Simultaneous determination of 30 hormones illegally added to anti-ageing functional foods using UPLC-MS/MS coupled with SPE clean-up

References

• Abdel-Khalik J, Björklund E, Hansen M. 2013. Simultaneous determination of endogenous steroid hormones in human and animal plasma and serum by liquid or gas chromatography coupled to tandem mass spectrometry. J Chromatogr B. 928:58–77.
   PubMed Web of Science ®Google Scholar
• Backe WJ, Ort C, Brewer AJ, Field JA. 2011. Analysis of androgenic steroids in environmental waters by large-volume injection liquid chromatography tandem mass spectrometry. Anal Chem. 83:2622–2630.
   PubMed Web of Science ®Google Scholar
• Blasco C, Poucke CV, Peteghem CV. 2007. Analysis of meat samples for anabolic steroids residues by liquid chromatography/tandem mass spectrometry. J Chromatogr A. 1154:230–239.
   PubMed Web of Science ®Google Scholar
• Chang H, Wang Y, Hu J. 2009. Determination and source apportionment of five classes of steroid hormones in urban rivers. Environ Sci Technol. 43:7691–7698.
   PubMed Web of Science ®Google Scholar
• Chen XQ, Jin YY, Tang G. 2007. New materia medica. 16th ed. [M]. Beijing: People’s Medical Publishing House; p. 622.
   Google Scholar
• Colosi DM, Bowden JA, Mora-Montero DC, Garrett TJ, Yost RA. 2009. Investigation of HPLC-MS using a monolithic column to separate a diverse suite of steroids. J Chromatogr Sci. 47:52–56.
   PubMed Web of Science ®Google Scholar
• Courant F, Antignac JP, Maume D, Monteau F, Andre F, Le Bizec B. 2007b. Determination of naturally occurring oestrogens and androgens in retail samples of milk and eggs. Food Addit Contam: Part A. 24:1358–1366.
   PubMed Web of Science ®Google Scholar
• Díaz-Bao M, Barreiro R, Regal P, Cepeda A, Fente C. 2012. Evaluation of molecularly imprinted polymers for the simultaneous SPE of six corticosteroids in milk. Chromatographia. 75:223–231.
   Web of Science ®Google Scholar
• Farré M, Brix R, Kuster M, Rubio F, Goda Y, López de Alda MJ, Barceló D. 2006. Evaluation of commercial immunoassays for the detection of estrogens in water by comparison with high-performance liquid chromatography tandem mass spectrometry HPLC–MS/MS (QqQ). Anal Bioanal Chem. 385:1001–1011.
   PubMed Web of Science ®Google Scholar
• Guo F, Liu Q, Qu GB, Song SJ, Sun JT, Shi JB, Jiang GB. 2013. Simultaneous determination of five estrogens and four androgens in water samples by online solid-phase extraction coupled with high-performance liquid chromatography-tandem mass spectrometry. J Chromatogr A. 1281:9–18.
   PubMed Web of Science ®Google Scholar
• Kataoka H, Matsuura E, Mitani K. 2007. Determination of cortisol in human saliva by automated in-tube solid-phase microextraction coupled with liquid chromatography-mass spectrometry. J Pharm Biomed Anal. 44:160–165.
   PubMed Web of Science ®Google Scholar
• Koal T, Schmiederer D, Pham-Tuan H, Röhring C, Rauh M. 2012. Standardized LC-MS/MS based steroid hormone profile-analysis. J Steroid Biochem Mol Biol. 129:129–138.
   PubMed Web of Science ®Google Scholar
• Lei YP, Yin S, Wu GP. 2009. Proprietary Chinese medicine and health food illegally added in adrenal cortical hormone drugs detection method research. J Traditional Chin Med Guides. 15:81–83.
   Google Scholar
• Li TM. 2009. Rational use of glucocorticoid. Rev Trad Chin Med. 6:165.
   Google Scholar
• Li YP, Gong L. 2008. Treatment and research status quo of anti-aging drugs. Shanxi Med J. 37:457–459.
   Google Scholar
• Nielen MWF, Van Engelen MC, Zuiderent R, Ramaker R. 2007. Screening and confirmation criteria for hormone residue analysis using liquid chromatography accurate mass time-of-flight, Fourier transform ion cyclotron resonance and orbitrap mass spectrometry techniques. Anal Chim Acta. 586:122–129.
   PubMed Web of Science ®Google Scholar
• Olędzka I, Kowalski P, Dziomba S, Szmudanowski P, Bączek T. 2013. Optimization of a Pre-MEKC separation SPE procedure for steroid molecules in human urine samples. Molecules. 18:14013–14032.
   PubMed Web of Science ®Google Scholar
• Poelmans S, De Wasch K, Noppe H, Van Hoof N, Van Cruchten S, Le Bizec B, Deceuninck Y, Sterk S, Van Rossum HJ, Hoffman MK, et al. 2005. Endogenous occurrence of some anabolic steroids in swine matrices. Food Addit Contam: Part A. 22:808–815.
