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Original Articles

Synthesis and NMR (1H and 13C) Study OF (Monoamino)Dimethylarsines

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Pages 427-444 | Received 09 Oct 1990, Accepted 07 Nov 1990, Published online: 23 Sep 2006

References

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  • A, transamination (heating °C/time); B, aminolysis; C, amination
  • Percentage conversion values from NMR
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  • O. 20 M; C6D6;room temperature
  • First-order spectrum
  • Calculated chemical shifts from iterative non-first-order analysis
  • Complex spectrum; approximate values (±0.01 ppm)
  • Complex spectrum, single peaks broadened by partially resolved coupling
  • From 2-D heteronuclear correlated NMR
  • No spectral analysis reported
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