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Food Additives & Contaminants: Part A Volume 29, 2012 - Issue 4: Ministério da Agricultura, Pecuária e Abastecimento do Brasil – Laboratórios Nacionais Agropecuários: Methods of analysis for residues and contaminants in the food chain
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Original Articles

Optimisation and validation of a quantitative and confirmatory LC-MS method for multi-residue analyses of β-lactam and tetracycline antibiotics in bovine muscle

C.P. Rezende Ministry of Agriculture, Livestock and Food Supply, MAPA, National Agricultural Laboratory, LANAGRO/MG, BrazilCorrespondence[email protected]
,
M.P. Almeida Ministry of Agriculture, Livestock and Food Supply, MAPA, National Agricultural Laboratory, LANAGRO/MG, Brazil
,
R.B. Brito Ministry of Agriculture, Livestock and Food Supply, MAPA, National Agricultural Laboratory, LANAGRO/MG, Brazil
,
C.K. Nonaka Bolsista CNPq, National Agricultural Laboratory, LANAGRO/MG, Brazil
&
M.O. Leite Veterinary School of Federal University of Minas Gerais – UFMG, Belo Horizonte/MG, 31270-901, Brazil
Pages 541-549 | Received 23 Nov 2010, Accepted 31 Aug 2011, Published online: 10 Nov 2011

References

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  • Fagerquist , CK , Lightfield , AR and Lehotay , SJ . 2005 . Confirmatory and quantitative analysis of β-lactam antibiotic in bovine kidney tissue by dispersive solid-phase extraction and liquid chromatography-tandem mass spectrometry . Analyt. Chem , 77 : 1473 – 1482 .
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  • Holthoon , FV , Mulder , PPJ , Bennekom , EOV , Heskamp , H , Zuidema , T and Rhijn , HJAV . 2010 . Quantitative analysis of penicillins in porcine tissues, milk and animal feed using derivatisation with piperidine and stable isotope dilution liquid chromatography tandem mass spectrometry . Analyt Bioanalyt Chem , 396 : 3027 – 3040 .
  • Msagati , TAM and Nindi , MM . 2007 . Determination of β-lactam residues in food stuffs of animal origin using supported liquid membrane extraction and liquid chromatography-mass spectrometry . Food Chem , 100 : 836 – 844 .
  • Riediker , S , Rytz , A and Stadler , RH . 2004 . Cold-temperature stability of five β-lactam antibiotics in bovine milk and milk extracts prepared for liquid chromatography-electrospray ionization tandem mass spectrometry analysis . J Chromatogr A , 1054 : 359 – 363 .
  • Souza , SVC . 2007. Procedimento para validação intralaboratorial de métodos de ensaio: delineamento e aplicabilidade em análise de alimentos. Tese de doutorado. Belo Horizonte/MG, Brazil

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