Phosphodiesterase-5 inhibitors in Chinese tonic liquors by liquid chromatography coupled with quadrupole time of flight mass spectrometry

References

• Ackermann BL, Berna MJ, Eckstein JA, Ott LW, Chaudhary AK. 2008. Current applications of liquid chromatography/mass spectrometry in pharmaceutical discovery after a decade of innovation. Annual Rev Anal Chem. 1:357–396.
   PubMed Web of Science ®Google Scholar
• Anastassiades M, Lehotay SJ, Štajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce. J AOAC Int. 86:412–431.
   PubMed Web of Science ®Google Scholar
• CFDA release. 2015. At least 51 distillers have added doses of sildenafil-the generic name for Viagra-to their spirits. Available from http://www.sfda.gov.cn/WS01/CL0050/125640.html
   Google Scholar
• Chapman JD, Goodlett DR, Masselon CD. 2014. Multiplexed and data-independent tandem mass spectrometry for global proteome profiling. Mass Spectrom Rev. 33:452–470.
   PubMed Web of Science ®Google Scholar
• Damiano F, Silva C, Gregori A, Vacondio F, Mor M, Menozzi M, Di Giorgio D. 2014. Analysis of illicit dietary supplements sold in the Italian market: identification of a sildenafil thioderivative as adulterant using UPLC–TOF/MS and GC/MS. Sci Justice. 54:228–237.
   PubMed Web of Science ®Google Scholar
• Eli Lilly and company. 2016. Cialis(tadalafil) Tablets, for oral use. Full prescribing information. IN 46285 USA. Indianapolis
   Google Scholar
• Fejős I, Neumajer G, Béni S, Jankovics P. 2014. Qualitative and quantitative analysis of PDE-5 inhibitors in counterfeit medicines and dietary supplements by HPLC–UV using sildenafil as a sole reference. J Pharm Biomed Anal. 98:327–333.
   PubMed Web of Science ®Google Scholar
• Gilard V, Balayssac S, Tinaugus A, Martins N, Martino R, Malet-Martino M. 2015. Detection, identification and quantification by 1H NMR of adulterants in 150 herbal dietary supplements marketed for improving sexual performance. J Pharm Biomed Anal. 102:476–493.
   PubMed Web of Science ®Google Scholar
• Guan Y-Z, Liang RH, Wu QY, Zhang SY, Xu CH, Liu C. 2011. Pharmacodynamics study of qirong health wine. Pharmacy Today. 21:91–93.
   Google Scholar
• Hoffmann WD, Jackson GP. 2015. Forensic Mass Spectrometry. Annu Rev Anal Chem. 8:419–440. [2015 July 22].
   PubMed Web of Science ®Google Scholar
• Jeong JH, Lee JH, Kim HJ, Park HJ, Hwang IS, Han KM, Yoon CY, Cho S, Kim WS. 2016. LC-ESI-MS/MS analysis of phosphodiesterase-5 inhibitors and their analogues in foods and dietary supplements in Korea. Food Addit Contam B. 9:1–8.
   PubMed Web of Science ®Google Scholar
• Kim S-H, Kim HJ, Son J, Jeon BW, Jeong ES. 2012. Simultaneous determination of synthetic phosphodiesterase-5 inhibitors in dietary supplements by liquid chromatography-high resolution/mass spectrometry. Mass Spectrom Lett. 3:50.
   Google Scholar
• Lebedev AT. 2013. Environmental Mass Spectrometry. Annual Rev Anal Chem. 6:163–189.
   PubMed Web of Science ®Google Scholar
• Lebel P, Gagnon J, Furtos A, Waldron KC. 2014. A rapid, quantitative liquid chromatography-mass spectrometry screening method for 71 active and 11 natural erectile dysfunction ingredients present in potentially adulterated or counterfeit products. J Chromatogr A. 1343:143–151.
   PubMed Web of Science ®Google Scholar
• Li A. 2009. Considerations on the research and development of health Liquor. Liquor Making. 36:87–89.
   Google Scholar
• Li L, Low M-Y, Ge X, Bloodworth B, Koh H-L. 2013. Isolation and structural elucidation of a new sildenafil analogue from a functional coffee. Anal Bioanal Chem. 405:4443–4450.
   PubMed Web of Science ®Google Scholar
• Lu X. 2001. Chinese health tonic wine. Beijing: Science and Technology Document Press.
   Google Scholar
• Marshall AG, Hendrickson CL. 2008. High-resolution mass spectrometers. Annual Rev Anal Chem. 1:579–599.
   PubMed Web of Science ®Google Scholar
• Park S-R, Lee JG, Roh SH, Kim G, Kwon CH, Park HR, Kwon KS, Kim D, Kwon SW. 2012. Determination of PDE-5 inhibitors and appetite suppressants in adulterated dietary supplements using LC/PDA and LC/MS. Food Addit Contam B. 5:29–32.
   PubMed Web of Science ®Google Scholar
• Patel DN, Li L, Kee C-L, Ge X, Low M-Y, Koh H-L. 2014. Screening of synthetic PDE-5 inhibitors and their analogues as adulterants: analytical techniques and challenges. J Pharm Biomed Anal. 87:176–190.
   PubMed Web of Science ®Google Scholar
• Ren Y, Wu C, Zhang J. 2012. Simultaneous screening and determination of 18 illegal adulterants in herbal medicines and health foods for male sexual potency by ultra-fast liquid chromatography-electrospray ionization tandem mass spectrometry. J Sep Sci. 35:2847–2857.
   PubMed Web of Science ®Google Scholar
• Roemmelt AT, Steuer AE, Poetzsch M, Kraemer T. 2014. Liquid Chromatography, in Combination with a Quadrupole Time-of-Flight Instrument (LC QTOF), with Sequential Window Acquisition of All Theoretical Fragment-Ion Spectra (SWATH) acquisition: systematic Studies on its use for screenings in clinical and forensic toxicology and comparison with Information-Dependent Acquisition (IDA). Anal Chem. 86:11742–11749.
   PubMed Web of Science ®Google Scholar
• Said MM, Gibbons S, Moffat AC, Zloh M. 2014. Rapid detection of sildenafil analogue in Eurycoma longifolia products using a new two-tier procedure of the near infrared (NIR) spectra database. Food Chem. 158:296–301.
   PubMed Web of Science ®Google Scholar
• Shindel AW. 2009. Continuing medical education: 2009 update on phosphodiesterase type 5 inhibitor therapy part 2: updates on optimal utilization for sexual concerns and rare toxicities in this class (CME). J Sex Med. 6:2352–2364.
   PubMed Web of Science ®Google Scholar
• Vaclavik L, Krynitsky AJ, Rader JI. 2014. Targeted analysis of multiple pharmaceuticals, plant toxins and other secondary metabolites in herbal dietary supplements by ultra-high performance liquid chromatography–quadrupole-orbital ion trap mass spectrometry. Anal Chim Acta. 810:45–60.
   PubMed Web of Science ®Google Scholar
• Venhuis BJ, De Kaste D. 2012. Towards a decade of detecting new analogues of sildenafil, tadalafil and vardenafil in food supplements: A history, analytical aspects and health risks. J Pharm Biomed Anal. 69:196–208.
   PubMed Web of Science ®Google Scholar