesis of C1–C10 and C11–C13 segments. Tetrahedron 1991, 47(12–13), 2291–2316.
  • Michailof, C.; Sfetsas, T.; Stefanidis, S.; Kalogiannis, K.; Theodoridis, G.; Lappas, A. Quantitative and Qualitative Analysis of Hemicellulose, Cellulose and Lignin Bio-oils by Comprehensive Two-dimensional Gas Chromatography with Time-of-flight Mass Spectrometry. J. Chromatogr. A 2014, 1369, 147–160.
  • Schneider, J. K.; da Cunha, M. E.; dos Santos, A. L.; Maciel, G. P. S.; Brasil, M. C.; Pinho, A. R.; Mendes, F. L.; Jacques, R. A.; Caramão, E. B. Comprehensive Two Dimensional Gas Chromatography with Fast-quadrupole Mass Spectrometry Detector Analysis of Polar Compounds Extracted from the Bio-oil from the Pyrolysis of Sawdust. J. Chromatogr. A 2014, 1356, 236–240.
  • Sfetsas, T.; Michailof, C.; Lappas, A.; Li, Q.; Kneale, B. Qualitative and Quantitative Analysis of Pyrolysis Oil by Gas Chromatography with Flame Ionization Detection and Comprehensive Two-dimensional Gas Chromatography with Time-of-flight Mass Spectrometry. J. Chromatogr. A 2011, 1218(21), 3317–3325.
  • Bogolitsyna, A.; Becker, M.; Dupont, A.-L.; Borgards, A.; Rosenau, T.; Potthast, A. Determination of Carbohydrate- and Lignin-derived Components in Complex Effluents from Cellulose Processing by Capillary Electrophoresis with Electrospray Ionization–Mass Spectrometric Detection. J. Chromatogr. A 2011, 1218(47), 8561–8566.
  • Castellví Barnés, M.; Lange, J. P.; van Rossum, G.; Kersten, S. R. A. A New Approach for Bio-oil Characterization based on Gel Permeation Chromatography Preparative Fractionation. J. Anal. Appl. Pyrolysis 2015, 113, 444–453.
  • Tessini, C.; Vega, M.; Müller, N.; Bustamante, L.; von Baer, D.; Berg, A.; Mardones, C. High Performance Thin Layer Chromatography Determination of Cellobiosan and Levoglucosan in Bio-oil Obtained by Fast Pyrolysis of Sawdust. J. Chromatogr. A 2011, 1218(24), 3811–3815.
  • Djokic, M. R.; Dijkmans, T.; Yildiz, G.; Prins, W.; Van Geem, K. M. Quantitative Analysis of Crude and Stabilized Bio-oils by Comprehensive Two-dimensional Gas-Chromatography. J. Chromatogr. A 2012, 1257, 131–140.
  • Zhurinsh, A.; Dobele, G.; Rizhikovs, J.; Zandersons, J.; Grigus, K. Effect of Pre-treatment Conditions on the Analytical Pyrolysis Products from Birch Wood Lignocellulose. J. Anal. Appl. Pyrolysis 2013, 103, 227–231.
  • Reddy Kannapu, H. P.; Mullen, C. A.; Elkasabi, Y.; Boateng, A. A. Catalytic Transfer Hydrogenation for Stabilization of Bio-oil Oxygenates: Reduction of p-cresol and Furfural over Bimetallic Ni–Cu Catalysts using Isopropanol. Fuel Process. Technol. 2015, 137, 220–228.
  • Wang, Z.; Wang, X.; Jiang, J.; Fu, Y.; Qin, M. Fractionation and Characterization of Saccharides and Lignin Components in Wood Prehydrolysis Liquor from Dissolving Pulp Production. Carbohydr. Polym. 2015, 126, 185–191.
  • Jarboe, L. R.; Wen, Z.; Choi, D.; Brown, R. C. Hybrid Thermochemical Processing: Fermentation of Pyrolysis-derived Bio-oil. Appl. Microbiol. Biotechnol. 2011, 91(6), 1519–1523.
  • Le Masle, A.; Angot, D.; Gouin, C.; D’Attoma, A.; Ponthus, J.; Quignard, A.; Heinisch, S. Development of On-line Comprehensive Two-dimensional Liquid Chromatography Method for the Separation of Biomass Compounds. J. Chromatogr. A 2014, 1340, 90–98.
  • Barnaba, C.; Dellacassa, E.; Nicolini, G.; Nardin, T.; Malacarne, M.; Larcher, R. Identification and Quantification of 56 Targeted Phenols in Wines, Spirits, and Vinegars by Online Solid-phase Extraction–Ultra high-performance Liquid Chromatography–Quadrupole-orbitrap Mass Spectrometry. J. Chromatogr. A 2015, 1423, 124–135.
  • ACQUITY UPLC BEH Columns. Waters Corporation: USA, 2014; pp. 1–13.
  • Olsen, B. A.; Pack, B. W. Hydrophilic Interaction Chromatography: A Guide for Practitioners. John Wiley & Sons: USA, 2012; p. 336.
  • McCabe, D.; Hudalla, C. Overcoming Challenges in Carbohydrate Separations. 2015, http://www.sepscience.com.
  • Parson, W. W. Modern Optical Spectroscopy: With Excersises and Examples for Biophysics and Biochemistry, 2nd Ed.; Springer: USA, 2011.
  • Young, C. S.; Dolan, J. W. Success with Evaporative Light-Scattering Detection. LC GC N Am, 2003, 22(2), 246–250.
  • Liu, X.; Ai, N.; Zhang, H.; Lu, M.; Ji, D.; Yu, F.; Ji, J. Quantification of Glucose, Xylose, Arabinose, Furfural, and HMF in Corncob Hydrolysate by HPLC–PDA–ELSD. Carbohydr. Res. 2012, 353, 111–114.
  • Ma, C.; Sun, Z.; Chen, C.; Zhang, L.; Zhu, S. Simultaneous Separation and Determination of Fructose, Sorbitol, Glucose and Sucrose in Fruits by HPLC–ELSD. Food Chem. 2014, 145, 784–788.
  • Kailemia, M. J.; Ruhaak, L. R.; Lebrilla, C. B.; Amster, I. J. Oligosaccharide Analysis by Mass Spectrometry: A Review of Recent Developments. Fundam. Appl. Rev. Anal. Chem. 2014, 86(1), 196–212.
  • Meile, K.; Zhurinsh, A.; Dobele, G. Characterization of the Anhydrosugar Content in Pyrolysis Liquids with Column Chromatography and Iodometric Titration. Energetika 2014, 60(3), 162–168.
  • Ren, S.; Ye, X. P.; Borole, A. P.; Kim, P.; Labbé, N. Analysis of Switchgrass-derived Bio-oil and Associated Aqueous Phase Generated in a Semi-pilot Scale Auger Pyrolyzer. J. Anal. Appl. Pyrolysis 2016, 119, 97–103.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.