   PubMedGoogle Scholar
• Qin F, Zhao YY, Sawyer MB, Li XF. 2008. Hydrophilic interaction liquid chromatography−tandem mass spectrometry determination of estrogen conjugates in human urine. Anal Chem. 80:3404–3411.
   PubMed Web of Science ®Google Scholar
• Regal P, Cepeda A, Fente C. 2012. Development of an LC-MS/MS method to quantify sex hormones in bovine milk and influence of pregnancy in their levels. Food Addit Contam: Part A. 29:770–779.
   PubMed Web of Science ®Google Scholar
• Scarth J, Akre C, Van Ginkel L, Le Bizec B, De Brabander H, Korth W, Points J, Teale P, Kay J. 2009. Presence and metabolism of endogenous androgenic-anabolic steroid hormones in meat-producing animals: a review. Food Addit Contam: Part A. 26:640–671.
   Web of Science ®Google Scholar
• Schlusener MP, Bester K. 2005. Determination of steroid hormones, hormone conjugates and macrolide antibiotics in influents and effluents of sewage treatment plants utilising high-performance liquid chromatography/tandem mass spectrometry with electrospray and atmospheric pressure chemical ionisation. Rapid Commun Mass Spectrom. 19:3269–3278.
   PubMed Web of Science ®Google Scholar
• Sharef OA, Feely J, Kavanagh PV, Scott KR, Sharma SC. 2007. An HPLC method for the determination of the free cortisol/cortisone ratio in human urine. Biomed Chromatogr. 21:1201–1206.
   PubMed Web of Science ®Google Scholar
• Snoj T, Dolenc J, Kobal S. 2014. Sex steroid levels in urine of cattle of different ages: evaluation of abuse control procedures. Food Addit Contam: Part A. 31:614–620.
   PubMed Web of Science ®Google Scholar
• Sun XS, Yang Y. 2009. The research progress of the anti-aging mechanism and drug. J Guangzhou Univ Trad Chin Med. 26:395–597.
   Google Scholar
• Trinh T, Harden NB, Coleman HM, Khan SJ. 2011. Simultaneous determination of estrogenic and androgenic hormones in water by isotope dilution gas chromatography–tandem mass spectrometry. J Chromatogr A. 1218:1668–1676.
   PubMed Web of Science ®Google Scholar
• Union E. 1996. Council Directive 96/22/EC of 29 April 1996 concerning the prohibition on the use in stock farming of certain substances having hormonal or tyrostatic action and of beta-agonists and replacing Directives 81/602/EEC, 88/146/EEC and 88/299/EEC. Off J Eur Union L. 125:3–9.
   Google Scholar
• Wang ML, Yan HF, Fu SL, Zhang F, Yao JT, Dai H, Li YJ. 2012. Rapid screening and confirmation of hormones in health foods by high performance liquid chromatography-ion trap-time of flight tandem mass spectrometry. Chin J Chromatogr. 30:980–985.
   Google Scholar
• Yang Y, Shao B, Zhang J, Wu YN, Duan HJ. 2009. Determination of the residues of 50 anabolic hormones in muscle, milk and liver by very-high-pressure liquid chromatography-electrospray ionization tandem mass spectrometry. J Chromatogr B. 877:489–496.
   PubMed Web of Science ®Google Scholar
• You YW, Uboh CE, Soma LR, Guan FY, Li XQ, Liu Y, Rudy JA, Chen JW, Tsang DB. 2011. Simultaneous separation and determination of 16 testosterone and nandrolone esters in equine plasma using ultra-high-performance liquid chromatography–tandem mass spectrometry for doping control. J Chromatogr A. 1218:3982–3993.
   PubMed Web of Science ®Google Scholar
• Zhang L, Chen J, He Y, Chi Y, Chen G. 2009. A new mixed micellar electrokinetic chromatography method for analysis of natural and synthetic anabolic steroids. Talanta. 77:1002–1008.
   PubMed Web of Science ®Google Scholar
• Zhang Y, Lan F, Zhang F, Shen JC, Chu XG. 2011. Determination of 41 hormones in cereal feeds by liquid chromatography-tandem mass spectrometry. Chin J Chromatogr. 29:523–534.
   Google Scholar
• Zhang AZ, Wang QL, Shen J, Zhang SF, Chen LR. 2010. Simultaneous determination of seven sex hormones in fish products using ultra performance liquid chromatography-tandem mass spectrometry. Chin J Chromatogr. 28:190–196.
   Google Scholar
• Zhang HC, Yu XJ, Yang WC, Peng JF, Xu T, Yin DQ, Hu XL. 2011. MCX based solid phase extraction combined with liquid chromatography tandem mass spectrometry for the simultaneous determination of 31 endocrine-disrupting compounds in surface water of Shanghai. J Chromatogr B. 879:2998–3004.
   PubMed Web of Science ®Google Scholar
• Zhong WX, Wang P, Zeng F. 2012. Determination of 6 adrenal corticostreroids illicitly added in Chinese traditional medicine or health-care foods by HPLC. Pharm Today. 22:282–284.
   Google Scholar