397
Views
5
CrossRef citations to date
0
Altmetric
Articles

Size-exclusion and the void volume of HPLC column

&
Pages 89-98 | Received 28 Jan 2019, Accepted 28 Jan 2019, Published online: 29 Mar 2019

References

  • Rimmer, C. A.; Simmons, C. R.; Dorsey, J. G. The Measurement and Meaning of Void Volumes in Reversed-phase Liquid Chromatography. J Chromatogr A. 2002, 965, 219–232.
  • Unger, K. K.; Liapis, A. I. Adsorbents and Columns in Analytical high-performance Liquid Chromatography: A Perspective with Regard to Development and Understanding. J. Sep. Sci. 2012, 35, 1201–1212. DOI: 10.1002/jssc.201200042.
  • Guan, H.; Guiochon, G. Study of Physico-chemical Properties of Some Packing Materials: I. Measurements of the External Porosity of Packed Columns by Inverse Size-exclusion Chromatography. J. Chromatogr., A. 1996, 731, 27–40. DOI: 10.1016/0021-9673(95)01197-8.
  • Wang, M.; Mallette, J.; Parcher, J. F. Strategies for the Determination of the Volume and Composition of the Stationary Phase in Reversed-phase Liquid Chromatography. J. Chromatogr. A 2008, 1190, 1–7. DOI: 10.1016/j.chroma.2008.02.099.
  • Majors, R. E.; Carr, P. W. Glossary of liquid-Phase Separation Terms. LC-Gc. 2001, 19, 124–162.
  • Rustamov, I.; Farcas, T.; Ahmed, F.; Chan, F.; LoBrutto, R.; McNair, H.; Kazakevich, Y. V. Geometry of Chemically Modified Silica. J Chromatogr A. 2001, 913, 49–63.
  • Rafferty, J. L.; Zhang, L.; Siepmann, J. I.; Schure, M. R. Retention Mechanism in Reversed-phaseliquid Chromatography: A Molecular Perspective. Anal. Chem. 2007, 79, 6551–6558. DOI: 10.1021/ac0705115.
  • Gritti, F.; Leonardis, I.; Shock, D.; Stevenson, P.; Shalliker, A.; Guiochon, G. Performance of Columns Packed with the New Shell Particles, Kinetex-C18. J Chromatogr A. 2010, 1217, 1589–1603. DOI: 10.1016/j.chroma.2009.12.079.
  • Miyabe, K.; Kawaguchi, Y.; Guiochon, G. Kinetic Study on External Mass Transfer in High Performance Liquid Chromatography System. J. Chromatogr. A. 2010, 1217, 3053–3062. DOI: 10.1016/j.chroma.2010.02.075.
  • Gritti, F.; Leonardis, I.; Abia, J.; Guiochon, G. Physical Properties and Structure of Fine Core–shell Particles Used as Packing Materials for Chromatography: Relationships between Particle Characteristics and Column Performance. J. Chromatogr. A. 2010, 1217, 3819–3843. DOI: 10.1016/j.chroma.2010.04.026.
  • Langsi, V.; Ashu-Arrah, B.; Glennon, J. Sub-2-μm Seeded Growth Mesoporous Thin Shell Particles for High-performance Liquid Chromatography: Synthesis, Functionalisation and Characterisation. J. Chromatogr. A. 2015, 1402, 17–26. DOI: 10.1016/j.chroma.2015.04.034.
  • Fetters, L. J.; Hadjichristidis, N.; Lindner, J. S.; Mays, J. W. Molecular Weight Dependence of Hydrodynamic and Thermodynamic Properties for Well-defined Linear Polymers in Solution. J. Phys. Chem. Ref. Data 1994, 23, 620–638.
  • Matsumoto, T.; Nisioka, N.; Fujita, H. Excluded-volume Effects in Dilute Polymer Solutions. J. Polym. Sci. A-2 Polym. Phys. 1972, 10, 23. DOI: 10.1002/pol.1972.160100103.
  • Nakamura, Y.; Akasaka, K.; Katayama, K.; Norisuye, T.; Teramoto, A. Second and Third Virial Coefficients for Polyisobutylene in Cyclohexane. Macromolecules. 1992, 25, 1134. DOI: 10.1021/ma00029a020.
