527
Views
30
CrossRef citations to date
0
Altmetric
Original Articles

Graphene as dispersive solidphase extraction materials for pesticides LC-MS/MS multi-residue analysis in leek, onion and garlic

, , , &
Pages 250-261 | Received 04 Jul 2013, Accepted 10 Nov 2013, Published online: 22 Jan 2014

References

  • Anagnostopoulos C, Miliadis GE. 2013. Development and validation of an easy multiresidue method for the determination of multiclass pesticide residues using GC-MS/MS and LC-MS/MS in olive oil and olives. Talanta. 112:1–10.
  • Anastassiades M, Lehotay SJ, Šttajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce. J AOAC Int. 86:412–431.
  • Berrada H, Font G, Molto JC. 2004. Application of solid-phase microextraction for determining phenylurea herbicides and their homologous anilines from vegetables. J Chromatogr A. 1042:9–14.
  • Blasco C, Pico Y, Manes J, Font G. 2002. Determination of fungicide residues in fruits and vegetables by liquid chromatography–atmospheric pressure chemical ionization mass spectrometry. J Chromatogr A. 947:227–235.
  • Cai Y, Cai Y, Mou S, Lu Y. 2005. Multi-walled carbon nanotubes as a solid-phase extraction adsorbent for the determination of chlorophenols in environmental water samples. J Chromatogr A. 1081:245–247.
  • Cao XW, Shen WJ, Jiang Y, Zhao ZY, Wu B, Yu KY, Liu H, Lian HZ. 2011. Determination of 17 pyrethroid residues in troublesome matrices by gas chromatography/mass spectrometry with negative chemical ionization. Talanta. 84:141–147.
  • Deng XJ, Lu LL, Li HW, Luo F. 2012. The adsorption properties of Pb(II) and Cd(II) on functionalized graphene prepared by electrolysis method. J Hazard Mater. 183:923–930.
  • Du D, Wang M, Zhang J, Cai J, Tu H, Zhang A. 2008. Application of multiwalled carbon nanotubes for solid-phase extraction of organophosphate pesticide. Electrochem Commun. 10:85–89.
  • El-Sheikh AH, Insisi AA, Sweileh JA. 2007. Effect of oxidation and dimensions of multi-walled carbon nanotubes on solid phase extraction and enrichment of some pesticides from environmental waters prior to their simultaneous determination by high performance liquid chromatography. J Chromatogr A. 1164:25–32.
  • Ershova OV, Lillestolen TC, Bichoutskaia E. 2010. Study of polycyclic aromatic hydrocarbons adsorbed on graphene using density functional theory with empirical dispersion correction. Phys Chem Chem Phys. 12:6483–6491.
  • European Commission, Directorate General Health and Consumer Protection. 2010. Guidance Document on Method Validation and Quality Control Procedures for Pesticide Residues Analyses in Food and Feed; SANCO/10684/2009. Brussels (Belgium): European Commission.
  • Guan WB, Li ZN, Zhang HY, Hong HJ, Rebeyev N, Ye Y, Ma YQ. 2013. Amine modified graphene as reversed-dispersive solid phase extraction materials combined with liquid chromatography-tandem mass spectrometry for pesticide multi-residue analysis in oil crops. J Chromatogra A. 1286:1–8.
  • Guan WB, Xu PJ, Wang K, Song Y, Zhang HY. 2011. Determination and study on dissipation of 1-naphthylacetic acid in garlic and soil using high performance liquid chromatography-tandem mass spectrometry. Food Chem Toxicol. 49:2869–2874.
  • Gupta SS, Sreeprasad TS, Maliyekkal SM, Das SK, Pradeep T. 2012. Graphene from sugar and its application in water purification. ACS Appl Mater Interfaces. 4:4156–4163.
  • Hou XL, Li JL, Drew SC, Tang B, Sun L, Wang XG. 2013. Tuning radical species in graphene oxide in aqueous solution by photoirradiation. J Phys Chem C. 117:6788–6793.
