Surveillance study of novobiocin and phenylbutazone residues in raw bovine milk using liquid chromatography-tandem mass spectrometry

References

• Compendium of Veterinary Products . 2003 . Eighth Canadian edition of the Compendium of Veterinary Products , Hansall (ON) : North American Compendiums .
   Google Scholar
• Damian , P , Craigmill , AL and Riviere , JE . 1997 . Extralabel use of nonsteroidal anti-inflammatory drugs . J Am Vet Med Assoc , 211 ( 7 ) : 860 – 861 .
   Google Scholar
• De Veau , EJ . 1996 . Determination of phenylbutazone residues in bovine milk by liquid chromatography with UV detection . J AOAC Int , 79 ( 5 ) : 1050 – 1053 .
   Google Scholar
• Dowling , G , Gallo , P , Fabbrocino , S , Serpe , L and Regan , L . 2008 . Determination of ibuprofen, ketoprofen, diclofenac and phenylbutazone in bovine milk by gas chromatography-tandem mass spectrometry . Food Addit Contam , 25 ( 12 ) : 1497 – 1508 .
   Google Scholar
• Dowling , G , Gallo , P , Malone , E and Regan , L . 2009 . Rapid confirmatory analysis of non-steroidal anti-inflammatory drugs in bovine milk by rapid resolution liquid chromatography tandem mass spectrometry . J Chrom A , 1216 ( 46 ) : 8117 – 8131 .
   Google Scholar
• Eurachem/CITAC. 2000. Eurachem/CITAC guide, Quantifying uncertainty in analytical measurement. 2nd ed. QUAM:2000.P1. [Internet]. National Measurement System (UK); [cited 26 Feb 2010]. Available from: http://www.eurachem.org/guides/QUAM2000-1.pdf/
   Google Scholar
• European Community. 2002. Commission Decision of 12 August 2002, implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results, 2002/657/EC. Off J Eur Comm. L221/8–36
   Google Scholar
• Fitzpatrick , JL , Young , FJ , Eckersall , D , Logue , DN , Knight , CJ and Nolan , A . 1998 . “ Recognizing and controlling pain and inflammation in mastitis ” . In Paper presented at: British Mastitis Conference. Proceedings of the British Mastitis Conference 1998. 36 – 44 . [Internet]. Compton (UK): Institute for Animal Health; [cited 2009 Apr 16]. Available from: http://www.iah.ac.uk/BMC/1998/Papers/PDF%20format%20papers/Fitzpatrick.pdf/
   Google Scholar
• Gallo , P , Fabbrocino , S , Vinci , F , Fiori , M , Danese , V and Serpe , L . 2008 . Confirmatory identification of sixteen non-steroidal anti-inflammatory drug residues in raw milk by liquid chromatography coupled with ion trap mass spectrometry . Rapid Commun Mass Spectrom , 22 ( 6 ) : 841 – 854 .
   Google Scholar
• Health Canada. 2008a. Administrative maximum residue limits (AMRLs) and maximum residue limits (MRLs) set by Canada. [Internet]. Veterinary Drugs Directorate (Canada); [cited 28 Apr 2009]. Available from: http://www.hc-sc.gc.ca/dhp-mps/vet/mrl-lmr/mrl-lmr_versus_new-nouveau-eng.php/
   Google Scholar
• Health Canada. 2008b. Policy on extra-label drug use (ELDU) in food producing animals. [Internet]. Veterinary Drugs Directorate (Canada); [cited 30 Apr 2009]. Available from: http://www.hc-sc.gc.ca/dhp-mps/vet/label-etiquet/pol_eldu-umdde-eng.php/
   Google Scholar
• Inoue , K , Nitta , S , Hino , T and Oka , H . 2009 . LC-MS/MS and centrifugal ultrafiltration method for the determination of novobiocin in chicken, fish tissues, milk and human serum . J Chromatogr B , 877 ( 4 ) : 461 – 464 .
   Google Scholar
• Kopcha , M , Kaneene , JB , Shea , ME , Miller , RA and Ahl , AS . 1992 . Use of nonsteroidal anti-inflammatory drugs in food animal practice . J Am Vet Med Assoc , 201 ( 12 ) : 1868 – 1872 .
