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Original Articles

Multiresidue method for simultaneous analysis of aflatoxin M1, avermectins, organophosphate pesticides and milbemycin in milk by ultra-performance liquid chromatography coupled to tandem mass spectrometry

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Pages 995-1002 | Received 12 Feb 2016, Accepted 29 Mar 2016, Published online: 24 May 2016

References

  • Aguilera-Luiz MM, Plaza-Bolaños P, Vidal JLM, Romero-González R, Frenich A. 2011. Comparison of the efficiency of different extraction methods for the simultaneous determination of mycotoxins and pesticides in milk samples by ultra high-performance liquid chromatography-tandem mass spectrometry. Anal Bioanal Chem. 399:2863–2875.
  • Anastassiades M, Lehothay SJ, Stajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residue in produce. J AOAC Int. 86:412–431.
  • Antunes AEC, Pacheco MTB. 2009. Leite para adultos: mitos e fatos frente à ciência [Milk for adults: myths and facts front of the science]. São Paulo: Livraria Varella; p. 457. Portuguese.
  • Bastos LHP, Cardoso MHWM, Nóbrega AW, Jacob SC. 2011. Possíveis fontes de contaminação do alimento leite, por agrotóxicos, e estudos de monitoramento de seus resíduos: uma revisão nacional [Possible sources of milk contamination by pesticides, and monitoring studies of their residues: a national review]. Cad Saúde Colet. 19:51–60. Portuguese.
  • Beltrane MA, Machinski Júnior M. 2005. Principais riscos químicos no leite: um problema de saúde pública [Main Chemical Hazards in milk: a public health problem]. Arqu Ciênc Saúde Unipar. 9:141–145. Portuguese.
  • Biancardi A, Piro R, Dall’asta C, Galaverna G. 2013. A simple and reliable chomatography tandem mass spectrometry method for the determination of aflatoxin M1 in milk. Food Addit Contam. 30:381–388.
  • Brasil. Ministério da Agricultura Pecuária e Abastecimento [Internet]. 2011. Manual de garantia da qualidade analítica [Analytical quality assurance manual]. Ministério da Agricultura Pecuária e Abastecimento. Secretaria de Defesa Agropecuária. Brasília: MAPA/ACS; p. 227. Portuguese.
  • Brasil. Ministério da Agricultura, Pecuária e Abastecimento [Internet]. 2014. Instrução Normativa SDA nº 11 de 07 de maio de 2014. Publica o Subprograma de Monitoramento em Carnes (Bovina, Aves, Suína e Equina), Leite, Pescado, Mel, Ovos e Avestruz para o exercício de 2014, referente ao Plano Nacional de Controle de Resíduos e Contaminantes – PNCRC, na forma dos Anexos I e II a presente Instrução Normativa. Diário Oficial [da] República Federativa do Brasil. Brasília, DF, 07 mai. 2014. Seção 1. Available from: http://www.agricultura.gov.br/arq_editor/file/CRC/IN11-PNCRB2014
  • Brito LG. [Internet]. 2007. Carrapatograma: um aliado do produtor na exploração leiteira [Carrapatograma: an ally of the producer in the dairy farm]. In: Portal do Agronegócio, Embrapa Rondônia. Portuguese. Available from: http://www.portaldoagronegocio.com.br/conteudo.php?id=23487
  • Codex Alimentarius. 2015. General standard for contaminants and toxins in food and feed. Codex stan 193-1995. Amended in 2015; p. 1–59.
  • Commission Decision No. 657/2002. 2002. Implementing council directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Commun. L221:8–36.
  • Commission Regulation (EC) No. 1881/2006. 2006. Setting maximum levels for certain contaminants in foodstuffs. Off J Eur Commun. L364:5–24.
  • Durden DA. 2007. Positive and negative electrospray LC–MS–MS methods for quantitation of the anti-parasitic endectocides drugs, abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin and selamectin in milk. J Chromatogr B. 850:134–146.
  • Fernandes VC, Lehotay SJ, Geis-Asteggiante L, Kwon H, Mol HGJ, van der Kamp H, Mateus N, Domingues VF, Delerue-Matos C. 2014. Analysis of pesticides residues in strawberries and soils by GC-MS/MS, LC-MS/MS and two dimensional GC-time-of-flight MS comparing organic and integrated pest management farming. Food Addit Contam. 31:262–270.
  • [IARC] International Agency for Research on Cancer. [WHO] World Health Organization. 2002. IARC monographs on the evaluation of carcinogenic risks to humans. Some Tradition Herb Med, Some Mycotoxins, Naphthalene and Styrene. 82:183–193.
  • Maldaner L, Jardim ICSF. 2009. O estado da arte da cromatografia líquida de ultraeficiência [The art state of ultra performance liquid chromatography]. Quim Nova. 32:214–222. Portuguese.
  • Ortelli D, Cognard E, Jan P, Edder P. 2009. Comprehensive fast multiresidue screening of 150 veterinary drugs in milk by ultra-performance liquid chromatography coupled to time of flight mass spectrometry. J Chromatogr B. 877:2363–2374.
  • Prestes OD, Friggi CA, Adaime MB, Zanella R. 2009. QuECheRS –um método moderno de preparo de amostra para determinação multirresíduo de pesticidas em alimentos por métodos cromatográficos acoplados à espectrometria de massas [QuEChERS-a modern method of sample preparation for multiresidue determination of pesticides in food by chromatographic methods coupled to mass spectrometry]. Quim Nova. 32:1620–1634. Portuguese.
  • Rubensam G, Barreto F, Hoff RB, Kist TL, Pizzolatto TM. 2011. A liquid–liquid extraction procedure followed by a low temperature purification step for the analysis of macrocyclic lactones in milk by liquid chromatography–tandem mass spectrometry and fluorescence detection. Anal Chim Acta. 705:24–29.
  • Sindan. Sindicato Nacional da Indústria de Produtos para Saúde Animal [Internet]. 2015. Compêndio de produtos veterinários de uso permitido no Brasil [Compendium of veterinary products of allowed use in Brazil]. Available from: http://www.cpvs.com.br/cpvs/index.html. Portuguese.

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