  • Hua J, Guo Z, Glasiusc M, Kristensenc K, Xiao L, Xu X. 2011. Pressurized liquid extraction of ginger (Zingiber officinale Roscoe) with bioethanol: an efficient and sustainable approach. J Chromatogr A. 1218:5765–5773.
  • Hummers WS, Offeman RE, Am J. 1958. A new structure model of graphite oxide. J Am Chem Soc. 80:1339–1348.
  • Koesukwiwat U, Ehotay SJ, Mastovska K, Dorweiler KJ, Leepipatpiboon N. 2010. Extension of the QuEChERS method for pesticide residues in cereals to flaxseeds, peanuts, and doughs. J Agric Food Chem. 58:5950–5958.
  • Lagunas-Allué L, Sanz-Asensio J, Martínez-Soria MT. 2012. Comparison of four extraction methods for the determination of fungicide residues in grapes through gas chromatography–mass spectrometry. J Chromatogr A. 1270:62–71.
  • Lehotay SJ. 2007. Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study. J AOAC Int. 90:485–520.
  • Li Y, Zhang P, Du Q, Peng X, Liu T, Wang Z, Xia Y, Zhang W, Wang K, Zhu H, et al. 2011. Adsorption of fluoride from aqueous solution by graphene. J Colloid Interface Sci. 363:348–354.
  • Liu Q, Shi JB, Sun JT, Wang T, Zeng LX, Jiang GB. 2011. Graphene and graphene oxide sheets supported on silica as versatile and high-performance adsorbents for solid-phase extraction. Angew Chem Int Ed. 50:5913–5917.
  • Liu X, Guan WB, Hao XH, Wu XL, Ma YQ, Pan CP. 2014. Pesticide multi-​residue analysis in tea using d-SPE sample cleanup with graphene mixed with primary secondary amine and graphitized carbon black prior to LC-MS/MS. Chromatographia. 77:31–37.
  • Liu XT, Zhang HY, Ma YQ, Wu XL, Meng LX, Guo YL, Yu G, Liu YQ. 2012. Graphene-coated silica as a highly efficient sorbent for residual organophosphorus pesticides in water. J Mater Chem A. 1:1875–1879.
  • Liu Z, Robinson JT, Sun XM, Dai HJ. 2008. PEGylated nanographene oxide for delivery of water-insoluble cancer drugs. J Am Chem Soc. 130:10876–10877.
  • Ma XD, Li CJ, Tao CJ, Liu W, Zheng SS. 2001. Multi-residue determination of 41 insecticides in garlic by gas chromatography and ion trap mass spectrometry using the selective ion storage technique. Rapid Commun Mass Spectrom. 15:15–19.
  • Maliyekkal SM, Sreeprasad TS, Krishnan D, Kouser S, Mishra AK, Waghmare UV, Pradeep T. 2012. Graphene: a reusable substrate for unprecedented adsorption of pesticides. Small. 7:1876–1881.
  • Oyer AJ, Carrillo JMY, Hire CC, Schniepp HC, Asandei AD, Dobrynin AV, Adamson DH. 2012. Stabilization of graphene sheets by a structured benzene/hexafluorobenzene mixed solvent. J Am Chem Soc. 134:5018–5021.
  • Qu LJ, Zhang H, Zhu JH, Yang GS, Aboul-Enein HY. 2010. Rapid determination of organophosphorous pesticides in leeks by gas chromatography-triple quadrupole mass spectrometry. Food Chem. 122:327–332.
  • Qu LT, Liu Y, Baek JB, Dai L. 2010. Nitrogen-doped graphene as efficient metal-free electrocatalyst for oxygen reduction in fuel cells. ACS Nano. 4:1321–1326.
  • Ramesha GK, Kumara AV, Muralidhara HB, Sampath S. 2011. Graphene and graphene oxide as effective adsorbents toward anionic and cationic dyes. J. Colloid Interface Sci. 361:270−277.
