Micro-solid-phase extraction (µ-SPE) of organophosphorous pesticides from wheat followed by LC-MS/MS determination

References

• Aguilera-Luiz MM, Vidal JL, Romero-González R, Frenich AG. 2008. Multi-residue determination of veterinary drugs in milk by ultra-high-pressure liquid chromatography-tandem mass spectrometry. J Chrom A. 1205:10–16.
   PubMed Web of Science ®Google Scholar
• Ahmadi F, Shahsavari AA, Rahimi-Nasrabadi M. 2008. Automated extraction and preconcentration of multiresidue of pesticides on a micro-solid-phase extraction system based on polypyrrole as sorbent and off-line monitoring by gas chromatography–flame ionization detection. J Chrom A. 1193:26–31.
   PubMed Web of Science ®Google Scholar
• Anastassiades M, Lehotay SJ, Stajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and ‘dispersive solid-phase extraction’ for the determination of pesticide residues in produce. J AOAC Int. 86:412–431.
   PubMed Web of Science ®Google Scholar
• Androutsopoulos VP, Hernandez AF, Liesivuori J, Tsatsakis AM. 2013. .A mechanistic overview of health associated effects of low levels of organochlorine and organophosphorous pesticides. Toxicology. 307:89–94.
   PubMed Web of Science ®Google Scholar
• Augusto F, Hantao LW, Mogollón NGS, Braga SCGN. 2013. New materials and trends in sorbents for solid-phase extraction. TrAC Trends Anal Chem. 43:14–23.
   Web of Science ®Google Scholar
• Backe WJ, Jennifer A. 2012. Is SPE necessary for environmental analysis? A quantitative comparison of matrix effects from large-volume injection and solid-phase extraction based methods. Field Environ Sci Techn. 46:6750–6758.
   PubMed Web of Science ®Google Scholar
• Basheer C, Alnedhary AA, Rao BSM, Lee HK. 2009. Determination of carbamate pesticides using micro-solid-phase extraction combined with high-performance liquid chromatography. J Chrom A. 1216:211–216.
   PubMed Web of Science ®Google Scholar
• Basheer C, Narasimhan K, Yin M, Zhao C, Choolani M, Lee HK. 2008. Application of micro-solid-phase extraction for the determination of persistent organic pollutants in tissue samples. J Chrom A. 1186:358–364.
   PubMed Web of Science ®Google Scholar
• British Standard EN 15662. 2008. Foods of plant origin-determination of pesticide residues using GC–MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE-QuEChERS-method. Londra: British Standards Institution.
   Google Scholar
• Buszewski B, Szultka M. 2012. Past, present, and future of solid phase extraction: A review. Crit Rev Anal Chem. 42:198–213.
   Web of Science ®Google Scholar
• Cairns T, Luke MA, Chiu KS, Navarro KS, Siegmund E. 1993. Multiresidue pesticide analysis by ion-trap technology: A clean-up approach for mass spectral analysis. Rapid Commun Mass Spectrom. 7:1070–1076.
   Web of Science ®Google Scholar
• Dagnac T, Garcia-Chao M, Pulleiro P, Garcia-Jares C, Llompart M. 2009. Dispersive solid-phase extraction followed by liquid chromatography–tandem mass spectrometry for the multi-residue analysis of pesticides in raw bovine milk. J Chrom A. 1216:3702–3709.
   PubMed Web of Science ®Google Scholar
• Dardiotis E, Xiromerisiou G, Hadjichristodoulou C, Tsatsakis AM, Wilks MF, Hadjigeorgiou GM. 2013. The interplay between environmental and genetic factors in Parkinson’s disease susceptibility: The evidence for pesticides. Toxicology. 307:17–23.
   PubMed Web of Science ®Google Scholar
• Del Carlo M, Pepe A, Mascini M, De Gregorio M, Visconti A, Compagnone D. 2005. Determining pirimiphos-methyl in durum wheat samples using an acetylcholinesterase inhibition assay. Anal Bioanal Chem. 381:1367–1372.
   PubMed Web of Science ®Google Scholar
• Etemad L, Moshiri M, Moallem AD. 2014. Basic and clinical toxicology organophosphorus compound. London: Springer. Chapter 4, Chronic toxicity of organophosphorus compounds; p. 79–118.
   Google Scholar
• European Food Safety Authority (EFSA). 2011. EFSA J (Annu Rep.). 3:3130.
   Google Scholar
• González-Curbelo MÁ, Herrera-Herrera AV, Ravelo-Pérez LM, Hernández-Borges J. 2012. Sample-preparation methods for pesticide-residue analysis in cereals and derivatives. TrAC Trends Anal Chem. 38:32–51.
   Web of Science ®Google Scholar
• Guan H, Brewer WE, Garrias ST, Craft C, Morgan SL. 2010a. Multiresidue analysis of pesticides in fruits and vegetables using disposable pipette extraction (DPX) and micro-Luke method. J Agric Food Chem. 58:5973–5981.
   PubMed Web of Science ®Google Scholar
• Guan H, Brewer WE, Garrias ST, Morgan SL. 2010b. Disposable pipette extraction for the analysis of pesticides in fruit and vegetables using gas chromatography/mass spectrometry. J Chrom A. 1217:1867–1874.
   PubMed Web of Science ®Google Scholar
• Guan H, Brewer WE, Morgan SL. 2009. New approach to multiresidue pesticide determination in foods with high fat content using disposable pipette extraction (DPX) and gas chromatography–spectrometry (GC-MS). J Agric Food Chem. 57:10531–10538.
