452
Views
7
CrossRef citations to date
0
Altmetric
Original Articles

Quantitative determination of sodium monofluoroacetate “1080” in infant formulas and dairy products by isotope dilution LC-MS/MS

, , , , , & show all
Pages 1885-1892 | Received 01 Jun 2015, Accepted 20 Aug 2015, Published online: 08 Oct 2015

References

  • Allender WJ. 1990. The determination of sodium monofluoroacetate (compound 1080) in formulation and technical samples by high pressure liquid chromatography. J Liq Chrom. 13:3465–3471.
  • Baron ML, Bothroyd CM, Rogers GI, Staffa A, Rae I. 1987. Detection and measurement of fluoroacetate in plant extracts by 19F NMR. Phytochemistry. 26:2293–2295.
  • Barwick VJ, Ellison SLR. 2000. Valid Analytical Measurement (VAM) project: development and harmonization of measurement uncertainty principles. Part d: protocol for uncertainty evaluation from validation data. LGC/VAM/1998/088. Teddington: LGC Limited.
  • Casper H, McMahon T, Paulson G. 1985. Capillary gas chromatography – mass spectrometry determination of fluoroacetate residues in animal tissues. J AOAC. 68:722–725.
  • Chen C-Y, Chang S-N, Wang G-S. 2009. Determination of ten haloacetic acids in drinking water using high-performance and ultra-performance liquid chromatography–tandem mass spectrometry. J Chrom Sci. 47:67–74.
  • Collins DM, Fawcett JP, Rammell CG. 1981. Determination of sodium fluoroacetate (compound 1080) in poison baits by HPLC. Bull Environ Contam Toxicol. 26:669–673.
  • Cook D, Lee ST, Taylor CM, Bassüner B, Riet-Correa F, Pfister JA, Gardner DR. 2014. Detection of toxic monofluoroacetate in Palicourea species. Toxicon. 80:9–16.
  • Demarchi ACCO, Menezes ML, Mercadante A, Vassillief I. 2001. Determination of the sodium monofluoroacetate in serum by gas chromatography. Chromatographia. 54:402–404.
  • Domino MM, Pepich BV, Munch DJ, Fair PS. 2004. Optimizing the determination of haloacetic acids in drinking waters. J Chrom A. 1035:9–16.
  • Eason C. 2002. Sodium monofluoroacetate (1080) risk assessment and risk communication. Toxicology. 181–182:523–530.
  • Eason C, Miller A, Ogilvie S, Fairweather A. 2011. An updated review of the toxicology and ecotoxicology of sodium fluoroacetate (1080) in relation to its use as a pest control tool in New Zealand. NZ J Ecol. 35:1–20.
  • European Union Commission Decision 2002/657/EC of 12 August 2002. implementing council Directive 96/23/EC concerning the performance of analytical methods and interpretation of results. Off J Eur Commun. [Internet]. [ cited 2014 Jan 10];L221:8–36. Available from: http://ec.europa.eu/food/food/chemicalsafety/residues/lab_analysis_en.htm
  • Giannitti F, Anderson M, Caspe SG, Mete A, East NE, Mostrom M, Poppenga R. 2013. An outbreak of sodium fluoroacetate (1080) intoxication in selenium- and copper-deficient sheep in California. Vet Pathol. 50:1022–1027.
  • Hamelin EI, Mawhinney DB, Parry R, Kobelskib RJ. 2010. Quantification of monofluoroacetate and monochloroacetate in human urine by isotope dilution liquid chromatography tandem mass spectrometry. J Chrom B. 878:1045–1050.
  • ISO 5725-2:. 1994 Accuracy (Trueness and Precision) of measurement methods and results; Part 2: basic method for the determination of repeatability and reproducibility of a standard measurement method.
  • Kimball BA, Mishalanie EA. 1993. Gas chromatographic determination of sodium monofluoroacetate as the free acid in an aqueous solvent. J Chrom. 634:289–296.
  • Koryagina NL, Savelieva EI, Khlebnikova NS, Goncharov NV, Jenkins RO, Radilov AS. 2006. Determination of fluoroacetic acid in water and biological samples by GC-FID and GC-MS in combination with solid-phase microextraction. Anal Bioanal Chem. 386:1395–1400.
