Optimization and validation of a HPLC method for simultaneous determination of aflatoxin B₁, B₂, G₁, G₂, ochratoxin A and zearalenone using an experimental design

References

• Abdulkadar , AHW , Al-Ali , AA , Al-Kildi , AM and Al-Jedah , JH . 2004 . Mycotoxins in food products available in Qatar . Food Control , 15 : 543 – 548 .
   Web of Science ®Google Scholar
• Bhoop , B , Kumar , R and Ahuja , N . 2005 . Optimizing drug delivery systems using systematic “design of experiments.” Part I: fundamental aspects . Crit Rev Ther Drug Carrier Syst , 22 : 27 – 105 .
   PubMed Web of Science ®Google Scholar
• Chan , D , MacDonald , SJ , Boughtflower , V and Brereton , P . 2004 . Simultaneous determination of aflatoxins and ochratoxin A in food using a fully automated immunoaffinity column cleanup and liquid chromatography–fluorescence detection . J Chromatogr A , 1059 : 13 – 16 .
   PubMed Web of Science ®Google Scholar
• Destandau , E , Vial , J , Jardy , A , Hennion , MC , Bonnet , D and Lancelin , P . 2006 . Robustness study of a reversed-phase liquid chromatographic method for the analysis of carboxylic acids in industrial reaction mixtures . Anal Chim Acta , 572 : 102 – 112 .
   PubMed Web of Science ®Google Scholar
• European Commission. 2002. Commission regulation (EC) No. 657/2002 of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Union L. 221: 8–36
   Google Scholar
• European Commission. 2006. Commission regulation (EC) No. 401/(2006) of 23 February 2006 laying down the methods of sampling and analysis for the official control of the levels of mycotoxins in foodstuffs. Off J Eur Union L. 70/12: 19–23
   Google Scholar
• Ferracane , R , Tafuri , A , Logieco , A , Galvano , F , Balzano , D and Ritieni , A . 2007 . Simultaneous determination of aflatoxin B1 and ochratoxin A and their natural occurrence in Mediterranean virgin olive oil . Food Addit Contam , 24 : 173 – 180 .
   PubMed Web of Science ®Google Scholar
• Ferreira , SLC , Bruns , RE , Silva , EGP , Santos , WNL , Quintella , CM , David , JM , Andrade , JB , Breitkreitz , MC , Jardim , ICSF and Barros Neto , B . 2007 . Statistical designs and response surface techniques for the optimization of chromatographic systems . J Chromatogr A , 1158 : 2 – 14 .
   PubMed Web of Science ®Google Scholar
• Garcia-Villanova , RJ , Cordon , C , Gonzalez Paramas , AM , Aparicio , P and Garcia Rosales , ME . 2004 . Simultaneous immunoaffinity column clean-up and HPLC analysis of aflatoxins and ochratoxin A in Spanish bee pollen . J Agric Food Chem , 52 : 7235 – 7239 .
   PubMed Web of Science ®Google Scholar
• Garcia-Villar , N , Saurina , J and Hernandez-Cassou , S . 2006 . High-performance liquid chromatographic determination of biogenic amines in wines with an experimental design optimization procedure . Anal Chim Acta , 575 : 97 – 105 .
   PubMed Web of Science ®Google Scholar
• Ghali , R , Hmaissia-khlifa , K , Ghorbel , H , Maaroufi , K and Hedili , A . 2008 . Incidence of aflatoxins, ochratoxin A and zearalenone in tunisian foods . Food Control , 19 : 921 – 924 .
   Web of Science ®Google Scholar
• Gheshlaghi , R , Scharer , JM , Moo-Young , M and Douglas , PL . 2008 . Application of statistical design for the optimization of amino acid separation by reverse-phase HPLC . Anal Biochem , 383 : 93 – 102 .
   PubMed Web of Science ®Google Scholar
• Gilbert , J and Anklam , E . 2002 . Validation of analytical methods for determining mycotoxins in foodstuffs . Trends Anal Chem , 21 : 468 – 486 .
