Production and purification of anhydrous sodium sulfide

References

• Xu X, Zhou D, Qin X, et al. A room-temperature sodium–sulfur battery with high capacity and stable cycling performance. Nat Commun. 2018;9(1):3870.
   Google Scholar
• Yang H, Zhang B, Wang YX, et al. Alkali-metal sulfide as cathodes toward safe and high-capacity metal (M = Li, Na. K) sulfur batteries. Adv Energy Mater. 2020;10(37):2001764.
   Web of Science ®Google Scholar
• Yu X, Manthiram A. Performance enhancement and mechanistic studies of room-temperature sodium–Sulfur Batteries with a Carbon-coated functional nafion separator and a Na2S/activated Carbon nanofiber cathode. Chem Mater. 2016;28(3):896–905.
   Web of Science ®Google Scholar
• Noi K, Hayashi A, Tatsumisago M. Structure and properties of the Na2S–P2S5 glasses and glass–ceramics prepared by mechanical milling. J Power Sources. 2014;269:260–265.
   Web of Science ®Google Scholar
• Hayashi A, Masuzawa N, Yubuchi S, et al. A sodium-ion sulfide solid electrolyte with unprecedented conductivity at room temperature. Nat Commun. 2019;10(1):5266.
   Google Scholar
• Dive A, Zhang Y, Yao Y, et al. Investigations of the structure of Na2S+P2S5 glassy electrolytes and its impact on Na+ ionic conductivity through ab initio molecular dynamics. Solid State Ionics. 2019;338:177–184.
   Web of Science ®Google Scholar
• Miura A, Ito H, Bartel C, et al. Selective metathesis synthesis of MgCr2S4 by control of thermodynamic driving forces [10.1039/C9MH01999E]. Mater Horiz. 2020.
   Web of Science ®Google Scholar
• Chandrasekaran S, Yao L, Deng L, et al. Recent advances in metal sulfides: from controlled fabrication to electrocatalytic, photocatalytic and photoelectrochemical water splitting and beyond. Chem Soc Rev. 2019 Jul 29;48(15):4178–4280.
   PubMed Web of Science ®Google Scholar
• Zhang F, Wong SS. Controlled synthesis of semiconducting metal sulfide nanowires. Chem Mater. 2009;21(19):4541–4554.
   Web of Science ®Google Scholar
• Borodkin Y, Rusanov E, Marchenko A, et al. Synthesis and chemical properties of Di(2-fluoro-2-polyfluoroalkyl- alkenyl)sulfides and 2,6-bis(polyfluoroalkyl)-1,4-oxathiine 4,4-dioxides. J Sulfur Chem. 2019;40(4):416–425.
   Web of Science ®Google Scholar
• Szabo C, Papapetropoulos A. International union of basic and clinical pharmacology. CII: Pharmacological modulation of H2S levels: H2S donors and H2S biosynthesis inhibitors. Pharmacol Rev. 2017 Oct;69(4):497–564.
   PubMed Web of Science ®Google Scholar
• Butts D, Bush DR. Sodium sulfates and sulfides. kirk-othmer encyclopedia of chemical technology. New York: John Wiley & Sons, Inc; 2013.
   Google Scholar
• Li X, Zhao Y, Brennan A, et al. Reactive precipitation of anhydrous Alkali Sulfide Nanocrystals with concomitant abatement of hydrogen sulfide and cogeneration of hydrogen. ChemSusChem. 2017 Jul 21;10(14):2904–2913.
   PubMed Web of Science ®Google Scholar
• Hietala K, Zhao Y, Yang Y, et al. Scalable Synthesis of Alkali Sulfide nanocrystals using a bubble column reactor. Ind Eng Chem Res. 2018;57(25):8436–8442.
   Web of Science ®Google Scholar
• Zhao Y, Yang Y, Wolden CA. Scalable Synthesis of size-controlled Li2S nanocrystals for next-generation battery technologies. ACS Applied Energy Materials. 2019;2(3):2246–2254.
   Web of Science ®Google Scholar
• Zhao Y, Smith W, Wolden CA. Scalable synthesis of Li2S nanocrystals for solid-state electrolyte applications. J Electrochem Soc. 2020;167:070520.
   Web of Science ®Google Scholar
• Kizilyalli M, Bilgin M, Kizilyalli HM. Solid-state synthesis and X-ray diffraction studies of Na2S. J Solid State Chem. 1990;85(2):283–292.
   Web of Science ®Google Scholar
• Beckenkamp K, Lutz HD, Jacobs H, et al. Polymorphism and phase transitions of the isostructural MSH (M = Na, K, and Rb). J Solid State Chem. 1994;109(2):241–250.
   Web of Science ®Google Scholar
• Rosen E, Tegman R. A preparative and X-ray powder diffraction study of the polysulfides Na2S2, Na2S4 and Na2S5. Acta Chem Scand. 1971;25:3329–3336.
   Google Scholar
• Nakamoto K. Infrared and Raman spectra of inorganic and coordination compounds. New York: John Wiley & Sons, Ltd.; 2006.
   Google Scholar
• Zhang Q. The synthesis and characterization of sodium polysulfides for Na-S battery application. Blacksburg, VA: Virginia Polytechnic Institute and State University; 2019.
   Google Scholar
• Cross PC, Burnham J, Leighton PA. The Raman spectrum and the structure of water. J Am Chem Soc. 1937;59(6):1134–1147.
   Google Scholar
• Barstow EO, Heath SB. inventors; Dow Chemical Co, assignee. Process of Dehydrating Magnesium Chloride patent US1874735. 1929.
   Google Scholar
• Anderson JY, Azoulay M. Mechanisms and kinetics of the thermal decomposition of sodium sulphide pentahydrate under controlled water vapour pressure. J Chem Soc Dalton Trans. 1986;3:469–475.
   Google Scholar
• Courtois MG, Lebeau MP. Preparation of anhydrous sodium sulfide. Weekly Reports of Meetings of the Académie des Sciences. 1938;207:1220–1221.
   Google Scholar
• Copes JP, McKinley C. inventors; General Aniline & Film Corporation, assignee. Dehydration of Sodium Sulfide. U.S.A. patent US2533163. 1950.
   Google Scholar
• Maeda K, Aoyama Y. inventors; Sankyo Kasei Co., assignee. Process for preparing crystals of anhydrous sodium sulfide patent US5071632. 1991.
   Google Scholar
• Sheppard DA, Jepsen LH, Jensen TR, et al. New directions for hydrogen storage: sulphur destabilised sodium aluminium hydride. J Mater Chem A. 2013;1(41):12775.
   Web of Science ®Google Scholar
• Froment GF, Bischoff KB, De Wilde J. Heterogeneous model with shrinking unreacted core. chemical reactor analysis and design. Hoboken (NJ): John Wiley & Sons, Inc; 2011.
   Google Scholar
• Cho H, Walker S, Plunkett M, et al. Scalable Gas-phase purification of boron nitride nanotubes by Selective chlorine etching. Chem Mater. 2020;32(9):3911–3921.
   Web of Science ®Google Scholar
• Nagy P, Palinkas Z, Nagy A, et al. Chemical aspects of hydrogen sulfide measurements in physiological samples. Biochim Biophys Acta. 2014 Feb;1840(2):876–891.
   PubMed Web of Science ®Google Scholar