Determination of Selected Phthalates by Gas Chromatography–Mass Spectrometry in Personal Perfumes

REFERENCES

• Amorello, D., and Orecchio, S. 2013. Micro determination of dithiocarbamates in pesticide formulations using voltammetry. Microchem. J. 110: 334–339.
   Web of Science ®Google Scholar
• Api, A. M. 2001. Toxicological profile of diethyl phthalate: A vehicle for fragrance and cosmetic ingredients. Food Chem Toxicol. 39: 97–108.
   PubMed Web of Science ®Google Scholar
• Barreca, S., Indelicato, R., Orecchio, S., and Pace, A. 2014. Photodegradation of selected phthalates on mural painting surfaces under UV light irradiation. Microchem. J. 114: 192–196.
   Web of Science ®Google Scholar
• Beving, H. F., Petren, S., and Vesterberg, O. 1990 Increased isotransferrin ratio and reduced erythrocyte and platelet volumes in blood from thermoplastic industry workers. Ann. Occup. Hyg. 34: 391–397.
   PubMed Web of Science ®Google Scholar
• Billot, M., and Wells, F. V. 1975. The perfumer’s raw materials: Products of natural origin. In Perfumery technology, chap. 3. Chichester, UK: Springer Ellis Horwood.
   Google Scholar
• Birnbaum, L. S., and Schug, T. T. 2013 Phthalates in our food. Endocr. Disrupt. 1: e25078.
   Google Scholar
• Bornehag, G., Sundell, J., Weschler, C. J., Sigsgaard, T., Lundgren, B., Hasselgren, M., and Hägerhed-Engman, L. 2004. The association between asthma and allergic symptoms in children and phthalates in house dust: A nested case-control study. Environ. Health Perspect. 112: 1393–1397.
   PubMed Web of Science ®Google Scholar
• Casabianca, H., Graff, J. B., Jame, P., Perrucchietti, C., and Chastrette, M. 1995. Application of hyphenated techniques to the chromatographic authentication of flavors in food-products and perfumes. J. High Res. Chromatogr. 18: 279–292.
   Google Scholar
• Chen, H., Wang, C., Wang, X., Hao, N., and Liu, J. 2005. Determination of phthalate esters in cosmetics by gas chromatography with flame ionization detection and mass spectrometric detection. Int. J. Cosmet. Sci. 27: 205–210.
   PubMedGoogle Scholar
• Choi, S. M., and Lee, B. M. 2004 An alternative mode of action of endocrine disrupting chemicals and chemoprevention. J. Toxicol. Environ. Health B 7: 451–463.
   PubMed Web of Science ®Google Scholar
• De Orsi, D., Gagliardi, L., Porrà, R., Berri, S., Chimenti, P., Granese, A., Carpani, I., Tonelli, D. A. 2006. Environmentally friendly reversed-phase liquid chromatography method for phthalates determination in nail cosmetics. Anal. Chim. Acta 555: 238–241.
   Web of Science ®Google Scholar
• European Community. 2009. Annex II, Regulation (EC) no 1223/2009 of the European Parliament and of the Council of 30 November 2009 on cosmetic products.
   Google Scholar
• European Economic Community. 1976. Annex II, Council Directive of 27 July 1976 on the approximation of the laws of the Member States relating to cosmetic products (76/768/EEC).
   Google Scholar
• Ferguson, K. K., O’Neill, M. S., and Meeker, J. D. 2013. J. Toxicol. Environ. Health B 16: 69–113.
   Web of Science ®Google Scholar
• Greenpeace. 2005. Perfume—An investigation of chemicals in 36 eau de toilette and eau de parfume. Greenpeace International. http://www.greenpeace.org/international/en/publications/reports/perfume-an-investigation
   Google Scholar
• Harrison, P. T. C., Holmes, P., and Humfrey, C. D. N. 1997. Reproductive health in humans and wildlife: Are adverse trends associated with environmental chemical exposure? Sci. Total Environ. 205: 97–106.
   PubMed Web of Science ®Google Scholar
• Health Canada. 2009a. Cosmetics and personal care. Health Canada (EC), Consumer Product Safety. www.hc-sc.gc.ca/cps-spc/person/cosmet/index-eng.phpS.
   Google Scholar
• Health Canada. 2009b. Proposed phthalates regulations for soft vinyl children’s toys and child care articles. http://hc-sc.gc.ca/cps-spc/legislation/consultation/phthalates-phthalates-eng.phpS
   Google Scholar
• Horwitz, W., and Albert, R. J. 2006. The Horwitz Ratio (HorRat): A useful index of method performance with respect to precision. J. Assoc. Off. Anal. Chem. 89: 1095–1109.