   Web of Science ®Google Scholar
• Göbel , R and Lusky , K . 2004 . Simultaneous determination of aflatoxins, ochratoxin A and zearalenone in grains by new immunoaffinity column/liquid chromatography . J AOAC Int , 87 : 411 – 416 .
   PubMed Web of Science ®Google Scholar
• Kazakevich , Y and LoBrutto , R . 2007 . HPLC for pharmaceutical scientists , 9 – 257 . New York : Wiley Interscience .
   Google Scholar
• Myers , R and Montgomery , DC . 2002 . Response surface methodology: Process and product optimization using designed experiment, , 2nd ed , New York : Wiley Interscience .
   Google Scholar
• Pardo , O , Yusa , V , Leon , N and Pastor , A . 2009 . Development of a method for the analysis of seven banned azo-dyes in chilli and hot chilli food samples by pressurised liquid extraction and liquid chromatography with electrospray ionization-tandem mass spectrometry . Talanta , 78 : 178 – 186 .
   PubMed Web of Science ®Google Scholar
• Rahmani , A , Jinap , S and Soleimany , F . 2009 . Qualitative and quantitative analysis of mycotoxins . Comp Rev Food Sci Food Saf , 8 : 202 – 251 .
   PubMed Web of Science ®Google Scholar
• Rahmani , A , Jinap , S and Soleimany , F . 2010 . Validation of the procedure for the simultaneous determination of aflatoxins ochratoxin A and zearalenone in cereals using HPLC-FLD . Food Addit Contam , 27 : 1683 – 1693 .
   Web of Science ®Google Scholar
• Rahmani , A , Jinap , S , Soleimany , F , Khatib , A and Tan , CP . 2011 . Sample preparation optimization for the simultaneous determination of mycotoxins in cereals , Eur Food Res Technol : 10. . doi: DOI 1007/s00217-011-1431-y
   Google Scholar
• Sangar-Tigori , B , Moukha , S , Kouadio , HJ , Betbeder , AM , Dano , DS and Creppy , EE . 2006 . Co-occurrence of aflatoxin B1, fumonisin B1, ochratoxin A and zearalenone in cereals and peanuts from Côte d’Ivoire . Food Addit Contam , 23 : 1000 – 1007 .
   PubMedGoogle Scholar
• Trucksess , MW , Weaver , CM , Oles , CJ , D’Ovidio , K and Rader , JI . 2006 . Determination of aflatoxins and ochratoxin A in ginseng and other botanical roots by immunoaffinity column cleanup and liquid chromatography with fluorescence detection . J AOAC Int , 89 : 624 – 630 .
   PubMed Web of Science ®Google Scholar
• Wang , Y , Chai , T , Lu , G , Quan , C , Duan , H , Yao , M , Zucker , BA and Schlenker , G . 2008 . Simultaneous detection of airborne aflatoxin, ochratoxin and zearalenone in a poultry house by immunoaffinity clean-up and high-performance liquid chromatography . Environ Res , 107 : 139 – 144 .
   PubMed Web of Science ®Google Scholar
• Wang , Y , Harrison , M and Clark , BJ . 2006a . Experimental design for a basic mixture on a fluorinated packing: the effect of composition of the mobile phase . J Chromatogr A , 1105 : 77 – 86 .
   PubMed Web of Science ®Google Scholar
• Wang , Y , Harrison , M and Clark , BJ . 2006b . Optimising reversed-phase liquid chromatographic separation of an acidic mixture on a monolithic stationary phase with the aid of response surface methodology and experimental design . J Chromatogr A , 1105 : 199 – 207 .
   PubMed Web of Science ®Google Scholar
• Zinedine , A , Soriano , JM , Molto , JC and Manes , J . 2007 . Review on the toxicity, occurrence, metabolism, detoxification, regulations and intake of zearalenone: An oestrogenic mycotoxin . Food Chem Toxicol , 45 : 1 – 18 .
   PubMed Web of Science ®Google Scholar