  • Lee ST, Cook D, Pfister JA, Allen JG, Colegate SM, Riet-Correa F, Taylor CM. 2014. Monofluoroacetate-containing plants that are potentially toxic to livestock. J Agric Food Chem. 62:7345–7354.
  • Lee ST, Cook D, Riet-Correa F, Pfister JA, Anderson WR, Lima FG, Gardner DR. 2012. Detection of monofluoroacetate in Palicourea and Amorimia species. Toxicon. 60:791–796.
  • Loos R, Barcelo D. 2001. Determination of haloacetic acids in aqueous environments by solid-phase extraction followed by ion-pair liquid chromatography–electrospray ionization mass spectrometric detection. J Chrom A. 938:45–55.
  • Mori M, Nakajima H, Seto Y. 1996. Determination of fluoroacetate in aqueous samples by headspace gas chromatography. J Chrom A. 736:229–234.
  • New Zealand Government - Department of Conservation - 1080 information. 2015 Available from: http://www.doc.govt.nz/conservation/threats-and-impacts/animal-pests/methods-of-control/1080-poison-for-pest-control/#othercountries
  • Noonan GO, Begley TH, Diachenko GW. 2007. Rapid quantitative and qualitative confirmatory method for the determination of monofluoroacetic acid in foods by liquid chromatography–mass spectrometry. J Chrom A. 1139:271–278.
  • O’Hagan DO, Perry R, Lock JM, Meyer JJM, Dasaradhi L, Hamilton JTG, Harper DB. 1993. High levels of monofluoroacetate in Dichapetalum braunii. Phytochemistry. 33:1043−1045.
  • Ozawa H, Tsukioka T. 1987. Gas chromatographic determination of sodium monofluoroacetate in water by derivatization with dicyclohexylcarbodiimide. Anal Chem. 59:2914–2917.
  • Prieto-Blanco MC, Alpendurada MF, López-Mahía P, Muniategui-Lorenzo S, Prada-Rodríguez D, Machado S, Gonçalves C. 2012. Improving methodological aspects of the analysis of five regulated haloacetic acids in water samples by solid-phase extraction, ion-pair liquid chromatography and electrospray tandem mass spectrometry. Talanta. 94:90–98.
  • Proudfoot AT, Bradberry SM, Vale JA. 2006. Sodium fluoroacetate poisoning. Toxicol Rev. 25:213–219.
  • Guidance document on analytical quality control and validation procedures for pesticide residues analysis in food and feed. SANCO/12571/2013. Available from: http://ec.europa.eu/food/plant/pesticides/guidance_documents/docs/qualcontrol_en.pdf
  • Takino M, Daishima S, Yamaguchi K. 2000. Determination of haloacetic acids in water by liquid chromatography-electrospray ionization-mass spectrometry using volatile ion-pairing reagents. Analyst. 125:1097–1102.
  • The New Zealand Herald - New Zealand investigating threat to poison baby formula - Tuesday Mar 10, 2015. Available from: http://www.nzherald.co.nz/world/news/article.cfm?c_id=2&objectid=11415072
  • Tokarnia CH, Döbereiner J, Peixoto PV. 2002. Poisonous plants affecting livestock in Brazil. Toxicon. 40:1635–1660.
  • Vartiainen T, Kauranen P. 1984. The determination of traces of fluoroacetic acid by extractive alkylation, pentafluorobenzylation and capillary gas chromatography-mass spectrometry. Anal Chim Acta. 157:91–97.
  • Xie Y. 2001. Analyzing haloacetic acids using gas chromatography/mass spectrometry. Wat Res. 35:1599–1602.
  • Xie Z, Shi W, Liu L, Deng Q. 2007a. Determination of Sodium monofluoroacetate (1080) in Biological Samples as its 4-Bromomethyl-7-Methoxycoumarin Derivative by RP-HPLC. J Chrom Sci. 45:405–408.
  • Xie Z, Shi W, Liu L, Deng Q. 2007b. Quantitative analysis of monofluoroacetate in biological samples by high-performance liquid chromatography using fluorescence labeling with 9-chloromethylanthracene. J Chrom B. 857:53–58.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.