Non-destructive chromatographic determination of surface area in reverse phase chromatographic columns

References

• Guillemin, C. L. Specific Surface Area: The Neglected Parameter in Chromatography. J. Chromatogr. A 1978, 158, 21–32. DOI: 10.1016/S0021-9673(00)89952-5.
   Web of Science ®Google Scholar
• Kiselev, A. V. Problems of Molecular Adsorption Chromatography. J. Chromatogr. 1970, 49, 84–129. DOI: 10.1016/S0021-9673(00)93615-X.
   Google Scholar
• Kiselev, A. V.; Nikitin, Y. S.; Frolov, I. I.; Yashin, Y. I. Problems of Selectivity and Efficiency in Liquid-Solid Chromatography. J. Chromatogr. 1974, 91, 187–200. DOI: 10.1016/S0021-9673(01)97899-9.
   Web of Science ®Google Scholar
• Ahmad, I. A. H.; Losacco, G. L.; Figus, M.; Korani, D.; Gunsch, M. J.; Lhotka, H. R.; Hullen, K.; Hartman, R.; Lohani, S.; Hamilton, S.; et al. Generic Reversed-Phase Ultra-High-Pressure Liquid Chromatography Methodology Developed by Using Computer-Assisted Modeling for Streamlined Performance Evaluation of a Wide Range of Stationary Phase Columns. Sep. Sci. Plus. 2022, 5, 138–145. DOI: 10.1002/sscp.202200002.
   Web of Science ®Google Scholar
• Mattrey, F. T.; Makarov, A. A.; Regalado, E. L.; Bernardoni, F.; Figus, M.; Hicks, M. B.; Zheng, J.; Wang, L.; Schafer, W.; Antonucci, V.; et al. Current Challenges and Future Prospects in Chromatographic Method Development for Pharmaceutical Research. TrAC, Trends Anal. Chem 2017, 95, 36–46. DOI: 10.1016/j.trac.2017.07.021.
   Web of Science ®Google Scholar
• Horváth, C.; Melander, W.; Molnár, I. Solvophobic Interactions in Liquid Chromatography with Nonpolar Stationary Phases. J. Chromatogr. 1976, 125, 129–156. DOI: 10.1016/S0021-9673(00)93816-0.
   Web of Science ®Google Scholar
• Kazakevich, Y. V.; Lobrutto, R. HPLC for Pharmaceutical Scientists; John Wiley & Sons, Inc.: Hoboken, 2007.
   Google Scholar
• Synder, L. R.; Kirkland, J. J.; Glajch, J. L. Practical HPLC Method Development, 2nd ed.; Wiley: New York, 1997.
   Google Scholar
• Kazakevich, Y. V. High-Performance Liquid Chromatography Retention Mechanisms and Their Mathematical Descriptions. J. Chromatogr. A 2006, 1126, 232–243. DOI: 10.1016/j.chroma.2006.05.022.
   PubMed Web of Science ®Google Scholar
• Vailaya, A.; Horváth, C. Retention in Reversed-Phase Chromatography: Partition or Adsorption? J. Chromatogr. A 1998, 829, 1–27. DOI: 10.1016/s0021-9673(98)00727-4.
   PubMed Web of Science ®Google Scholar
• Wang, H. L.; Duda, J. L.; Radke, C. J. Solution Adsorption from Liquid Chromatography. J. Colloid. Interface Sci. 1978, 66, 153–165. DOI: 10.1016/0021-9797(78)90196-0.
   Web of Science ®Google Scholar
• Riedo, F.; Kováts, E. Adsorption from Liquid Mixtures and Liquid Chromatography. J. Chromatogr. 1982, 239, 1–28. DOI: 10.1016/S0021-9673(00)81964-0.
   PubMed Web of Science ®Google Scholar
• Buntz, S.; Figus, M.; Liu, Z.; Kazakevich, Y. V. Excess Adsorption of Binary Aqueous Organic Mixtures on Various Reversed-Phase Packing Materials. J. Chromatogr. A 2012, 1240, 104–112. DOI: 10.1016/j.chroma.2012.03.087.