   Google Scholar
• Martin , K , Andersson , L , Stridsberg , M , Wiese , B and Appelgren , L-E . 1984 . Plasma concentration, mammary excretion and side-effects of phenylbutazone after repeated oral administration in healthy cows . J Vet Pharmacol Therap , 7 ( 2 ) : 131 – 138 .
   Google Scholar
• Martin , K , Stridsberg , MI and Wiese , BM . 1983 . High-performance liquid chromatographic method for determination of phenylbutazone in bovine milk with special reference to the fat content in milk . J Chromatogr B , 276 : 224 – 229 .
   Google Scholar
• Moats , WA and Leskinen , L . 1988 . Determination of novobiocin residues in milk, blood, and tissues by liquid chromatography . J AOAC Int , 71 ( 4 ) : 776 – 778 .
   Google Scholar
• Nouws , J , van Edmond , H , Smulders , I , Loeffen , G , Schouten , J and Stegeman , H . 1999 . A microbiological assay system for assessment of raw milk exceeding EU maximum residue levels . Int Dairy J , 9 ( 2 ) : 85 – 90 .
   Google Scholar
• Ortelli , D , Cognard , E , Jan , P and Edder , P . 2009 . Comprehensive fast multiresidue screening of 150 veterinary drugs in milk by ultra-performance liquid chromatography coupled to time of flight mass spectrometry . J Chromatogr B , 877 ( 23 ) : 2363 – 2374 .
   Google Scholar
• Owens , WE and Nickerson , SC . 1990 . Treatment of Staphylococcus aureus mastitis with penicillin and novobiocin: antibiotic concentrations and bacteriologic status in milk and mammary tissue . J Dairy Sci , 73 ( 1 ) : 115 – 124 .
   Google Scholar
• Reeves , VB . 1995 . Liquid chromatographic procedure for the determination of novobiocin residues in bovine milk: interlaboratory study . J Assoc Off Anal Chem. , 78 ( 1 ) : 55 – 58 .
   Google Scholar
• Stolker , AAM , Rutgets , P , Oosterink , E , Lasaroms , JJP , Peters , RJB , van Rhijn , JA and Nielen , MWF . 2008 . Comprehensive screening and quantification of veterinary drugs in milk using UPLC-ToF-MS . Anal Bioanal Chem , 391 ( 6 ) : 2309 – 2322 .
   Google Scholar
• Sundlof , SF , Kaneene , JB and Miller , RA . 1995 . National survey on veterinarian-initiated drug use in lactating dairy cows . J Am Vet Med Assoc , 207 ( 3 ) : 347 – 352 .
   Google Scholar
• United States Pharmacopeia (USP). 2004. Veterinary anti-inflammatory monographs–phenylbutazone. [Internet]. The United States Pharmacopeial Convention; [cited 2009 Apr 24]. Available from: http://www.usp.org/pdf/EN/veterinary/phenylbutazone.pdf/
   Google Scholar
• US Food and Drug Administration (USFDA). 2003a. New animal drugs; phenylbutazone; extralabel animal drug use; order of prohibition. [Internet]. Federal Register. 68(40):9528–9530. [cited 2009 Apr 24]. Available from: http://www.fda.gov/OHRMS/DOCKETS/98fr/03-4741.htm/
   Google Scholar
• US Food and Drug Administration (USFDA). 2003b. Guidance for Industry: Mass Spectrometry for Confirmation of the Identity of Animal Drug Residues. [Internet]; [cited 2009 Oct 2]. Available from: http://www.fda.gov/downloads/AnimalVeterinary/GuidanceComplianceEnforcement/GuidanceforIndustry/UCM052658.pdf/
   Google Scholar
• US Food and Drug Administration (USFDA). 2008. Tolerances for residues of new animal drugs in food. [Internet]. United States Food and Drug Administration, Department of Health and Human Services, Code of Federal Regulations, Title 21–Food and Drugs, Chapter 1, Part 556. [cited 2009 Apr 28]. Available from: http://www.accessdata.fda.gov/scripts/cdrh/cfdocs/cfCFR/CFRSearch.cfm?CFRPart=556&showFR=1/
   Google Scholar