β-lactam antibiotics residues analysis in bovine milk by LC-ESI-MS/MS: a simple and fast liquid–liquid extraction method

References

• Bailón-Pérez , MI , García-Campaña , AM , del Olmo-Iruela , M , Gámiz-Gracia , L and Cruces-Blanco , C . 2009 . Trace determination of 10 β-lactam antibiotics in environmental and food samples by capillary liquid chromatography . J Chromatogr A , 47 : 8355 – 8361 .
   Web of Science ®Google Scholar
• Becker , M , Zittlau , E and Petz , M . 2004 . Residue analysis of 15 penicillins and cephalosporins in bovine muscle, kidney and muscle by liquid chromatography-tandem mass spectrometry . Analyt Chim Acta , 520 : 19 – 32 .
   Web of Science ®Google Scholar
• Bittencourt MS. 2003. Cefixima: validaçãso de métodos analíticos e estudo preliminar da estabilidade [master thesis]. Porto Alegre: Universidade Federal do Rio Grande do Sul
   Google Scholar
• European Commission . 1990 . Council Regulation (EEC) No. 2377/90 of 26 June 1990: laying down a Community procedure for the establishment of maximum residue limits of veterinary medicinal products in foodstuffs of animal origin . Off J Eur Comm , L224 : 1 – 8 .
   Google Scholar
• European Commission . 2002 . Commission Decision 2002/657/EC of 12 August 2002: implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results . Off J Eur Comm , L221 : 8 – 36 .
   Google Scholar
• Feng , Q , Zheng , WJ , Chen , GL and Qiu , SL . 2009 . Determination of six penicillins residues in milk by LC-MS/MS . Chin J Antibiot , 36 : 248 – 351 .
   Google Scholar
• Gaugain-Juhel , M , Delépine , B , Gautier , S , Fourmond , MP , Gaudin , V , Hurtaud-Pessel , D , Verdon , E and Sanders , P . 2009 . Validation of a liquid chromatography-tandem mass spectrometry screening method to monitor 58 antibiotics in milk: a qualitative approach . Food Addit Contam , 26 : 1459 – 1471 .
   Web of Science ®Google Scholar
• Kantiani , L , Farré , M , Freixedas , JMG and Barceló , D . 2010 . Development and validation of a pressurised liquid extraction liquid chromatography-electrospray-tandem mass spectrometry method for β-lactams and sulfonamides in animal feed . J Chromatogr A , 1217 : 4247 – 4254 .
   PubMed Web of Science ®Google Scholar
• Kantiani , L , Farré , M , Sibum , M , Postigo , C , Alda , ML and Barceló , D . 2009 . Fully automated analysis of β-lactams in bovine milk by online solid phase extraction-liquid chromatography-electrospray-tandem mass spectrometry . Analyt Chem , 81 : 4285 – 4295 .
   PubMed Web of Science ®Google Scholar
• Kress , C , Seidler , C , Kerp , B , Schneider , E and Usleber , E . 2007 . Experiences with an identification and quantification program for inhibitor-positive milk samples . Analyt Chim Acta , 586 ( 1–2 ) : 275 – 279 .
   PubMed Web of Science ®Google Scholar
• Mastovska , K and Lightfield , AR . 2008 . Streamlining methodology for the multiresidue analysis of β-lactam antibiotics in bovine kidney using liquid chromatography-tandem mass spectrometry . J Chromatogr A , 1202 ( 2 ) : 118 – 123 .
   PubMed Web of Science ®Google Scholar
• Mauricio , AQ , Lins , ES and Alvarenga , MB . 2009 . A national residue control plan from the analytical perspective – the Brazilian case . Analyt Chim Acta , 637 ( 1–2 ) : 333 – 336 .
   PubMed Web of Science ®Google Scholar
• Mendes , CG , Sakamoto , SM , Silva , JBA and Leite , AI . 2008 . Pesquisa de Resíduos de Beta-Lactâmicos no leite cru comercializado clandestinamente no município de Mossoró, RN, utilizando o Delvotest SP . Arquivos do Instituto de Biologia , 75 : 95 – 98 .
   Google Scholar
• Michaelidou , AM . 2008 . Factors influencing nutritional and health profile of milk and milk products . Small Ruminant Res , 79 : 42 – 50 .
   Web of Science ®Google Scholar
• Ministério da Agricultura, Pecuária e Abastecimento (MAPA). 2009. Projeções dos Agronegócios – Brasil 2008/09 a 2018/19. Brasília: MAPA. p. 30–31
   Google Scholar
• Ortelli , D , Cognard , E , Jan , P and Edder , P . 2009 . Comprehensive fast multiresidue screening of 150 veterinary drugs in milk by ultra-performance liquid chromatography coupled to time of flight mass spectrometry . J Chromatogr B , 23 : 2363 – 2374 .
   Web of Science ®Google Scholar
• Riediker , S , Rytz , A and Stadler , R . 2004 . Cold-temperature stability of five β-lactams antibiotics in bovine milk and milk extracts prepared for liquid chromatography-electrospray ionization tandem mass spectrometry analysis . J Chromatogr A , 1054 : 359 – 363 .
   PubMed Web of Science ®Google Scholar
• Stolker , AAM , Rutgers , P , Oosterink , E , Lasaroms , JJP , Peters , RBJ , van Rhijn , JA and Nielen , MWF . 2008 . Comprehensive screening and quantification of veterinary drugs in milk using UPLC-ToF-MS . Analyt Bioanalyt Chem , 391 : 2309 – 2322 .
   PubMed Web of Science ®Google Scholar
• Turnipseed , SB , Andersen , WC , Karbiwnyk , CM , Madson , MR and Miller , KE . 2008 . Multi-class, multi-residue liquid chromatography/tandem mass spectrometry and confirmation methods for drug residues in milk . Rapid Comm Mass Spectrom , 22 : 1467 – 1480 .
   PubMed Web of Science ®Google Scholar
• van Holthoon , F , Mulder , PPJ , van Bennekom , EO , Heskamp , H , Zuidema , T and van Rhijin , HA . 2010 . Quantitative analysis of penicillins in porcine tissues, milk and animal feed using derivatisation with piperidine and stable isotope dilution liquid chromatography tandem mass spectrometry . Analyt Bioanalyt Chem , 396 : 3027 – 3040 .
   PubMed Web of Science ®Google Scholar