188
Views
6
CrossRef citations to date
0
Altmetric
Original Articles

In-house validation and factorial effect analysis of a LC-MS/MS method for the determination of steroids in bovine and porcine blood plasma

&
Pages 1027-1036 | Received 28 Aug 2012, Accepted 17 Feb 2013, Published online: 08 May 2013

References

  • Biancotto G, Angeletti R, Traldi P, Silvestri M, Saccon M, Guidugli F. 2002. Determination of 17beta-estradiol in bovine plasma: development of a highly sensitive technique by ion trap gas chromatography-tandem mass spectrometry using negative chemical ionization. J Mass Spectrom. 37:1266–1271.
  • Chen G, Ren L, Yang SM, Qiu J, Kamal-Eldin A, Lundström K. 2010. Determination of androstenone levels in porcine plasma by LC-MS/MS. Food Chem. 122:1278–1282.
  • De Brabander HF, Noppe H, Verheyden K, Vanden Bussche J, Wille K, Okerman L, Vanhaecke L, Reybroeck W, Ooghe S, Croubels S. 2009. Residue analysis: future trends from a historical perspective. J Chrom A. 1216:7964–7976, and references cited.
  • EURACHEM. 2002. EURACHEM, EURACHEM/CITAC guide. 2nd ed. ISBN 0948926 15 5.
  • European Commission. 2009. Commission Staff Working Document on the Implementation of National Residue Monitoring Plans in the member states 2000–2009. [Internet]. [cited 2013 Apr 10]. Available from: http://ec.europa.eu/food/food/chemicalsafety/residues/control_en.htm
  • European Union. 1996a. Council Directive 96/22/EC of 29 April 1996 concerning the prohibitionon the use in stockfarming of certain substances having a hormonal or thyreostatic action and of beta-agonists (1996). Off J Eur Commun. 1996 L 125:3–9, including its amending Directive 2003/74/EC concerning the prohibition on the use in stockfarming of certain substances having a hormonal or thyreostatic action and of beta-agonists.
  • European Union. 1996b. Council Directive 96/23/EC of 29 April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products (1996). Off J Eur Commun. 1996 L 125:10–32.
  • European Union. 2002. Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results (2002). Off J Eur Commun. L221:8.
  • European Union. 2004. Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 on official controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules (2004). Off J Eur Commun. L 165:1–141.
  • European Union. 2008. Document SANCO 2726/2004 rev. 4. Guidelines for the Implementation of Decision 2002/657/EC. [Internet]. [cited 2013 Apr 10] Available from: http://ec.europa.eu/food/food/chemicalsafety/residues/guidelines_2002-657.pdf
  • Gowik P, Polzer J, Uhlig S. 2007. Reference material in residue control: assessment of matrix effects. Accred Qual Assur. 12:161–166.
  • Jülicher B, Gowik P, Uhlig S. 1998. Assessment of detection methods in trace analysis by means of a statistically based in-house validation concept. Analyst. 123:173–179.
  • Jülicher B, Gowik P, Uhlig S. 1999. A top-down in-house validation based approach for the investigation of the measurement uncertainty using fractional factorial experiments. Analyst. 124:537–545.
  • Lone KP. 1997. Natural sex steroids and their xenobiotic analogs in animal production: growth, carcass quality, pharmacokinetics, metabolism, mode of action, residues, methods, and epidemiology. Crit Rev Food Sci Nutr. 37:93–209.
  • Schmidt K, Stachel C, Gowik P. 2008. Development and in-house validation of an LC-MS/MS method for the determination of stilbenes and resorcylic acid lactones in bovine urine. Anal Bioanal Chem. 391:1199–1210.
  • Schmidt KS, Stachel CS, Gowik P. 2009. In-house validation and factorial effect analysis of a liquid chromatography-tandem mass spectrometry method for the determination of steroids in bovine muscle. Anal Chim Acta. 637:156–164.
  • Stolker AAM, Groot MJ, Lasaroms JJP, Nijrolder AWJM, Blokland MH, Riedmaier I, Becker C, Meyer HHD, Nielen MWF. 2009. Detectability of testosterone esters and estradiol benzoate in bovine hair and plasma following pour-on treatment. Anal Bioanal Chem. 395:1075–1087.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.