   Google Scholar
• Horwitz, W., Kamps, L. R., and Boyer, R. W. 1980. Quality assurance in the analysis of foods for trace constituents. J. Assoc. Off. Anal. Chem. 63: 1344–1354.
   PubMedGoogle Scholar
• Houlihan, J., Brody, C., and Schwan, B. 2002. ‘Not too pretty.’ Phthalates, beauty products and the FDA. www.ewg.org/reports/nottoopretty
   Google Scholar
• Hubinger, J. C., and Harvey, D. C. 2006 Analysis of consumer cosmetic products for phthalate esters. J. Cosmet. Sci. 57: 127–137.
   PubMed Web of Science ®Google Scholar
• Hyun, H. K., and Lee, B. M. 2004. Estimated exposure to phthalates in cosmetics and risk assessment. J. Toxicol. Environ. Health A 67: 1901–1914.
   PubMed Web of Science ®Google Scholar
• International Agency for Research on Cancer. 2000. Di(2-ethylhexyl) phthalate. IARC Monogr. Eval. Carcinogen. Risk Chem. Hum. 77: 148. http://monographs.iarc.fr/ENG/Monographs/vol177.pdf-141
   Google Scholar
• Indelicato, R., Barreca, S., and Orecchio, S. 2014. Determination of selected phthalates by gas chromatography–mass spectrometry in mural paintings from Palermo (Italy). Microchem. J. 114: 187–191.
   Web of Science ®Google Scholar
• Jurewicz, J., and Hanke, W. 2011. Exposure to phthalates: Reproductive outcome and children health. A review of epidemiological studies. Int. J. Occup. Med. Environ. Health 24: 114–141.
   Web of Science ®Google Scholar
• Kavlock, R., Boekelheide, K., Chapin, R., Cunningham, M., Faustman, E., and Foster, P. 2002. Center for the evaluation of risks to human reproduction: Phthalates expert panel report on the reproductive and developmental toxicity of butyl benzylphthalate. Reprod. Toxicol. 16: 453–653.
   PubMed Web of Science ®Google Scholar
• Kim, T. S., Jung, K. J., Kim, S. S., Kang, I.H., Baek, J. H., Nam, H. S., Hong, S. K., Lee, B. M., Hong, J. T., Oh, K. W., Han, S. Y., and Kang, T. S. 2010. Effects of in utero exposure to di(n-butyl) phthalate on development of male reproductive tracts in Sprague-Dawley rats. J. Toxicol. Environ. Health A 73: 1544–1559.
   PubMed Web of Science ®Google Scholar
• Koniecki, D., Wang, R., Moody, R. P., and Zhu, J. 2011. Phthalates in cosmetic and personal care products: Concentrations and possible dermal exposure. Environ. Res. 111: 329–336.
   PubMed Web of Science ®Google Scholar
• Larsen, S. T., Hansen, J. S., Hansen, E. W., Clausen, P. A., and Nielsen, G. D. 2007. Airway inflammation and adjuvant effect after repeated airborne exposures to di-(2-ethylhexyl)phthalate and ovalbumin in BALB/c mice. Toxicology 235: 119–129.
   PubMed Web of Science ®Google Scholar
• López-Nogueroles, M., Benedé, J. L., Chisvert, A., and Salvador, A. 2013. A rapid and sensitive gas chromatography-mass spectrometry method for the quality control of perfumes: Simultaneous determination of phthalates. Anal. Methods 5: 409–415.
   Web of Science ®Google Scholar
• Mannino, M. R., and Orecchio, S. 2011. Chemical characterization of ancient potteries from Himera and Pestavecchia necropolis (Sicily, Italy) by inductively coupled plasma-optical emission spectrometry (ICP-OES). Microchem. J. 97: 165–172.
   Web of Science ®Google Scholar
• Martinez-Arguelles, D. B., Culty, M., Zirkin, D. R., and Papadopoulos, V. 2009. In utero exposure to di-(2-ethylhexyl) phthalate decreases mineralocorticoid receptor expression in the adult testis. Endocrinology 150: 5575–5585.
   PubMed Web of Science ®Google Scholar
• Mendiola, J., Meeker, J. D., Jørgensen, N., Andersson, A. M., Liu, F., Calafat, A. M., Redmon, J. B., Drobnis, E. Z., Sparks, A. E., Wang, C., Hauser, R., and Swan, S. H. 2012. Urinary concentrations of di(2-ethylhexyl) phthalate metabolites and serum reproductive hormones: Pooled analysis of fertile and infertile men. J. Androl. 33: 488–498.