  • Gritti, F.; Guiochon, G. Thermodynamics of Adsorption of Binary Aqueous Organic Liquid Mixtures on a RPLC Adsorbent. J Chromatogr A 2007, 1155, 85–99. DOI: 10.1016/j.chroma.2007.04.024.
  • Handbook of Chemistry and Physics, 98th ed.; CRCpress: New York (NY), 2017.
  • Kazakevich, Y. V.; McNair, H. M. Low-energy Interactions in High-performance Liquid Chromatography. J. Chromatogr. A. 2000, 872, 49–59. DOI: 10.1016/S0021-9673(99)01206-6.
  • Giaquinto, A.; Liu, Z.; Bach, A.; Kazakevich, Y. Surface Area of Reversed-phase HPLC Columns. Anal. Chem. 2008, 80, 6358–6364. DOI: 10.1021/ac800772s.
  • Buntz, S.; Figus, M.; Liu, Z.; Kazakevich, Y. V. Excess Adsorption of Binary Aqueous Organic Mixtures on Various Reversed-phase Packing Materials. J. Chromatogr. A 2012, 1240, 104–112. DOI: 10.1016/j.chroma.2012.03.087.
  • McElwee, J.; Helmy, R.; Fadeev, A. Y. Thermal Stability of Organic Monolayers Chemically Grafted to Minerals. J. Colloid and Interface Sci. 2005, 285, 551–556. DOI: 10.1016/j.jcis.2004.12.006.
  • Chan, F.; Yeung, L. S.; LoBrutto, R.; Kazakevich, Y. V. Characterization of Phenyl-type HPLC Adsorbents. J Chromatogr A. 2005, 1069, 217–224.
  • Gritti, F.; Kazakevich, Y.; Guiochon, G. Measurement of Hold-up Volumes in Reverse-phase Liquid Chromatography: Definition and Comparison between Static and Dynamic Methods. J. Chromatogr. A. 2007, 1161, 157–169. DOI: 10.1016/j.chroma.2007.05.102.
  • Wang, M.; Mallette, J.; Parcher, J. F. Comparison of Void Volume, mobile Phase Volume and Accessible Volume Determined from Retention Data for Oligomers in Reversed-phase Liquid Chromatographic Systems. J. Chromatogr. A. 2011, 1218, 2995–3001. DOI: 10.1016/j.chroma.2011.03.037.
  • Heimenz, P.; Lodge, T. Polymer Chemistry, 2 ed.; CRC Press; Boca Raton (FL), 2007. pp. 338–339
  • Benoit, H. A Universal Calibration for Gel Permeation Chromatography. J. Polym. Sci. B Polym. Lett. 1967, 5, 753–759. DOI: 10.1002/pol.1967.110050903.
  • Kazakevich, Y.; LoBrutto R. (eds.), HPLC for Pharmaceutical Scientists; Wiley: New York (NY), 2007. p. 204.
  • Moore, J.C. Gel Permeation Chromatography. I. A New Method for Molecular Weight Distribution of High Polymers. J. of Polymer Sci. A. 1964, 2, 835–843.
  • Glöckner, G. Polymer Characterization by Liquid Chromatography. J. Chromatogr. Library. 1987, 34, Elsevier: Amsterdam, p 118.
  • Fadeev, A. Y.; Borisova, O. R.; Lisichkin, G. V. Fractality of Porous Silicas: A Comparison of Adsorption and Porosimetry Data. J. Coll. and Inter. Sci. 1996, 183, 1–5. DOI: 10.1006/jcis.1996.0511.
  • Buyanova, N. E.; Zagrafskaya, R. V.; Karnaukhov, A. P.; Shepelina, A. S. Determination of the Area Occupied by Molecules of Argon, nitrogen, and Krypton in a Monolayer. Knet. Catal. 1983, 24, 1011–1017.
  • Gregg, S. J.; Sing, K. S. W. Adsorption, Surface Area and Porosity; Academic Press: London, UK, 1982.
  • Garcia-Lopera, R.; Irurzun, I.; Abad, C.; Campos, A. Fractal Calibration in Size-exclusion Chromatography: I. An Introduction. J. Chromatogr. A. 2003, 996, 33–43. DOI: 10.1016/S0021-9673(03)00609-5.
  • Garcia, R.; Recalde, I. B.; Figueruelo, J. E.; Campos, A. Quantitative Evaluation of the Swelling and Crosslinking Degrees in Two Organic Gel Packings for SEC. Macromol. Chem. Phys. 2001, 202, 3352. DOI: 10.1002/1521-3935(20011101)202:17<3352::AID-MACP3352>3.0.CO;2-C.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.