276
Views
13
CrossRef citations to date
0
Altmetric
Original Articles

Investigation of the presence of prednisolone in bovine urine

, , , , &
Pages 605-613 | Received 19 Aug 2013, Accepted 18 Dec 2013, Published online: 03 Mar 2014

References

  • Annual Report of the Belgian Hormone Commission. 2011. Multidisciplinary Belgian Hormone Commission. [Internet]. [cited 2013 Aug 15]. Available from: http://issuu.com/fedpolbelgium/docs/jaarverslag_mdhc_2011
  • Antignac JP, Le Bizec B, Monteau F, André F. 2002. Study of natural and artificial corticosteroid phase II metabolites in bovine urine using HPLC-MS/MS. Steroids. 67:873–882.
  • Arioli F, Fidani M, Casati A, Fracchiolla ML, Pompa G. 2010. Investigation on possible transformations of cortisol, cortisone and cortisol glucuronide in bovine faecal matter using liquid chromatography–mass spectrometry. Steroids. 75:350–354.
  • Arioli F, Gavinelli MP, Fracchiolla ML, Casati A, Fidani M, Ferrer E, Pompa G. 2008. Evaluation of boldenone formation and related steroids transformations in veal faeces by liquid chromatography/tandem mass spectrometry. Rapid Commun Mass Spectrom. 22:217–223.
  • Baiocchi C, Brussino M, Pazzi M, Medana C, Marini C, Genta E. 2003. Separation and determination of synthetic corticosteroids in bovine liver by LC-ion-trap-MS-MS on porous graphite. Chromatographia. 58:11–14.
  • Blokland MH, van Rossum HJ, Sterk SS, van Ginkel LA, Stephany RW. 2007. Development of a method which discriminates between endogenous and exogenous β-boldenone. Anal Chim Acta. 586:147–153.
  • Bredehöft M, Baginski R, Parr MK, Thevis M, Schänzer W. 2010. Investigations of the microbial transformation of cortisol to prednisolone in urine samples. J Steroid Biochem Mol Biol. 129:54–60.
  • Cannizzo FT, Capra P, Divari S, Ciccotelli V, Biolatti B, Vincenti M. 2011. Effects of low-dose dexamethasone and prednisolone long term administration in beef calf: chemical and morphological investigation. Anal Chim Acta. 700:95–104.
  • Commission Decision 2002/657/EC. Commission Decision of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results [Internet]. [cited 2013 Aug 15]. Available from: http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2002:221:0008:0036:EN:PDF
  • European Union. 2009. Commission regulation (EU) No 37/2010 of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin. Off J Eur Union. L15:1–72.
  • European Union. 1996. Council Directive 96/23/EC of 29 April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products and repealing Directives 85/358/EEC and 86/469/EEC and Decisions 89/187/EEC and 91/664/EEC. Available from: http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=CONSLEG:1996L0023:20090807:EN:PDF
  • Courtheyn D, LeBizec B, Brambilla G, De Brabander HF, Cobbaert E, Van de Wiele M, Vercammen J, DeWasch K. 2002. Recent developments in the use and abuse of growth promoters. Anal Chim Acta. 473:71–82.
  • CRL 2007. CRLs view on state of the art analytical methods for national residue control plans. [Internet; cited 2013 Aug 15]. Available from: http://www.bvl.bund.de/SharedDocs/Downloads/09_Untersuchungen/EURL_Empfehlungen_Konzentrationsauswahl_Methodenvalierungen.pdf?__blob=publicationFile
  • Dusi G, Gasparini M, Curatolo M, Assini W, Bozzoni E, Tognoli N, Ferretti E. 2011. Development and validation of a liquid chromatography–tandem mass spectrometry method for the simultaneous determination of nine corticosteroid residues in bovine liver samples. Anal Chim Acta. 700:49–57.
  • European Commission Staff Working Document. 2010. Commission staff working document on the implementation of national residue monitoring plans in the member states in 2010 (Council Directive 96/23/EC) [Internet]. [cited 2013 Aug 15]. Available from: http://ec.europa.eu/food/food/chemicalsafety/residues/docs/workdoc_2010_en.pdf
  • Ferranti C, delli Quadria F, Palleschi L, Marchiafava C, Pezzolato M, Bozzetta E, Caramelli M, Draiscia R. 2011. Studies on the presence of natural and synthetic corticosteroids in bovine urine. Steroids. 76:616–625.
  • Fidani M, Pompa G, Mungiguerra F, Casati A, Fracchiolla ML, Arioli F. 2012. Investigation of the presence of endogenous prednisolone in equine urine by high-performance liquid chromatography mass spectrometry and high-resolution mass spectrometry. Rapid Commun Mass Spectrom. 26:879–886.
  • Garg V, Jusko WJ. 1991. Simultaneous analysis of prednisone, prednisolone and their major hydroxylated metabolites in urine by high-performance liquid chromatography. J Chromatogr B. 567:39–47.
  • Möstl E, Maggs JL, Schrötter G, Besenfelder U, Palme R. 2002. Measurement of cortisol metabolites in faeces of ruminants. Vet Res Commun. 26:127–139.
  • Möstl E, Messmann S, Bagu E, Robia C, Palme R. 1999. Measurement of glucocorticoid metabolite concentrations in faeces of domestic livestock. Zentralblatt fur Veterinarmedizin Reihe A. 46:621–631.
  • Palme R, Fischer P, Schildorfer H, Ismail MN. 1996. Excretion of infused C-14-steroid hormones via faeces and urine in domestic livestock. Anim Reprod Sci. 43:43–63.
  • Pompa G, Arioli F, Casati A, Fidani M, Bertocchi L, Dusi G. 2011. Investigation of the origin of prednisolone in cow urine. Steroids. 76:104–110.
  • Rijk JCW, Bovee TFH, Groot MJ, Peijnenburg AAC, Nielen MWF. 2008. Evidence of the indirect hormonal activity of prohormones using liver S9 metabolic bioactivation and an androgen bioassay. Anal Bioanal Chem. 392:417–425.
  • Vincenti M, Leporati M, Capra P, Gatto AA, Barbarino G, Nebbia C. 2012. A field survey on the presence of prednisolone and prednisone in urine samples from untreated cows. Food Addit Contam Part A. 29:1–8.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.