  • Rao CNR, Sood AK, Subrahmanyam KS, Govindaraj A. 2009. Graphene: the new two-dimensional nanomaterial. Angew Chem Int Ed. 48:7752–7777.
  • Ravelo-Perez LM, Hernandez-Borges J, Rodríguez-Delgado M. 2008. Multi-walled carbon nanotubes as efficient solid-phase extraction materials of organophosphorus pesticides from apple, grape, orange and pineapple fruit juices. J Chromatogr A. 1211:33–42.
  • Song B, Li D, Qi WP, Elstner M, Fan CH, Fang HP. 2011. Graphene on Au(111): a highly conductive material with excellent adsorption properties for high-resolution bio/nanodetection and identification. ChemPhysChem. 11:585–589.
  • Song SL, Ma XD, Li CJ. 2007. Multi-residue determination method of pesticides in leek by gel permeation chromatography and solid phase extraction followed by gas chromatography with mass spectrometric detector. Food Contr. 18:448–453.
  • Su R, Wang X, Xu X, Wang Z, Li D, Zhao X, Li X, Zhang H, Yu A. 2010. Application of multiwall carbon nanotubes-based matrix solid phase dispersion extraction for determination of hormones in butter by gas chromatography mass spectrometry. J Chromatogr A. 1218:5047–5054.
  • Ueno E, Oshima H, Saito I, Matsumoto H, Nakazawa H. 2003. Determination of organophosphorus pesticide residues in onion and welsh onion by gas chromatography with pulsed flame photometric detector. J Pestic Sci. 28:422–428.
  • Varghese N, Mogera U, Govindaraj A, Das A, Maiti PK, Sood AK, Rao CNR. 2009. Binding of DNA nucleobases and nucleosides with graphene. ChemPhysChem. 10:206.
  • Wang JH, Xu QA, Jiao K. 1998. Supercritical fluid extraction and off-line clean-up for the analysis of organochlorine pesticide residues in garlic. J Chromatogr A. 818:138–143.
  • Wang L, Zhao H, Qiu Y, Zhou Z. 2006. Determination of four benzodiazepine residues in pork using multiwalled carbon nanotube solid-phase extraction and gas chromatography-mass spectrometry. J Chromatogr A. 1136:99–105.
  • Wu S, Lan XQ, Cui LJ, Zhang LH, Tao SY, Wang HN, Han M, Liu ZG, Meng CG. 2011. Application of graphene for preconcentration and highly sensitive stripping voltammetric analysis of organophosphate pesticide. Analytica Chimica Acta. 699:170–176.
  • Wu XL, Zhang HY, Meng LX, Liu XT, Ma YQ. 2012. Graphene for cleanup in trace analysis of pyrethroid insecticides in cucumber and spinach. Chromatographia. 75:1177–1183.
  • Xu J, Wang L, Zhu YF. 2012. Decontamination of bisphenol A from aqueous solution by graphene adsorption. Langmuir. 28:8418–8425.
  • Ye SB, Feng JC, Wu PY. 2013. Highly elastic graphene oxide–epoxy composite aerogels via simple freeze-drying and subsequent routine curing. J Mater Chem A. 1:3495–3502.
  • Zhang H, Chen Z, Yang G, Wang W, Li X, Li R, Wu Y. 2008. Microwave pretreatment and gas chromatography–mass spectrometry determination of herbicide residues in onion. Food Chem. 108:322–328.
  • Zhao PY, Wang L, Jiang YP, Zhang FZ, Pan CP. 2012. Dispersive cleanup of acetonitrile extracts of tea samples by mixed multiwalled carbon nanotubes, primary secondary amine, and graphitized carbon black sorbents. J Agric Food Chem. 60:4026–4033.
  • Zhu J, Wei S, Gu H, Rapole SB, Wang Q, Luo Z, Haldolaarachchige N, Young DP, Guo Z. 2012. One-pot synthesis of magnetic graphene nanocomposites decorated with core@double-shell nanoparticles for fast chromium removal. Environ Sci Technol. 46:977–985.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.