Advanced search
Publication Cover
Food Additives & Contaminants: Part A Volume 29, 2012 - Issue 4: Ministério da Agricultura, Pecuária e Abastecimento do Brasil – Laboratórios Nacionais Agropecuários: Methods of analysis for residues and contaminants in the food chain
Submit an article Journal homepage
230
Views
13
CrossRef citations to date
0
Altmetric
Original Articles

A multi-residue method for the determination of pesticides in high water content matrices by gas chromatography–single quadrupole mass spectrometry with electron ionisation (EI-GC/MS)

Mauro Lúcio Gonçalves de Oliveira Laboratório Nacional Agropecuário – LANAGRO/MG, Ministry of Agriculture, Livestock and Food Supply of Brazil, Pesticides Laboratory, Av. Rômulo Joviano s/n – Fazenda Modelo, Postal Code: 33.600-000, Pedro Leopoldo-MG/BrazilCorrespondence[email protected]
,
Fernando Diniz Madureira Laboratório Nacional Agropecuário – LANAGRO/MG, Ministry of Agriculture, Livestock and Food Supply of Brazil, Pesticides Laboratory, Av. Rômulo Joviano s/n – Fazenda Modelo, Postal Code: 33.600-000, Pedro Leopoldo-MG/Brazil
,
Fabiano Aurélio Laboratório Nacional Agropecuário – LANAGRO/MG, Ministry of Agriculture, Livestock and Food Supply of Brazil, Pesticides Laboratory, Av. Rômulo Joviano s/n – Fazenda Modelo, Postal Code: 33.600-000, Pedro Leopoldo-MG/Brazil
,
Ana Paula Pontelo Laboratório Nacional Agropecuário – LANAGRO/MG, Ministry of Agriculture, Livestock and Food Supply of Brazil, Pesticides Laboratory, Av. Rômulo Joviano s/n – Fazenda Modelo, Postal Code: 33.600-000, Pedro Leopoldo-MG/Brazil
,
Gilsara Silva Laboratório Nacional Agropecuário – LANAGRO/MG, Ministry of Agriculture, Livestock and Food Supply of Brazil, Pesticides Laboratory, Av. Rômulo Joviano s/n – Fazenda Modelo, Postal Code: 33.600-000, Pedro Leopoldo-MG/Brazil
,
Reginaldo Oliveira Laboratório Nacional Agropecuário – LANAGRO/MG, Ministry of Agriculture, Livestock and Food Supply of Brazil, Pesticides Laboratory, Av. Rômulo Joviano s/n – Fazenda Modelo, Postal Code: 33.600-000, Pedro Leopoldo-MG/Brazil
&
Cláudia Paes Laboratório Nacional Agropecuário – LANAGRO/MG, Ministry of Agriculture, Livestock and Food Supply of Brazil, Pesticides Laboratory, Av. Rômulo Joviano s/n – Fazenda Modelo, Postal Code: 33.600-000, Pedro Leopoldo-MG/Brazil
 show all
Pages 657-664 | Received 26 Nov 2010, Accepted 07 Nov 2011, Published online: 01 Feb 2012

References

  • [ABNT] ABNT, INMETRO, ISO, GUM. 2003. Guide to the expression of uncertainty in measurement. 2a ed. Brazilian Association of Technical Standards
  • [ABNT] ABNT, NBR, ISO/IEC 17025. 2005. General requirements for the competence of calibration and testing laboratories. Brazilian Association of Technical Standards
  • Bitencourt R. 2007. Uncertainty in chemical analysis: alternative approaches. Portugal: National Institute of Biological Resources. Pesticide Residue Laboratory/Directorate General for Crop Protection [LRP/DGPC]
  • [BRAZIL] Ministry of Agriculture, Livestock and Supply. 2009. National Plan of residues and contaminants in vegetal products. Normative instruction no. 21
  • [EA] European Co-operation for Accreditation. 2003. EA 4/16 guidelines on the expression of uncertainty in quantitative testing. EA Laboratory Committee
  • Ellison , SLR and Barwick , VJ . 1998 . Estimating measurement uncertainty: reconciliation using a cause and effect approach . Accred. Qual. Assur , 3 : 101 – 105 .
  • Eurachem/CITAC Guide. 2000. Quantifying uncertainty in analytical measurement. 2nd ed
  • [INMETRO] National Institute of Metrology, Standardization and Industrial Quality. 2010a. Guidelines on validation of analytical methods. DOQ-CGCRE-008
  • [INMETRO] National Institute of Metrology, Standardization and Industrial Quality. 2010b. Expression of uncertainty in measurement. Brazilian version of the document EA-4/02 Expression of Uncertainty of Measurement in Calibration. NIT-DICLA-021
  • [IPAC] Portuguese Institute for Accreditation. 2005. Guidelines for the accreditation of chemicals laboratories. Normative OGC002
  • [IPAC] Portuguese Institute for Accreditation. 2007. Guide to uncertainty measurement in chemical testing. Normative OGC007
  • Miller , JN and Miller , JC . 2002 . Statistics for analytical chemistry, , 4th , New York : Prentice Hall .
  • Pang , GF , Fan , CL , Liu , YM , Cao , YZ , Zhang , JJ , Fu , BL , Li , XM , Li , ZY and Wu , YP . 2006 . Multi-residue method for determination of 450 pesticide residues in honey, fruit juice and wine by double-cartridge solid-phase extraction/gas chromatography-mass spectrometry and liquid chromatography-tandem mass spectrometry . Food Addit Contam , 23 ( 8 ) : 777 – 810 .
  • Patel , K , Fussell , RJ , Macarthur , R , Goodall , DM and Keely , BJ . 2004 . Method validation of resistive heating-gas chromatography with flame photometric detection for the rapid screening of organophosphorus pesticides in fruit and vegetables . J Chromatogr A , 1046 ( 1 ) : 225 – 234 .
  • [SANCO] European Commission. 2009. Method validation and quality control procedures for pesticide residues analysis in food and feed. Document No. SANCO/10684/2009
  • Thompson MSLR, Ellison A, Fajgelj P, Willetts RW. 2000. Harmonised guidelines for the use of recovery information in analytical measurement. IUPAC/ISO/AOAC International/Eurachem
  • [WHO] World Health Organisation . 2003 . Guidelines on good laboratory practice in residue analysis CAC/GL 40-1993 (rev. 1) , Rome (Italy) : FAO/WHO .
  • [WHO] World Health Organisation . 2005 . Guidelines on the use of mass spectrometry (MS) for identification, confirmation and quantitative determination of residues CAC/GL 56-2005 , Rome (Italy) : FAO/WHO .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Order Reprints Request Corporate Permissions

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

Request Academic Permissions

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.

Related research

People also read lists articles that other readers of this article have read.

Recommended articles lists articles that we recommend and is powered by our AI driven recommendation engine.

Cited by lists all citing articles based on Crossref citations.
Articles with the Crossref icon will open in a new tab.