   PubMed Web of Science ®Google Scholar
• Chan, F.; Yeung, L. S.; LoBrutto, R.; Kazakevich, Y. Interpretation of the Excess Adsorption Isotherms of Organic Eluent Components on the Surface of Reversed-Phase Phenyl Modified Adsorbents. J. Chromatogr. A 2005, 1082, 158–165. DOI: 10.1016/j.chroma.2005.05.078.
   PubMed Web of Science ®Google Scholar
• Kazakevich, Y. V.; McNair, H. M. Study of the Excess Adsorption of the Eluent Components on Different Reversed-Phase Adsorbents. J. Chromatogr. Sci 1995, 33, 321–327. DOI: 10.1093/chromsci/33.6.321.
   Web of Science ®Google Scholar
• McCormick, R. M.; Karger, B. L. Distribution Phenomena of Mobile-Phase Components and Determination of Dead Volume in Reversed-Phase Liquid Chromatography. Anal. Chem. 1980, 52, 2249–2257. DOI: 10.1021/ac50064a005.
   Web of Science ®Google Scholar
• Giaquinto, A.; Liu, Z. X.; Bach, A.; Kazakevich, Y. Surface Area of Reversed-Phase HPLC Columns. Anal. Chem. 2008, 80, 6358–6364. DOI: 10.1021/ac800772s.
   PubMed Web of Science ®Google Scholar
• Unger, K. K.; Becker, N.; Roumeliotis, P. Recent Developments in the Evaluation of Chemically Bonded Silica Packings for Liquid Chromatography. J. Chromatogr. 1976, 125, 115–127. DOI: 10.1016/S0021-9673(00)93815-9.
   Web of Science ®Google Scholar
• Fóti, G.; Belvito, M. L.; Alvarez-Zepeda, A.; Kováts, E. s Retention on Non-Polar Adsorbents in Liquid-Solid Chromatography: Effect of Grafted Alkyl Chains. J. Chromatogr. 1992, 630, 1–20. DOI: 10.1016/0021-9673(93)80438-E.
   Web of Science ®Google Scholar
• Rustamov, I.; Farcas, T.; Ahmed, F.; Chan, F.; LoBrutto, R.; McNair, H. M.; Kazakevich, Y. V. Geometry of Chemically Modified Silica. J. Chromatogr. A 2001, 913, 49–63. DOI: 10.1016/s0021-9673(00)01076-1.
   PubMed Web of Science ®Google Scholar
• Sing, K. S. W.; Everett, D. H.; Haul, R. A. W.; Moscou, L.; Pierotti, R. A.; Rouquerol, J.; Siemieniewska, T. Reporting Physisorption Data for Gas/Solid Systems with Special Reference to the Determination of Surface Area and Porosity (Recommendations 1984). Pure Appl. Chem. 1985, 57, 603–619. DOI: 10.1351/pac198557040603.
   Web of Science ®Google Scholar
• Gregg, S. J.; Sing, K. S. W. Adsorption, Surface Area and Porosity, 2nd ed.; Academic Press: London, 1982.
   Google Scholar
• Brunauer, S.; Emmett, P. H.; Teller, E. Adsorption of Gases in Multimolecular Layers. J. Am. Chem. Soc. 1938, 60, 309–319. DOI: 10.1021/ja01269a023.
   Web of Science ®Google Scholar
• Emmett, P. H. Catalysis. Volume II. Pt. 2. Fundamental Principles; Reinhold Pub. Corp: New York, 1955.
   Google Scholar
• Unger, K. K. Porous Silica Its Properties and Use as Support in Column Liquid Chromatography; Elsevier Scientific Publishing Company: New York, 1979.
   Google Scholar
• Barrett, E. P.; Joyner, L. G.; Halenda, P. P. The Determination of Pore Volume and Area Distributions in Porous Substances. I. Computations from Nitrogen Isotherms. J. Am. Chem. Soc. 1951, 73, 373–380. DOI: 10.1021/ja01145a126.
