A multi-residue method for the determination of 90 pesticides in matrices with a high water content by LC–MS/MS without clean-up

References

• Alice-Web. Sistema de Análise das Informações de Comércio Exterior [Internet]. 2008. Brasília (DF): Ministério do Desenvolvimento, Indústria e Comércio Exterior do Brasil; [cited 2010 Mar 25]. Available from: http://aliceweb.desenvolvimento.gov.br
   Google Scholar
• Anastassiades , M , Lehotay , SJ , Stajnbaher , D and Schenck , FJ . 2003 . Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce . J AOAC Int , 86 : 412 – 431 .
   PubMed Web of Science ®Google Scholar
• Bhanti , M and Taneja , A . 2007 . Contamination of vegetables of different seasons with organophosphorous pesticides and related health risk assessment in northern India . Chemosphere , 69 : 63 – 68 .
   PubMed Web of Science ®Google Scholar
• Brasil . 2009 . Jul 02. Instrução Normativa N.21 de 30 de junho de 2009 . Diário Oficial da União. Sect , 1 : 4 (col. 1)
   Google Scholar
• Brasil/Mapa . 2009 . Ministério da Agricultura, Pecuária e Abastecimento (Mapa). A força da agricultura . Brasília , : Mapa/ACS
   Google Scholar
• Cajka , T , Hajslova , J , Lacina , O , Mastovska , K and Lehotay , SJ . 2008 . Rapid analysis of multiple pesticide residues in fruit-based baby food using programmed temperature vaporiser injection-low-pressure gas chromatography-high-resolution time-of-flight mass spectrometry . J Chromatogr A , 1186 : 281 – 294 .
   PubMed Web of Science ®Google Scholar
• Chrisman , JR , Koifman , S , Sarcinelli , PN , Moreira , JC , Koifman , RJ and Meyer , A . 2009 . Pesticide sales and adult male cancer mortality in Brazil . Int J Hyg Environ Health , 212 : 310 – 321 .
   PubMed Web of Science ®Google Scholar
• Codex Alimentarius [Internet]. 2003. CAC/GL 40-1993. Guidelines on good laboratory practice in residue analysis; [cited 2011 July 13]. Available from: http://www.codexalimentarius.net
   Google Scholar
• EURACHEM . 2000 . Quantifying uncertainty in analytical measurement, , 2nd , Berlin : EURACHEM/CITAC .
   Google Scholar
• European Commission . 2009 . Method validation and quality control procedures for pesticide residues analysis in food and feed. DG-SANCO, Document no. SANCO/10684/2009 , Brussels : European Commission .
   Google Scholar
• Faostat: FAO Statistics [Internet]. 2008. Food and Agriculture Organization of the United Nations; [cited 2010 Mar 25]. Available from: http://faostat.fao.org
   Google Scholar
• Hiemstra , M and de Kok , A . 2007 . Comprehensive multi-residue method for the target analysis of pesticides in crops using liquid chromatography–tandem mass spectrometry . J Chromatogr A , 1154 : 3 – 25 .
   PubMed Web of Science ®Google Scholar
• Húsková , R , Matisová , E and Kirchner , M . 2008 . Fast GC-MS pesticide multiresidue analysis of apples . Chromatographia , 68 ( suppl ) : S49 – S55 .
   Web of Science ®Google Scholar
• Klinsunthorn , N , Petsom , A and Nhujak , T . 2011 . Determination of steroids adulterated in liquid herbal medicines using QueChERS sample preparation and high-performance liquid chromatography . J Pharm Biomed Anal , 55 : 1175 – 1178 .
   PubMed Web of Science ®Google Scholar
• Kméllar , B , Fodor , P , Pareja , L , Ferrer , C , Martínez-Uroz , MA , Valverde , A and Fernandez-Alba , AR . 2008 . Validation and uncertainty study of a comprehensive list of 160 pesticide residues in multi-class vegetables by liquid chromatography–tandem mass spectrometry . J Chromatogr A , 1215 : 37 – 50 .