   PubMed Web of Science ®Google Scholar
• Orecchio, S. 2010. Analytical method, pattern and sources of polycyclic aromatic hydrocarbons (PAHs) in the stone of the Temples of Agrigento (Italy). J. Hazard. Mater. 176: 339–347.
   PubMed Web of Science ®Google Scholar
• Orecchio, S. 2011. Polycyclic aromatic hydrocarbons (PAHs) in indoor emission from decorative candles. Atmos. Environ. 45:1888–1895.
   Web of Science ®Google Scholar
• Orecchio, S., and Amorello, D. 2011. Platinum levels in urban soils from Palermo (Italy); Analytical method using voltammetry. Microchem. J. 99: 283–288.
   Web of Science ®Google Scholar
• Orecchio, S., Indelicato, R., and Barreca, S. 2013. The distribution of phthalate esters in indoor dust of Palermo (Italy). Environ. Geochem. Health 35: 613–624.
   PubMed Web of Science ®Google Scholar
• Romero-Franco, M., Hernández-Ramír, R. U., Calafat, A. M., Cebrián, M. E., Needham, L. L., Teitelbaum, S., Wolff, M. S., and López-Carrillo, L. 2011. Personal care product use and urinary levels of phthalate metabolites in Mexican women. Environ. Int. 37: 867–871.
   PubMed Web of Science ®Google Scholar
• Sanchez-Prado, L., Llompart, M., Lamas, J. P., Garcia-Jares, C., and Lores, M. 2011. Multicomponent analytical methodology to control phthalates, synthetic musks, fragrance allergens and preservatives in perfumes. Talanta 85: 370–379.
   PubMed Web of Science ®Google Scholar
• Schettler, T., Skakkebæk, N. E., De Kretser, D., and Leffers, H. 2006. Human exposure to phthalates via consumer products. Int. J. Androl. 29: 134–139.
   PubMed Web of Science ®Google Scholar
• Scientific Committee on Consumer Products. 2007. Opinion on phthalates in cosmetic products opinion adopted at the 11th plenary meeting of 21 March 2007, Brussels, SCCP/1016/06, 19.
   Google Scholar
• Shen, H. Y., Jiang, H. L., Mao, H. L., Pan, G., Zhou, L., and Cao, Y. F. 2007. Simultaneous determination of seven phthalates and four parabens in cosmetic products using HPLC-DAD and GC-MS methods. J. Separat. Sci. 30: 48–54.
   PubMed Web of Science ®Google Scholar
• Sonde, V., D’souza, A., Tarapore, R., Pereira, L., Khare, M. P., Sinkar, P., Krishnan, S., and Rao, C. V. 2000. Simultaneous administration of diethylphthalate and ethyl alcohol and its toxicity in male Sprague-Dawley rats. Toxicology 147: 23–31.
   PubMed Web of Science ®Google Scholar
• Su, R., Zhao, X., Li, Z., Jia, Q., Liu, P., and Jia, J. 2010. Poly(methacrylic acid-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography for the determination of phthalate esters in cosmetics. Anal. Chim. Acta 676: 103–108.
   PubMed Web of Science ®Google Scholar
• Thomson, E. M. 2013. Neurobehavioral and metabolic impacts of inhaled pollutants. Endocr. Disrupt. 1: e27489.
   Google Scholar
• U.S. Department of Health and Human Services, Public Health Service, Agency for Toxic Substances and Disease Registry. 1995. Toxicological profile for diethyl phthalate. June. http://www.atsdr.cdc.gov/toxprofiles/tp73.pdf
   Google Scholar
• Wolfe, G. W., and Layton, K. A. 2003. Multigeneration reproduction toxicity study in rats diethylhexylphthalate: Multigenerational reproductive assessment by continuous breeding when administered to Sprague-Dawley rats in the diet. The Immune Research Corporation, TRC Study no. 7244-200, Gaithersburg, MD.
   Google Scholar
• Yoon, K., Kwack, S. J., Kim, H. S., and Lee, B. M. 2014. Estrogenic endocrine-disrupting chemicals: Molecular mechanisms of actions on putative human diseases. J. Toxicol. Environ Health B 17: 127–174.
   PubMed Web of Science ®Google Scholar
• Zeng, F., Cui, K., Xie, Z., Wu, L., Luo, D., and Chen, L. 2009. Distribution of phthalate esters in urban soils of subtropical city, Guangzhou, China. Hazard. Mater. 164: 1171–1178.
   PubMed Web of Science ®Google Scholar