   Web of Science ®Google Scholar
• Knox, J. H.; Kaliszan, R. Theory of Solvent Disturbance Peaks and Experimental Determination of Thermodynamic Dead-Volume in Column Liquid Chromatography. J. Chromatogr. 1985, 349, 211–234. DOI: 10.1016/S0021-9673(01)83779-1.
   Web of Science ®Google Scholar
• Bocian, S.; Felinger, A.; Buszewski, B. Comparison of Solvent Adsorption on Chemically Bonded Stationary Phases in RP-LC. Chroma. 2008, 68, 19–26. DOI: 10.1365/s10337-008-0519-4.
   Web of Science ®Google Scholar
• Bocian, S.; Vajda, P.; Felinger, A.; Buszewski, B. Excess Adsorption of Commonly Used Organic Solvents from Water on Nonend-Capped C18-Bonded Phases in Reversed-Phase Liquid Chromatography. Anal. Chem. 2009, 81, 6334–6346. DOI: 10.1021/ac9005759.
   Web of Science ®Google Scholar
• Yeung, L. S. Assesment of Energetic Heterogenity of Reverse-Phase Surfaces Using Excess Adsorption Isotherm for HPLC Column Characterization. Chemistry Seton Hall University: South Orange, 2018.
   Google Scholar
• Riedo, F.; Czencz, M.; Liardon, O.; Kovats, E. S. Chemically Modified Silicon Dioxide Surfaces. Wetting Properties of Compact n-Alkyl-Dimethylsiloxy Layers, and Their Mixed Surface Crystals. The Question of Wetting of Molecularly Rough and Swollen Surfaces. Helv. Chim. Acta 1978, 61, 1912.
   Web of Science ®Google Scholar
• Bernardoni, F.; Kouba, M.; Fadeev, A. Y. Effect of Curvature on the Packing and Ordering of Organosilane Monolayers Supported on Solids. Chem. Mater. 2008, 20, 382–387. DOI: 10.1021/cm070842y.
   Web of Science ®Google Scholar
• Kazakevich, Y. V.; McNair, H. M. Thermodynamic Definition of HPLC Dead Volume. J. Chromatogr. Sci. 1993, 31, 317–322. DOI: 10.1093/chromsci/31.8.317.
   Web of Science ®Google Scholar
• Kazakevich, Y.; Kant, M. Size-Exclusion and the Void Volume of HPLC Column. J. Liq. Chromatogr. R T 2019, 42, 89–98. DOI: 10.1080/10826076.2019.1577255.
   Web of Science ®Google Scholar
• McElwee, J.; Helmy, R.; Fadeev, A. Y. Thermal Stability of Organic Monolayers Chemically Grafted to Minerals. J. Colloid Interface Sci. 2005, 285, 551–556. DOI: 10.1016/j.jcis.2004.12.006.
   PubMed Web of Science ®Google Scholar
• Gibbs, J. W. Thermodynamics, the Collected Works of J. Willard Gibbs, Vol. 1; Thermodynamics, Longmans Green: New York, 1928; pp. 438.
   Google Scholar
• Sing, K. The Use of Nitrogen Adsorption for the Characterization of Porous Materials. Colloids Surf. A 2001, 187-188, 3–9. DOI: 10.1016/S0927-7757(01)00612-4.
   Web of Science ®Google Scholar
• Pierce, C. Effects of Interparticle Condensation on Heats of Adsorption and Isotherm of Powdered Samples. J. Phys. Chem. 1959, 63, 1076–1079. DOI: 10.1021/j150577a011.
   Web of Science ®Google Scholar
• Lippens, B. C.; de Boer, J. H. Studies on Pore Systems in Catalysts: V. The t Method. J. Catal. 1965, 4, 319–323. DOI: 10.1016/0021-9517(65)90307-6.
   Web of Science ®Google Scholar
• Lippens, B. C.; Linsen, B. G.; Boer, J. Studies on Pore Systems in Catalysts I. The Adsorption of Nitrogen; Apparatus and Calculation. J. Catal. 1964, 3, 32–37. DOI: 10.1016/0021-9517(64)90089-2.
   Web of Science ®Google Scholar