   PubMed Web of Science ®Google Scholar
• Lee , SJ , Park , HJ , Kim , W , Jin , JS , El-Aty , AMA , Shim , JH and Shin , SC . 2008 . Multiresidue analysis of 47 pesticides in cooked wheat flour and polished rice by liquid chromatography with tandem mass spectrometry . Biomed Chromatogr , 23 : 434 – 442 .
   Web of Science ®Google Scholar
• Mauricio , AQ , Lins , E and Alvarenga , MB . 2009 . A national residue control plan from the analytical perspective – The Brazilian case . Anal Chim Acta , 637 : 333 – 336 .
   PubMed Web of Science ®Google Scholar
• Meyer , PC and Zünd , RE . 2000 . Statistical methods in analytical chemistry, , 2nd , New York : Wiley .
   Google Scholar
• Mol , HGJ , Plaza-Bolaños , P , Zomer , P , de Rijk , TC , Stolker , AAM and Mulder , PPJ . 2008 . Towards a generic extraction method for simultaneous determination of pesticides, mycotoxins, plant toxins, and veterinary drugs in feed and food matrixes . Anal Chem , 80 : 9450 – 9459 .
   PubMed Web of Science ®Google Scholar
• Pizzutti , IR , de Kok , A , Hiemstra , M , Wickert , C and Prestes , OD . 2009 . Method validation and comparison of acetonitrile and acetone extraction for the analysis of 169 pesticides in soya grain by liquid chromatography–tandem mass spectrometry . J Chromatogr A , 1216 : 4539 – 4552 .
   PubMed Web of Science ®Google Scholar
• Pizzutti , IR , de Kok , A , Zanella , R , Adaime , MB , Hiemstra , M , Wickert , C and Prestes , OD . 2007 . Method validation for the analysis of 169 pesticides in soya grain, without clean up, by liquid chromatography–tandem mass spectrometry using positive and negative electrospray ionization . J Chromatogr A , 1142 : 123 – 136 .
   PubMed Web of Science ®Google Scholar
• Prestes , OD , Friggi , CA , Adaime , MB and Zanella , R . 2009 . Quechers – a modern sample preparation method for pesticide multiresidue determination in food by chromatographic methods coupled to mass spectrometry . Química Nova , 32 : 1620 – 1634 .
   Web of Science ®Google Scholar
• Quackenbush , R , Hackley , B and Dixon , J . 2006 . Screening for pesticide exposure: A case study . J Midwif Women's Health , 51 : 3 – 11 .
   PubMed Web of Science ®Google Scholar
• Romero-González , R , Frenich , AG and Martínez-Vidal , JL . 2008 . Multiresidue method for fast determination of pesticides in fruit juices by ultra performance liquid chromatography coupled to tandem mass spectrometry . Talanta , 76 : 211 – 225 .
   PubMed Web of Science ®Google Scholar
• Souza , SVC and Junqueira , RGAJ . 2005 . Procedure to assess linearity by ordinary least squares method . Anal Chim Acta , 552 : 25 – 35 .
   Web of Science ®Google Scholar
• Stubbings , G and Bigwood , T . 2009 . The development and validation of a multiclass liquid chromatography tandem mass spectrometry (LC–MS/MS) procedure for the determination of veterinary drug residues in animal tissue using a QuEChERS (QUick, Easy, Cheap, Effective, Rugged and Safe) approach . Anal Chim Acta , 637 : 68 – 78 .
   PubMed Web of Science ®Google Scholar
• Tamura , M , Uyama , A and Mochizuki , N . 2011 . Development of a multi-mycotoxin analysis in beer-based drinks by a modified QuEChERS method and ultra-high-performance liquid chromatography coupled with tandem mass spectrometry . Anal Sci , 27 : 629 – 635 .
   PubMed Web of Science ®Google Scholar
• Venkateswarlu , P , Mohan , KR , Kumar , CR and Seshaiah , K . 2007 . Monitoring of multi-class pesticide residues in fresh grape samples using liquid chromatography with electrospray tandem mass spectrometry . Food Chem , 105 : 1760 – 1766 .
   Web of Science ®Google Scholar