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Regular Article

Rapid screening of undeclared hypoglycemics in counterfeit herbal antidiabetic products using HPTLC-MS

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References

  • Association, A. D. Diagnosis and Classification of Diabetes Mellitus. Diabetes Care 2011, 34, S62–S69. DOI: 10.2337/dc10-S062.
  • Kharroubi, A. T.; Darwish, H. M. Diabetes Mellitus: The Epidemic of the Century. World J. Diabetes 2015, 6, 850–867. DOI: 10.4239/wjd.v6.i6.850.
  • Kumar, A.; Goel, M. K.; Jain, R. B.; Khanna, P.; Chaudhary, V. India towards Diabetes Control: Key Issues. Australas. Med. J. 2013, 6, 524–531. DOI: 10.4066/AMJ.2013.1791.
  • Modak, M.; Dixit, P.; Londhe, J.; Ghaskadbi, S.; Devasagayam, T. P. A. Indian Herbs and Herbal Drugs Used for the Treatment of Diabetes. J. Clin. Biochem. Nutr. 2007, 40, 163–173. DOI: 10.3164/jcbn.40.163.
  • Salem, W. A.; Elkady, E. F.; Fouad, M. A.; Abdul-Azim Mohammad, M. Analysis of Metformin and Five Gliptins in Counterfeit Herbal Products: Designs of Experiment Screening and Optimization. J. AOAC Int. 2021, 104, 1667–1680. DOI: 10.1093/jaoacint/qsab106.
  • Priatni, S.; Ratnaningrum, D.; Kosasih, W.; Oladipo, I. C.; Lateef, A.; Kusuma, I. W. Identification of Glibenclamide in Antidiabetic Jamu by High Performance Liquid Chromatography Method : Study in Purwokerto, Indonesia. J. Phys. Conf. Ser. 2019, 1402, 055065. DOI: 10.1088/1742-6596/1402/5/055065.
  • Kumar, M.; Mandal, V.; Hemalatha, S. Detection of Metformin Hydrochloride in a Traditionally Used Indian Herbal Drug for Antidiabetic: A Case Report. Int. J. Pharma Bio Sci. 2011, 2, 307–313.
  • Kim, S. H.; Lee, J.; Yoon, T.; Choi, J.; Choi, D.; Kim, D.; Kwon, S. W. Simultaneous Determination of Anti-Diabetes/anti-Obesity Drugs by LC/PDA, and Targeted Analysis of Sibutramine Analog in Dietary Supplements by LC/MS/MS. Biomed. Chromatogr. 2009, 23, 1259–1265. DOI: 10.1002/bmc.1248.
  • Kim, N. S.; Kim, K. Y.; Yoo, G. J.; Lee, J. H.; Park, H. N.; Park, S.; Baek, S. Y. Determination of 26 Anti-Diabetic Compounds in Dietary Supplements Using a Validated UPLC Method. Food Addit. Contam. Part A Chem. Anal. Control Expo Risk Assess. 2018, 35, 387–394. DOI: 10.1080/19440049.2017.1332429.
  • Wu, X.; Zhu, B.; Lu, L.; Huang, W.; Pang, D. Optimization of a Solid Phase Extraction and Hydrophilic Interaction Liquid Chromatography – Tandem Mass Spectrometry Method for the Determination of Metformin in Dietary Supplements and Herbal Medicines. Food Chem. 2012, 133, 482–488. DOI: 10.1016/j.foodchem.2012.01.005.
  • Elkady, E. F.; El-Zaher, A. A.; Elwy, H. M.; Saleh, M. A. Validated Liquid Chromatographic Method for Simultaneous Determination of Metformin, Pioglitazone, Sitagliptin, Repaglinide, Glibenclamide and Gliclazide – Application for Counterfeit Drug Analysis. J. Anal. Bioanal. Tech. 2015, S13, 007. DOI: 10.4172/2155-9872.S13-007.
  • Jin, P.; Xu, S.; Xu, W.; He, X.; Kuang, Y.; Hu, X. Screening and Quantification of Fourteen Synthetic Antidiabetic Adulterants in Herbal Pharmaceuticals and Health Foods by HPLC and Confirmation by LC-Q-TOF-MS/MS. Food Addit. Contam. Part A Chem. Anal. Control Expo Risk Assess. 2020, 37, 11–18. DOI: 10.1080/19440049.2019.1675910.
  • Zhou, C.; Tang, B.; Xi, C.; Zhang, L.; Wang, G.; Xi, J.; Chen, Z. Simultaneous Determination of Seven Sulfonylurea-Type Oral anti-Diabetic Agents in Adulterated Dietary Supplements and Traditional Chinese Medicines by Ultraperformance Liquid Chromatography–Tandem Mass Spectrometry. Spectrosc. Lett. 2015, 48, 163–169. DOI: 10.1080/00387010.2013.866965.
  • Zhu, Q.; Cao, Y.; Cao, Y.; Chai, Y.; Lu, F. Rapid on-Site TLC–SERS Detection of Four Antidiabetes Drugs Used as Adulterants in Botanical Dietary Supplements. Anal. Bioanal. Chem. 2014, 406, 1877–1884. DOI: 10.1007/s00216-013-7605-7.
  • Yanchun, F.; Deqing, L.; Changqin, H. Rapid Identification of Illegal Synthetic Adulterants in Herbal anti-Diabetic Medicines Using near Infrared Spectroscopy. Spectrochim. Acta A Mol. Biomol. Spectrosc. 2014, 125, 363–374. DOI: 10.1016/j.saa.2014.01.117.
  • Wang, Z.; Cao, Y.; Lu, Y.; Zhang, F.; Su, Y.; Guo, Y. Ultrasonic Extraction and Nebulization in Real-Time Coupled with Carbon Fiber Ionization Mass Spectrometry for Rapid Screening of the Synthetic Drugs Adulterated into Herbal Products. Anal. Chim. Acta 2020, 1136, 62–71. DOI: 10.1016/j.aca.2020.08.045.
  • Cao, J.; Jiang, Q.; Li, R.; Xu, Q.; Li, H. Nanofibers Mat as Sampling Module of Direct Analysis in Real Time Mass Spectrometry for Sensitive and High-Throughput Screening of Illegally Adulterated Sulfonylureas in Antidiabetic Health-Care Teas. Talanta 2019, 204, 753–761. DOI: 10.1016/j.talanta.2019.06.066.
  • Xie, X.; Zhang, Y.; Yue, Z.; Wang, K.; Mai, X.; Liu, Y.; Zhu, M.; Fan, H.; Zhang, W. Multi-Fingerprint Profiling Analysis for Screening and Quantification of Illegal Adulterated Antidiabetics in a Functional Food Using HPLC Coupled to Diode Array Detection/Fluorescence Detection. Microchem. J. 2019, 149, 103995. DOI: 10.1016/j.microc.2019.103995.
  • Rani, R.; Medhe, S.; Srivastava, M. HPTLC–MS Based Method Development and Validation for the Detection of Adulterants in Spices. Food Measure. 2015, 9, 186–194. DOI: 10.1007/s11694-015-9223-x.

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