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Original Articles

High-throughput method for the determination of residues of β-lactam antibiotics in bovine milk by LC-MS/MS

, , , , &
Pages 1992-2001 | Received 04 Aug 2015, Accepted 20 Sep 2015, Published online: 15 Oct 2015

References

  • Becker M, Zittlau E, Petz M. 2003. Quantitative determination of ceftiofur-related residues in bovine raw milk by LC-MS/MS with electrospray ionization. Eur Food Res Technol. 217:449–456.
  • Becker M, Zittlau E, Petz M. 2004. Residue analysis of 15 penicillins and cephalosporins in bovine muscle, kidney and milk by liquid chromatography-tandem mass spectrometry. Anal Chim Acta. 520:19–32.
  • Bogialli S, Capitolino V, Curini R, Di Corcia A, Nazzari M, Sergi M. 2004. Simple and rapid liquid chromatography-tandem mass spectrometry confirmatory assay for determining amoxicillin and ampicillin in bovine tissues and milk. J Agric Food Chem. 52:3286–3291.
  • Bonfiglio R, King RC, Olah TV, Merkle K. 1999. The effects of sample preparation methods on the variability of the electrospray ionization response for model drug compounds. Rapid Commun Mass Spectrom. 13:1175–1185.
  • Brasil. Ministério da Agricultura Pecuária e Abastecimento. 2011. Manual de garantia da qualidade analítica. 1st ed. Brasília: MAPA/ACS.
  • Bruno F, Curini R, Di Corcia A, Nazzari M, Samperi R. 2001. Solid-phase extraction followed by liquid chromatography-mass spectrometry for trace determination of β-lactam antibiotics in bovine milk. J Agric Food Chem. 49:3463–3470.
  • De Queiroz Mauricio A, Lins ES. 2012. The national agricultural laboratories of Brazil and the control of residues and contaminants in food. Food Addit Contam Part Chem Anal Control Expo Risk Assess. 29:482–489.
  • European Commission. 2002. Commission decision 2002/657/EC of 12 August 2002: implementing council directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Comm. L221:8–36.
  • European Commission. 2010. Commission decision 2010/37/EC of 22 December 2009: on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin. Off J Eur Comm. L15:1–69.
  • Hoff RB, Rübensam G, Jank L, Barreto F, Ruaro Peralba MDC, Pizzolato TM, Díaz-Cruz MS, Barceló D. 2014. Analytical quality assurance in veterinary drug residue analysis methods: matrix effects determination and monitoring for sulfonamides analysis. 2015. Talanta. 132:443–450.
  • Jank L, Hoff RB, Tarouco PC, Barreto F, Pizzolato TM. 2012. β-lactam antibiotics residues analysis in bovine milk by LC-ESI-MS/MS: a simple and fast liquid-liquid extraction method. Food Addit Contam Part Chem Anal Control Expo Risk Assess. 29:497–507.
  • Kantiani L, Farré M, Barceló D. 2009a. Analytical methodologies for the detection of β-lactam antibiotics in milk and feed samples. TrAC - Trends Anal Chem. 28:729–744.
  • Kantiani L, Farré M, Sibum M, Postigo C, De Alda ML, Barceló D. 2009b. Fully automated analysis of β-lactams in bovine milk by online solid phase extraction-liquid chromatography-electrospray-tandem mass spectrometry. Anal Chem. 81:4285–4295.
  • Lara FJ, del Olmo-Iruela M, Cruces-Blanco C, Quesada-Molina C, García-Campaña AM. 2012. Advances in the determination of β-lactam antibiotics by liquid chromatography. TrAC - Trends Anal Chem. 38:52–66.
  • Ministério da Agricultura, Pecuária e Abastecimento (MAPA). 2014. Instrução Normativa SDA n° 11 of 07 May 2014. Brasília. Diário Of União; p. 5.
  • Pérez-Burgos R, Grzelak EM, Gokce G, Saurina J, Barbosa J, Barrón D. 2012. Quechers methodologies as an alternative to solid phase extraction (SPE) for the determination and characterization of residues of cephalosporins in beef muscle using LC-MS/MS. J Chromatogr B Analyt Technol Biomed Life Sci. 899:57–65.
  • Riediker S, Stadler RH. 2001. Simultaneous determination of five β-lactam antibiotics in bovine milk using liquid chromatography coupled with electrospray ionization tandem mass spectrometry. Anal Chem. 73:1614–1621.
  • Rübensam G, Barreto F, Hoff RB, Kist TL, Pizzolato TM. 2011. A liquid-liquid extraction procedure followed by a low temperature purification step for the analysis of macrocyclic lactones in milk by liquid chromatography-tandem mass spectrometry and fluorescence detection. Anal Chim Acta. 705:24–29.
  • Stolker AAM, Rutgers P, Oosterink E, Lasaroms JJP, Peters RJB, Van Rhijn JA, Nielen MWF. 2008. Comprehensive screening and quantification of veterinary drugs in milk using UPLC-ToF-MS. Anal Bioanal Chem. 391:2309–2322.

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