   PubMed Web of Science ®Google Scholar
• Hernández AF, Parrón T, Tsatsakis AM, Requena M, Alarcón R, López-Guarnido O. 2013. Toxic effects of pesticide mixtures at a molecular level: their relevance to human health. Toxicology. 307:136–145.
   PubMed Web of Science ®Google Scholar
• Huang J, Liu J, Zhang C, Wei J, Mei L, Yu S, Li G, Xu L. 2012. Determination of sulfonamides in food samples by membrane-protected micro-solid phase extraction coupled with high performance liquid chromatography. J Chrom A. 1219:66–74.
   PubMed Web of Science ®Google Scholar
• Huang Y, Zhou Q, Xie G. 2013. Development of sensitive determination method for fungicides from environmental water samples with Titanate nanotube array micro-solid phase extraction prior to high performance liquid chromatography. Chemosphere. 90:338–343.
   PubMed Web of Science ®Google Scholar
• Jin B, Xie L, Guo Y, Pang G. 2012. Multi-residue detection of pesticides in juice and fruit wine: A review of extraction and detection methods. Food Res Int. 46:399–409.
   Web of Science ®Google Scholar
• Khayoon WS, Saad B, Salleh B, Manaf NH, Latiff AA. 2014. Micro-solid phase extraction with liquid chromatography-tandem mass spectrometry for the determination of aflatoxins in coffee and malt beverage. Food Chem. 147:287–294.
   PubMed Web of Science ®Google Scholar
• Krause RT. 1980. Multiresidue method for determining N-methylcarbamate insecticides in crops using high performance liquid chromatography. J Assoc Off Anal Chem. 63:1114–1124.
   Google Scholar
• Kumazawa T, Hasegawa C, Lee X-P, Sato K. 2010. New and unique methods of solid-phase extraction for use before instrumental analysis of xenobiotics in human specimens. Forensic Toxicol. 28:61–68.
   Web of Science ®Google Scholar
• Lehotay SJ. 2007. Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study. J AOAC Int. 90:485–520.
   PubMed Web of Science ®Google Scholar
• Lehotay SJ, Mastovska K, Yun SJ. 2005. Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes. J AOAC Int. 88:630–638.
   PubMed Web of Science ®Google Scholar
• Luke MA, Froberg JE, Masumoto HT. 1975. Association of official analytical chemists. Extraction and cleanup of organochlorine, organophosphate, organonitrogen, and hydrocarbon pesticides in produce for determination by gas-liquid. J Assoc Off Anal Chem. 58:1020–1026.
   PubMedGoogle Scholar
• Luke MA, Froberg JE, Masumoto HT. 1981. Improved multiresidue gas chromatographic determination of organo-phosphorus, organonitrogen, and organohalogen pesticides in produce using flame photometric and electrolytic conductivity detectors. J Assoc Off Anal Chem. 64:1187–1195.
   PubMedGoogle Scholar
• Mascini M, Sergi M, Monti D, Del Carlo M, Compagnone D. 2008. Oligopeptides as mimic of acetylcholinesterase: from the rational design to the application in solid-phase extraction for pesticides. Anal Chem. 80:9150–9156.
   PubMed Web of Science ®Google Scholar
• Miyazaki S, Morisato K, Ishizuka N, Minakuchi H, Shintani Y, Furuno M, Nakanishi K. 2004. Development of a monolithic silica extraction tip for the analysis of proteins. J Chrom A. 1043:19–25.
   PubMed Web of Science ®Google Scholar
• Regulation (EC) No 396/. 2005. of the European parliament and of the council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin amending Council Directive 91/414/EEC. Off J Eur Union (16/3/2005).
   Google Scholar
• Saunders KC, Ghanem A, Hon WB, Hilder EF, Haddad PR. 2009. Separation and sample pre-treatment in bioanalysis using monolithic phases: A review. Anal. Chim Acta. 652:22–31.
   Web of Science ®Google Scholar
• Sawyer LD. 1985. The Luke et al. Method for determining multi-pesticide residues in fruits and vegetables: collaborative study. J Assoc Off Anal Chem. 68:64–71.
   PubMedGoogle Scholar
• Sergi M, Compagnone D, Curini R, D’Ascenzo G, Del Carlo M, Napoletano S, Risoluti R. 2010. Micro-solid phase extraction coupled with high-performance liquid chromatography–tandem mass spectrometry for the determination of stimulants, hallucinogens, ketamine and phencyclidine in oral fluids. Anal Chim Acta. 675:132–137.
   PubMed Web of Science ®Google Scholar
• Sergi M, Gentili A, Perret D, Marchese S, Materazzi S, Curini R. 2007. MSPD extraction of sulphonamides from meat followed by LC tandem MS. Chromatographia. 65:757–761.
   Web of Science ®Google Scholar
• Slotkin TA, Seidler FJ. 2012. Developmental neurotoxicity of organophosphates targets cell cycle and apoptosis, revealed by transcriptional profiles in vivo and in vitro. Neurotoxicol Teratol. 34:232–241.
   PubMed Web of Science ®Google Scholar
• Wang S. 2014. Food chemical hazard detection: development and application of new technologies. Oxford, UK: John Wiley & Sons.
   Google Scholar
• Wilkowska A, Biziuk M. 2011. Determination of pesticide residues in food matrices using the QuEChERS methodology. Food Chem. 125:803–812.
   Web of Science ®Google Scholar
• Zhang L, Liu S, Cui X, Pan C, Zhang A, Chen F. 2012. A review of sample preparation methods for the pesticide residue analysis in foods. Cent Eur J Chem. 10:900–925.
   Web of Science ®Google Scholar