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Journal of Liquid Chromatography & Related Technologies Volume 42, 2019 - Issue 9-10: Thin Layer Chromatography, Guest Editors: Dr. Joseph Sherma and Dr. Fred Rabel
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Articles

Experimental evaluation of solvent elution strength in reversed-phase TLC on medium polarity phases

Łukasz KomstaDepartment of Medicinal Chemistry, Faculty of Pharmacy, Medical University of Lublin, Lublin, PolandCorrespondence[email protected]
ORCID Iconhttp://orcid.org/0000-0003-2261-2692
ORCID Icon,
Robert SkibińskiDepartment of Medicinal Chemistry, Faculty of Pharmacy, Medical University of Lublin, Lublin, Poland
,
Joanna WróbelDepartment of Medicinal Chemistry, Faculty of Pharmacy, Medical University of Lublin, Lublin, Poland
,
Sebastian GadowskiDepartment of Medicinal Chemistry, Faculty of Pharmacy, Medical University of Lublin, Lublin, Poland
&
Karolina SkrzypiecDepartment of Medicinal Chemistry, Faculty of Pharmacy, Medical University of Lublin, Lublin, Poland
Pages 258-265 | Published online: 17 Apr 2019

References

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  • Snyder, L. R. Classification of the Solvent Properties of Common Liquids. J. Chromatogr. Sci. 1978, 16, 223–234. DOI: 10.1093/chromsci/16.6.223.
  • Snyder, L. R. Role of the Solvent in Liquid-Solid Chromatography. Review. Anal. Chem. 1974, 46, 1384–1393. DOI: 10.1021/ac60347a052.
  • Snee, R. D.; Marquardt, D. W. Screening Concepts and Designs for Experiments with Mixtures. Technometrics 1976, 18, 19–29. DOI: 10.2307/1267912.
  • De Juan, A.; Fonrodona, G.; Casassas, E. Solvent Classification Based on Solvatochromic Parameters: A Comparison with the Snyder Approach. Trends Anal. Chem. 1997, 16, 52–62. DOI: 10.1016/S0165-9936(96)00079-9.
  • Poole, S. K.; Poole, C. F. C.F. A Method for Estimating the Solvent Strength Parameter in Liquid-Solid Chromatography. Chromatographia 2001, 53, 162–166.
  • Komsta, Ł.; Stępkowska, B.; Skibiński, R. The Experimental Design Approach to Eluotropic Strength of 20 Solvents in Thin-Layer Chromatography on Silica Gel. J. Chromatogr. A. 2017, 1483, 138–141. DOI: 10.1016/j.chroma.2017.01.010.
  • Komsta, Ł.; Dunin, U.; Skibiński, R. Can RP-8 Plates Be Used in Normal-Phase Systems? A Chemometric Approach to Estimate the Elution Strength of Popular Solvents. J. Planar Chromatogr. 2017, 30, 401–404. DOI: 10.1556/1006.2017.30.5.9.
  • Komsta, Ł.; Skibiński, R.; Gadowski, S.; Wróbel, J.; Skrzypiec, K. Experimental Evaluation of Solvent Elution Strength in Reversed-Phase Thin-Layer Chromatography on RP2 and RP8 Plates. J. Planar Chromatogr. 2018, 31, 351–354. DOI: 10.1556/1006.2018.31.5.1.

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